Fabrication of Superhydrophobic Magnetic Sawdust as Effective and Recyclable Oil Sorbents

In this paper, a novel superhydrophobic magnetic sawdust (SMSD) was fabricated as an oil sorbent. The SMSD was functionalized with Fe3O4 nanoparticles using melamine formaldehyde resin (MFR) as a coupling agent and subsequently hydrophobically-treated with hexadecyltrimethoxysilane (HDTMS). The SMSD...

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Published inMaterials Vol. 12; no. 20; p. 3432
Main Authors Fan, Shumin, Pei, Shuai, Shen, Tianyu, Xu, Guangri, Li, Yuanchao, Fan, Wenxiu
Format Journal Article
LanguageEnglish
Published Basel MDPI AG 20.10.2019
MDPI
Subjects
Absorption
Activated carbon
Contact angle
emulsion separation
Ethanol
Fourier transforms
Hydrophobic surfaces
Hydrophobicity
Iron oxides
magnetic
Morphology
Nanoparticles
oil absorption
Oil spills
Organic chemistry
Organic materials
Porous materials
Sawdust
Sorbents
Spectrum analysis
Stretching
superhydrophobic
Vibration
Water pollution
United States > US
China
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Abstract In this paper, a novel superhydrophobic magnetic sawdust (SMSD) was fabricated as an oil sorbent. The SMSD was functionalized with Fe3O4 nanoparticles using melamine formaldehyde resin (MFR) as a coupling agent and subsequently hydrophobically-treated with hexadecyltrimethoxysilane (HDTMS). The SMSD showed excellent superhydrophobicity with the water contact angle of 155.3 ± 0.9°. Meanwhile it had remarkable environmental durability, long-term stability, and mechanical durable properties. Taking advantage of its magnetic characteristics, the SMSD could be easily controlled to absorb oil to separate oil–water mixtures with high oil absorption capacity and good reusability. Moreover, the emulsion was successfully separated by SMSD, including water-in-oil and oil-in-water emulsions. This study developed an effective oil absorbent, which was low cost and environmentally-friendly.
AbstractList In this paper, a novel superhydrophobic magnetic sawdust (SMSD) was fabricated as an oil sorbent. The SMSD was functionalized with Fe3O4 nanoparticles using melamine formaldehyde resin (MFR) as a coupling agent and subsequently hydrophobically-treated with hexadecyltrimethoxysilane (HDTMS). The SMSD showed excellent superhydrophobicity with the water contact angle of 155.3 ± 0.9°. Meanwhile it had remarkable environmental durability, long-term stability, and mechanical durable properties. Taking advantage of its magnetic characteristics, the SMSD could be easily controlled to absorb oil to separate oil–water mixtures with high oil absorption capacity and good reusability. Moreover, the emulsion was successfully separated by SMSD, including water-in-oil and oil-in-water emulsions. This study developed an effective oil absorbent, which was low cost and environmentally-friendly.
Introduction Oil spill problems have become more and more serious in water pollution, which is a major threat to human life and the ecosystem [1,2,3,4]. [...]more and more attention has been paid to efficient absorbent materials for oil spill pollution, such as porous materials, activated carbon, chemical synthetic organic materials, and oil absorption resin [5]. The Fe3O4 nanoparticles were wrapped in viscid MFR by a structure of MFR–Fe3O4 nanoparticles –MFR. [...]Fe3O4 nanoparticles could tightly adhere to the sawdust. 2.2.3. [...]the fiber structure of sawdust could still be observed. The asymmetric and symmetric stretching vibrations of –CH2 and –CH3 were at 2920 cm−1 and 2851 cm−1, confirming the existence of HDTMS. [...]the small absorption peaks around 1100 cm−1 and 800 cm−1 observed in SMSD corresponded to the Si–O–Si and C–Si stretching vibration of HDTMS, which was overlapped by the C–O stretching vibration of the sawdust.
In this paper, a novel superhydrophobic magnetic sawdust (SMSD) was fabricated as an oil sorbent. The SMSD was functionalized with Fe 3 O 4 nanoparticles using melamine formaldehyde resin (MFR) as a coupling agent and subsequently hydrophobically-treated with hexadecyltrimethoxysilane (HDTMS). The SMSD showed excellent superhydrophobicity with the water contact angle of 155.3 ± 0.9°. Meanwhile it had remarkable environmental durability, long-term stability, and mechanical durable properties. Taking advantage of its magnetic characteristics, the SMSD could be easily controlled to absorb oil to separate oil–water mixtures with high oil absorption capacity and good reusability. Moreover, the emulsion was successfully separated by SMSD, including water-in-oil and oil-in-water emulsions. This study developed an effective oil absorbent, which was low cost and environmentally-friendly.
In this paper, a novel superhydrophobic magnetic sawdust (SMSD) was fabricated as an oil sorbent. The SMSD was functionalized with Fe3O4 nanoparticles using melamine formaldehyde resin (MFR) as a coupling agent and subsequently hydrophobically-treated with hexadecyltrimethoxysilane (HDTMS). The SMSD showed excellent superhydrophobicity with the water contact angle of 155.3 ± 0.9°. Meanwhile it had remarkable environmental durability, long-term stability, and mechanical durable properties. Taking advantage of its magnetic characteristics, the SMSD could be easily controlled to absorb oil to separate oil−water mixtures with high oil absorption capacity and good reusability. Moreover, the emulsion was successfully separated by SMSD, including water-in-oil and oil-in-water emulsions. This study developed an effective oil absorbent, which was low cost and environmentally-friendly.
Author Xu, Guangri
Li, Yuanchao
Shen, Tianyu
Fan, Wenxiu
Fan, Shumin
Pei, Shuai
AuthorAffiliation School of Chemistry and Chemical Engineering, Henan Institute of Science and Technology, Xinxiang 453003, Henan, China xugr70@163.com (G.X.); liyuanchaozzu@126.com (Y.L.)
AuthorAffiliation_xml – name: School of Chemistry and Chemical Engineering, Henan Institute of Science and Technology, Xinxiang 453003, Henan, China xugr70@163.com (G.X.); liyuanchaozzu@126.com (Y.L.)
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Snippet In this paper, a novel superhydrophobic magnetic sawdust (SMSD) was fabricated as an oil sorbent. The SMSD was functionalized with Fe3O4 nanoparticles using...
Introduction Oil spill problems have become more and more serious in water pollution, which is a major threat to human life and the ecosystem [1,2,3,4]....
In this paper, a novel superhydrophobic magnetic sawdust (SMSD) was fabricated as an oil sorbent. The SMSD was functionalized with Fe 3 O 4 nanoparticles using...
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StartPage 3432
SubjectTerms Absorption
Activated carbon
Contact angle
emulsion separation
Ethanol
Fourier transforms
Hydrophobic surfaces
Hydrophobicity
Iron oxides
magnetic
Morphology
Nanoparticles
oil absorption
Oil spills
Organic chemistry
Organic materials
Porous materials
Sawdust
Sorbents
Spectrum analysis
Stretching
superhydrophobic
Vibration
Water pollution
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Title Fabrication of Superhydrophobic Magnetic Sawdust as Effective and Recyclable Oil Sorbents
URI https://www.proquest.com/docview/2333416972
https://search.proquest.com/docview/2307729612
https://pubmed.ncbi.nlm.nih.gov/PMC6829461
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Volume 12
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