Multiwalled carbon nanotubes as adsorbents for removal of herbicide diuron from aqueous solution

► The pseudo-second-order model can well describe the adsorption performance of diuron onto MWCNTs. ► The Polanyi–Manes isotherm showed the best fitting with the equilibrium data. ► The thermodynamic parameters indicated that the adsorption of diuron onto MWCNTs was spontaneous and exothermic. ► The...

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Published inChemical engineering journal (Lausanne, Switzerland : 1996) Vol. 193-194; pp. 339 - 347
Main Authors Deng, Jing, Shao, Yisheng, Gao, Naiyun, Deng, Yang, Tan, Chaoqun, Zhou, Shiqing, Hu, Xuhao
Format Journal Article
LanguageEnglish
Published Oxford Elsevier B.V 15.06.2012
Elsevier
Subjects
adsorbents
Adsorption
Applied sciences
carbon nanotubes
Chemical engineering
Cu2
Diuron
Exact sciences and technology
heat production
Multiwalled carbon nanotubes (MWCNTs)
Polanyi–Manes model
surface area
temperature
pH
Cu2
Diuron
Polanyi–Manes model
Adsorption
Multiwalled carbon nanotubes (MWCNTs)
Second order
Correlation
Pesticides
Modeling
Herbicide
Cu
Batchwise
Correlation analysis
Polanyi-Manes model
Aqueous solution
Surface area
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Abstract ► The pseudo-second-order model can well describe the adsorption performance of diuron onto MWCNTs. ► The Polanyi–Manes isotherm showed the best fitting with the equilibrium data. ► The thermodynamic parameters indicated that the adsorption of diuron onto MWCNTs was spontaneous and exothermic. ► The adsorption of diuron onto MWCNTs was found to be pH dependent and favorable under neutral and basic conditions. ► The presence of Cu2+ had different effect on the adsorption of diuron onto as-prepared and oxidized MWCNTs. The adsorption of diuron onto as-prepared and oxidized multiwalled carbon nanotubes (MWCNTs) from aqueous solution has been studied through batch experiments, in which the effect of contact time, temperature, pH and coexisting Cu2+ were investigated. The adsorption performance of diuron onto MWCNTs fitted the pseudo-second-order model and apparent equilibrium was reached within 1h. The experimental data showed good correlation with Freundlich, Langmuir and Polanyi–Manes models in the range of experimental concentrations, but followed Polanyi–Manes model most appropriate. The calculated thermodynamic parameters showed adsorption of diuron onto MWCNTs was exothermic and spontaneous. Except for the introduction of oxygen-containing functional groups onto the surfaces of MWCNTs, the oxidized treatment of as-prepared MWCNTs can also increase the surface area and the pore volume, which resulted in the increase adsorption of diuron in this study. The adsorption of diuron was found to be pH dependent, and more adsorption was observed under neutral and basic conditions. The presence of Cu2+ has no significant effect on the adsorption of diuron onto as-prepared MWCNTs, on the contrary, the presence of Cu2+ can greatly decrease the adsorption of diuron onto oxidized MWCNTs. In addition, competitive adsorption was greater at higher than at lower diuron concentrations.
AbstractList The adsorption of diuron onto as-prepared and oxidized multiwalled carbon nanotubes (MWCNTs) from aqueous solution has been studied through batch experiments, in which the effect of contact time, temperature, pH and coexisting Cu2+ were investigated. The adsorption performance of diuron onto MWCNTs fitted the pseudo-second-order model and apparent equilibrium was reached within 1 h. The experimental data showed good correlation with Freundlich, Langmuir and Polanyi-Manes models in the range of experimental concentrations, but followed Polanyi-Manes model most appropriate. The calculated thermodynamic parameters showed adsorption of diuron onto MWCNTs was exothermic and spontaneous. Except for the introduction of oxygen-containing functional groups onto the surfaces of MWCNTs, the oxidized treatment of as-prepared MWCNTs can also increase the surface area and the pore volume, which resulted in the increase adsorption of diuron in this study. The adsorption of diuron was found to be pH dependent, and more adsorption was observed under neutral and basic conditions. The presence of Cu2+ has no significant effect on the adsorption of diuron onto as-prepared MWCNTs, on the contrary, the presence of Cu2+ can greatly decrease the adsorption of diuron onto oxidized MWCNTs. In addition, competitive adsorption was greater at higher than at lower diuron concentrations.
