PLA-PHB/cellulose based films: Mechanical, barrier and disintegration properties
Nanocomposite films based on poly(lactic acid)-poly(hydroxybutyrate) (PLA-PHB) blends and synthesized cellulose nanocrystals (CNC) or surfactant modified cellulose nanocrystals (CNCs), as bio-based reinforcement, were prepared by melt extrusion followed by film forming. The obtained nanocomposites a...
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| Published in | Polymer degradation and stability Vol. 107; pp. 139 - 149 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Kidlington
Elsevier Ltd
01.09.2014
Elsevier |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Nanocomposite films based on poly(lactic acid)-poly(hydroxybutyrate) (PLA-PHB) blends and synthesized cellulose nanocrystals (CNC) or surfactant modified cellulose nanocrystals (CNCs), as bio-based reinforcement, were prepared by melt extrusion followed by film forming. The obtained nanocomposites are intended for short-term food packaging. Thus, the mechanical, optical, barrier and wettability properties were studied. Functionalized CNCs contribute to enhance the interfacial adhesion between PLA and PHB, leading to improved mechanical stiffness and increased film stretchability. The synergic effects of the PHB and CNCs on the PLA barrier properties were confirmed by increases in oxygen barrier properties and reductions in surface wettability of the nanocomposites. In addition, the measurements of the viscosity molecular weight for ternary systems showed practically no degradation of PLA and smaller degradation of PHB during processing due to nanocrystal presence. The disintegration process in composting conditions of PLA was delayed by the addition of PHB, while CNC speeded it up. PLA-PHB-CNCs formulations showed enhanced mechanical performance, improved water resistance, reduced oxygen and UV-light transmission, as well as appropriate disintegration in compost suggesting possible applications as packaging materials. |
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| AbstractList | Nanocomposite films based on poly(lactic acid)-poly(hydroxybutyrate) (PLA-PHB) blends and synthesized cellulose nanocrystals (CNC) or surfactant modified cellulose nanocrystals (CNCs), as bio-based reinforcement, were prepared by melt extrusion followed by film forming. The obtained nanocomposites are intended for short-term food packaging. Thus, the mechanical, optical, barrier and wettability properties were studied. Functionalized CNCs contribute to enhance the interfacial adhesion between PLA and PHB, leading to improved mechanical stiffness and increased film stretchability. The synergic effects of the PHB and CNCs on the PLA barrier properties were confirmed by increases in oxygen barrier properties and reductions in surface wettability of the nanocomposites. In addition, the measurements of the viscosity molecular weight for ternary systems showed practically no degradation of PLA and smaller degradation of PHB during processing due to nanocrystal presence. The disintegration process in composting conditions of PLA was delayed by the addition of PHB, while CNC speeded it up. PLA-PHB-CNCs formulations showed enhanced mechanical performance, improved water resistance, reduced oxygen and UV-light transmission, as well as appropriate disintegration in compost suggesting possible applications as packaging materials. |
| Author | Rayón, E. Arrieta, M.P. Fortunati, E. López, J. Kenny, J.M. Dominici, F. |
| Author_xml | – sequence: 1 givenname: M.P. orcidid: 0000-0003-1816-011X surname: Arrieta fullname: Arrieta, M.P. organization: Instituto de Tecnología de Materiales, Universitat Politècnica de Valencia, 03801 Alcoy, Alicante, Spain – sequence: 2 givenname: E. surname: Fortunati fullname: Fortunati, E. email: elena.fortunati@unipg.it organization: Materials Engineering Centre, UdR INSTM, NIPLAB, University of Perugia, 05100 Terni, Italy – sequence: 3 givenname: F. surname: Dominici fullname: Dominici, F. organization: Materials Engineering Centre, UdR INSTM, NIPLAB, University of Perugia, 05100 Terni, Italy – sequence: 4 givenname: E. surname: Rayón fullname: Rayón, E. organization: Instituto de Tecnología de Materiales, Universitat Politècnica de Valencia, E-46022 Valencia, Spain – sequence: 5 givenname: J. orcidid: 0000-0001-6904-2282 surname: López fullname: López, J. organization: Instituto de Tecnología de Materiales, Universitat Politècnica de Valencia, 03801 Alcoy, Alicante, Spain – sequence: 6 givenname: J.M. surname: Kenny fullname: Kenny, J.M. organization: Materials Engineering Centre, UdR INSTM, NIPLAB, University of Perugia, 05100 Terni, Italy |
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| SubjectTerms | adhesion Application fields Applied sciences Barrier properties Biodegradation Biological and medical sciences cellulose Composites composting Exact sciences and technology extrusion Food industries food packaging Forms of application and semi-finished materials Fundamental and applied biological sciences. Psychology General aspects Handling, storage, packaging, transport melting Modified cellulose nanocrystals molecular weight Nanocomposites nanocrystals oxygen packaging materials Poly(hydroxybutyrate) Poly(lactic acid) polylactic acid Polymer industry, paints, wood surfactants synergism Technology of polymers ultraviolet radiation viscosity wettability |
| Title | PLA-PHB/cellulose based films: Mechanical, barrier and disintegration properties |
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