Nano-Templates from Thermoresponsive Poly(ethoxytriethyleneglycol acrylate) for Polymeric Nano-Capsules

Temperature responsive poly(ethoxytriethyleneglycol acrylate) (PETEGA) of Mn = 8000 and Mw/Mn = 2.30 was synthesized by ATRP. Dilute aqueous solutions of PETEGA exhibit lower critical solution temperature (LCST) at around 34 °C. We found that PETEGA can form nano-sized uniform colloidal aggregates (...

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Published inMacromolecular symposia. Vol. 278; no. 1; pp. 89 - 95
Main Authors Dimitrov, Philip, Toncheva, Natalia, Weda, Pawel, Rangelov, Stanislav, Trzebicka, Barbara, Dworak, Andrzej, Tsvetanov, Christo B
Format Journal Article
LanguageEnglish
Published Weinheim Wiley-VCH Verlag 01.04.2009
WILEY-VCH Verlag
WILEY‐VCH Verlag
Subjects
Acrylamide
Acrylates
Aggregates
Core-shell particles
LCST
Manganese
nano-templates
Nanocomposites
Nanomaterials
Nanostructure
poly(ethoxytriethyleneglycol acrylate)
seeded free radical polymerization
stabilized core-shell particles
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Abstract Temperature responsive poly(ethoxytriethyleneglycol acrylate) (PETEGA) of Mn = 8000 and Mw/Mn = 2.30 was synthesized by ATRP. Dilute aqueous solutions of PETEGA exhibit lower critical solution temperature (LCST) at around 34 °C. We found that PETEGA can form nano-sized uniform colloidal aggregates (50-200 nm) above LCST either with or without an additional surfactant. Therefore PETEGA nano-aggregates were used as templates for the seeded free radical copolymerization of acrylamides or methacrylates together with a cross-linker to form acrylamide or methacrylate based core-shell particles. The formation of the PETEGA templates was investigated by dynamic light scattering (DLS) in order to find optimal conditions for obtaining narrow dispersed aggregates of desired sub-micron dimensions. Core-shell particles were characterized by DLS and scanning electron microscopy.
AbstractList Temperature responsive poly(ethoxytriethyleneglycol acrylate) (PETEGA) of Mn = 8000 and Mw/Mn = 2.30 was synthesized by ATRP. Dilute aqueous solutions of PETEGA exhibit lower critical solution temperature (LCST) at around 34 deg C. We found that PETEGA can form nano-sized uniform colloidal aggregates (50-200 nm) above LCST either with or without an additional surfactant. Therefore PETEGA nano-aggregates were used as templates for the seeded free radical copolymerization of acrylamides or methacrylates together with a cross-linker to form acrylamide or methacrylate based core-shell particles. The formation of the PETEGA templates was investigated by dynamic light scattering (DLS) in order to find optimal conditions for obtaining narrow dispersed aggregates of desired sub-micron dimensions. Core-shell particles were characterized by DLS and scanning electron microscopy.
Temperature responsive poly(ethoxytriethyleneglycol acrylate) (PETEGA) of Mn = 8000 and Mw/Mn = 2.30 was synthesized by ATRP. Dilute aqueous solutions of PETEGA exhibit lower critical solution temperature (LCST) at around 34 °C. We found that PETEGA can form nano‐sized uniform colloidal aggregates (50‐200 nm) above LCST either with or without an additional surfactant. Therefore PETEGA nano‐aggregates were used as templates for the seeded free radical copolymerization of acrylamides or methacrylates together with a cross‐linker to form acrylamide or methacrylate based core‐shell particles. The formation of the PETEGA templates was investigated by dynamic light scattering (DLS) in order to find optimal conditions for obtaining narrow dispersed aggregates of desired sub‐micron dimensions. Core‐shell particles were characterized by DLS and scanning electron microscopy.
Temperature responsive poly(ethoxytriethyleneglycol acrylate) (PETEGA) of Mn = 8000 and Mw/Mn = 2.30 was synthesized by ATRP. Dilute aqueous solutions of PETEGA exhibit lower critical solution temperature (LCST) at around 34 C. We found that PETEGA can form nano-sized uniform colloidal aggregates (50-200 nm) above LCST either with or without an additional surfactant. Therefore PETEGA nano-aggregates were used as templates for the seeded free radical copolymerization of acrylamides or methacrylates together with a cross-linker to form acrylamide or methacrylate based core-shell particles. The formation of the PETEGA templates was investigated by dynamic light scattering (DLS) in order to find optimal conditions for obtaining narrow dispersed aggregates of desired sub-micron dimensions. Core-shell particles were characterized by DLS and scanning electron microscopy.
Abstract Temperature responsive poly(ethoxytriethyleneglycol acrylate) (PETEGA) of Mn = 8000 and M w /M n  = 2.30 was synthesized by ATRP. Dilute aqueous solutions of PETEGA exhibit lower critical solution temperature (LCST) at around 34 °C. We found that PETEGA can form nano‐sized uniform colloidal aggregates (50‐200 nm) above LCST either with or without an additional surfactant. Therefore PETEGA nano‐aggregates were used as templates for the seeded free radical copolymerization of acrylamides or methacrylates together with a cross‐linker to form acrylamide or methacrylate based core‐shell particles. The formation of the PETEGA templates was investigated by dynamic light scattering (DLS) in order to find optimal conditions for obtaining narrow dispersed aggregates of desired sub‐micron dimensions. Core‐shell particles were characterized by DLS and scanning electron microscopy.
Author Rangelov, Stanislav
Dworak, Andrzej
Dimitrov, Philip
Tsvetanov, Christo B.
Toncheva, Natalia
Weda, Pawel
Trzebicka, Barbara
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Snippet Temperature responsive poly(ethoxytriethyleneglycol acrylate) (PETEGA) of Mn = 8000 and Mw/Mn = 2.30 was synthesized by ATRP. Dilute aqueous solutions of...
Temperature responsive poly(ethoxytriethyleneglycol acrylate) (PETEGA) of Mn = 8000 and Mw/Mn = 2.30 was synthesized by ATRP. Dilute aqueous solutions of...
Abstract Temperature responsive poly(ethoxytriethyleneglycol acrylate) (PETEGA) of Mn = 8000 and M w /M n  = 2.30 was synthesized by ATRP. Dilute aqueous...
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SubjectTerms Acrylamide
Acrylates
Aggregates
Core-shell particles
LCST
Manganese
nano-templates
Nanocomposites
Nanomaterials
Nanostructure
poly(ethoxytriethyleneglycol acrylate)
seeded free radical polymerization
stabilized core-shell particles
Title Nano-Templates from Thermoresponsive Poly(ethoxytriethyleneglycol acrylate) for Polymeric Nano-Capsules
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