► The pseudo-second-order model can well describe the adsorption performance of diuron onto MWCNTs. ► The Polanyi–Manes isotherm showed the best fitting with the equilibrium data. ► The thermodynamic parameters indicated that the adsorption of diuron onto MWCNTs was spontaneous and exothermic. ► The adsorption of diuron onto MWCNTs was found to be pH dependent and favorable under neutral and basic conditions. ► The presence of Cu2+ had different effect on the adsorption of diuron onto as-prepared and oxidized MWCNTs. The adsorption of diuron onto as-prepared and oxidized multiwalled carbon nanotubes (MWCNTs) from aqueous solution has been studied through batch experiments, in which the effect of contact time, temperature, pH and coexisting Cu2+ were investigated. The adsorption performance of diuron onto MWCNTs fitted the pseudo-second-order model and apparent equilibrium was reached within 1h. The experimental data showed good correlation with Freundlich, Langmuir and Polanyi–Manes models in the range of experimental concentrations, but followed Polanyi–Manes model most appropriate. The calculated thermodynamic parameters showed adsorption of diuron onto MWCNTs was exothermic and spontaneous. Except for the introduction of oxygen-containing functional groups onto the surfaces of MWCNTs, the oxidized treatment of as-prepared MWCNTs can also increase the surface area and the pore volume, which resulted in the increase adsorption of diuron in this study. The adsorption of diuron was found to be pH dependent, and more adsorption was observed under neutral and basic conditions. The presence of Cu2+ has no significant effect on the adsorption of diuron onto as-prepared MWCNTs, on the contrary, the presence of Cu2+ can greatly decrease the adsorption of diuron onto oxidized MWCNTs. In addition, competitive adsorption was greater at higher than at lower diuron concentrations.
The adsorption of diuron onto as-prepared and oxidized multiwalled carbon nanotubes (MWCNTs) from aqueous solution has been studied through batch experiments, in which the effect of contact time, temperature, pH and coexisting Cu²⁺ were investigated. The adsorption performance of diuron onto MWCNTs fitted the pseudo-second-order model and apparent equilibrium was reached within 1h. The experimental data showed good correlation with Freundlich, Langmuir and Polanyi–Manes models in the range of experimental concentrations, but followed Polanyi–Manes model most appropriate. The calculated thermodynamic parameters showed adsorption of diuron onto MWCNTs was exothermic and spontaneous. Except for the introduction of oxygen-containing functional groups onto the surfaces of MWCNTs, the oxidized treatment of as-prepared MWCNTs can also increase the surface area and the pore volume, which resulted in the increase adsorption of diuron in this study. The adsorption of diuron was found to be pH dependent, and more adsorption was observed under neutral and basic conditions. The presence of Cu²⁺ has no significant effect on the adsorption of diuron onto as-prepared MWCNTs, on the contrary, the presence of Cu²⁺ can greatly decrease the adsorption of diuron onto oxidized MWCNTs. In addition, competitive adsorption was greater at higher than at lower diuron concentrations.
Author Zhou, Shiqing
Deng, Jing
Deng, Yang
Shao, Yisheng
Hu, Xuhao
Gao, Naiyun
Tan, Chaoqun
Author_xml – sequence: 1
  givenname: Jing
  surname: Deng
  fullname: Deng, Jing
  organization: State Key Laboratory of Pollution Control Reuse, Tongji University, Shanghai 200092, China
– sequence: 2
  givenname: Yisheng
  surname: Shao
  fullname: Shao, Yisheng
  email: shaoyisheng2011@163.com
  organization: State Key Laboratory of Pollution Control Reuse, Tongji University, Shanghai 200092, China
– sequence: 3
  givenname: Naiyun
  surname: Gao
  fullname: Gao, Naiyun
  organization: State Key Laboratory of Pollution Control Reuse, Tongji University, Shanghai 200092, China
– sequence: 4
  givenname: Yang
  surname: Deng
  fullname: Deng, Yang
  organization: Department of Earth and Environmental Studies, Montclair State University, Montclair, NJ 07043, USA
– sequence: 5
  givenname: Chaoqun
  surname: Tan
  fullname: Tan, Chaoqun
  organization: State Key Laboratory of Pollution Control Reuse, Tongji University, Shanghai 200092, China
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– sequence: 7
  givenname: Xuhao
  surname: Hu
  fullname: Hu, Xuhao
  organization: State Key Laboratory of Pollution Control Reuse, Tongji University, Shanghai 200092, China
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Keywords pH
Cu2
Diuron
Polanyi–Manes model
Adsorption
Multiwalled carbon nanotubes (MWCNTs)
Second order
Correlation
Pesticides
Modeling
Herbicide
Cu
Batchwise
Correlation analysis
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Aqueous solution
Surface area
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Snippet ► The pseudo-second-order model can well describe the adsorption performance of diuron onto MWCNTs. ► The Polanyi–Manes isotherm showed the best fitting with...
The adsorption of diuron onto as-prepared and oxidized multiwalled carbon nanotubes (MWCNTs) from aqueous solution has been studied through batch experiments,...
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SubjectTerms adsorbents
Adsorption
Applied sciences
carbon nanotubes
Chemical engineering
Cu2
Diuron
Exact sciences and technology
heat production
Multiwalled carbon nanotubes (MWCNTs)
Polanyi–Manes model
surface area
temperature
Title Multiwalled carbon nanotubes as adsorbents for removal of herbicide diuron from aqueous solution
URI https://dx.doi.org/10.1016/j.cej.2012.04.051
https://search.proquest.com/docview/1038602399
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