Investigation of Ni-Mo and Co-Mo alloys electrodeposition involving choline chloride based ionic liquids
The paper presents several experimental results regarding the electrodeposition of Ni-Mo and Co-Mo alloy coatings from choline chloride based ionic liquids, applied onto Cu metallic substrates. Electrolytes containing Ni2+, Co2+ and Mo6+ salts in choline chloride – urea – citric acid ternary mixture...
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| Published in | Electrochimica acta Vol. 207; pp. 97 - 111 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
20.07.2016
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| Subjects | |
| Online Access | Get full text |
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| Abstract | The paper presents several experimental results regarding the electrodeposition of Ni-Mo and Co-Mo alloy coatings from choline chloride based ionic liquids, applied onto Cu metallic substrates. Electrolytes containing Ni2+, Co2+ and Mo6+ salts in choline chloride – urea – citric acid ternary mixtures have been taken into consideration.
The electrodeposited Ni-Mo and Co-Mo alloy coatings were adherent and uniform onto Cu metallic substrate. Ni-Mo alloys containing 2–35wt. % Mo and Co-Mo alloys with 6–63wt. % Mo have been obtained, depending on the metallic ions mass ratio and on the value of current density. As SEM analysis revealed, the operating parameters significantly influence the surface morphology of the obtained alloy coatings.
According to XRD analysis, both electrochemical alloy coatings showed a nanocrystalline structure, having crystallites average sizes in the range of 3–7nm.
The alloy coatings corrosion performance has also been discussed. |
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| AbstractList | The paper presents several experimental results regarding the electrodeposition of Ni-Mo and Co-Mo alloy coatings from choline chloride based ionic liquids, applied onto Cu metallic substrates. Electrolytes containing Ni super(2+), Co super(2+) and Mo super(6+) salts in choline chloride - urea - citric acid ternary mixtures have been taken into consideration. The electrodeposited Ni-Mo and Co-Mo alloy coatings were adherent and uniform onto Cu metallic substrate. Ni-Mo alloys containing 2-35 wt. % Mo and Co-Mo alloys with 6-63 wt. % Mo have been obtained, depending on the metallic ions mass ratio and on the value of current density. As SEM analysis revealed, the operating parameters significantly influence the surface morphology of the obtained alloy coatings. According to XRD analysis, both electrochemical alloy coatings showed a nanocrystalline structure, having crystallites average sizes in the range of 3-7 nm. The alloy coatings corrosion performance has also been discussed. The paper presents several experimental results regarding the electrodeposition of Ni-Mo and Co-Mo alloy coatings from choline chloride based ionic liquids, applied onto Cu metallic substrates. Electrolytes containing Ni2+, Co2+ and Mo6+ salts in choline chloride – urea – citric acid ternary mixtures have been taken into consideration. The electrodeposited Ni-Mo and Co-Mo alloy coatings were adherent and uniform onto Cu metallic substrate. Ni-Mo alloys containing 2–35wt. % Mo and Co-Mo alloys with 6–63wt. % Mo have been obtained, depending on the metallic ions mass ratio and on the value of current density. As SEM analysis revealed, the operating parameters significantly influence the surface morphology of the obtained alloy coatings. According to XRD analysis, both electrochemical alloy coatings showed a nanocrystalline structure, having crystallites average sizes in the range of 3–7nm. The alloy coatings corrosion performance has also been discussed. |
| Author | Anicai, Liana Manea, Adrian-Cristian Costovici, Stefania Visan, Teodor |
| Author_xml | – sequence: 1 givenname: Stefania surname: Costovici fullname: Costovici, Stefania organization: Center of Surface Science and Nanotechnology, University Politehnica of Bucharest, Splaiul Independentei 313, Bucharest, 060042, Romania – sequence: 2 givenname: Adrian-Cristian surname: Manea fullname: Manea, Adrian-Cristian organization: Department of Inorganic Chemistry, Physical Chemistry and Electrochemistry, Faculty of Applied Chemistry and Materials Science, University Politehnica of Bucharest, 132 Calea Grivitei, Romania, 010737, Romania – sequence: 3 givenname: Teodor surname: Visan fullname: Visan, Teodor organization: Department of Inorganic Chemistry, Physical Chemistry and Electrochemistry, Faculty of Applied Chemistry and Materials Science, University Politehnica of Bucharest, 132 Calea Grivitei, Romania, 010737, Romania – sequence: 4 givenname: Liana surname: Anicai fullname: Anicai, Liana email: lanicai@itcnet.ro, lanicai@hotmail.com organization: Center of Surface Science and Nanotechnology, University Politehnica of Bucharest, Splaiul Independentei 313, Bucharest, 060042, Romania |
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| SubjectTerms | Alloys Chlorides Choline Co-Mo alloy Coatings Cobalt base alloys Copper corrosion behavior electrodeposition Ionic liquids Ni-Mo alloy Nickel base alloys |
| Title | Investigation of Ni-Mo and Co-Mo alloys electrodeposition involving choline chloride based ionic liquids |
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