Synthesis and Electrochemical Performance of V6O13 Nanosheets Film Cathodes for LIBs
V6O13 thin films were deposited on indium-doped tin oxide (ITO) conductive glass by a concise low-temperature liquid-phase deposition method and through heat treatment. The obtained films were directly used as electrodes without adding any other media. The results indicate that the film annealed at...
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Published in | Materials Vol. 15; no. 23; p. 8574 |
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Language | English |
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Abstract | V6O13 thin films were deposited on indium-doped tin oxide (ITO) conductive glass by a concise low-temperature liquid-phase deposition method and through heat treatment. The obtained films were directly used as electrodes without adding any other media. The results indicate that the film annealed at 400 °C exhibited an excellent cycling performance, which remained at 82.7% of capacity after 100 cycles. The film annealed at 400 °C with diffusion coefficients of 6.08 × 10−12 cm2·s−1 (Li+ insertion) and 5.46 × 10−12 cm2·s−1 (Li+ extraction) in the V6O13 film electrode. The high diffusion coefficients could be ascribed to the porous morphology composed of ultrathin nanosheets. Moreover, the film endured phase transitions during electrochemical cycling, the V6O13 partially transformed to Li0.6V1.67O3.67, Li3VO4, and VO2 with the insertion of Li+ into the lattice, and Li0.6V1.67O3.67, Li3VO4, and VO2 partially reversibly transformed backwards to V6O13 with the extraction of Li+ from the lattice. The phase transition can be attributed to the unique structure and morphology with enough active sites and ions diffusion channels during cycles. Such findings reveal a bright idea to prepare high-performance cathode materials for LIBs. |
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AbstractList | V6O13 thin films were deposited on indium-doped tin oxide (ITO) conductive glass by a concise low-temperature liquid-phase deposition method and through heat treatment. The obtained films were directly used as electrodes without adding any other media. The results indicate that the film annealed at 400 °C exhibited an excellent cycling performance, which remained at 82.7% of capacity after 100 cycles. The film annealed at 400 °C with diffusion coefficients of 6.08 × 10−12 cm2·s−1 (Li+ insertion) and 5.46 × 10−12 cm2·s−1 (Li+ extraction) in the V6O13 film electrode. The high diffusion coefficients could be ascribed to the porous morphology composed of ultrathin nanosheets. Moreover, the film endured phase transitions during electrochemical cycling, the V6O13 partially transformed to Li0.6V1.67O3.67, Li3VO4, and VO2 with the insertion of Li+ into the lattice, and Li0.6V1.67O3.67, Li3VO4, and VO2 partially reversibly transformed backwards to V6O13 with the extraction of Li+ from the lattice. The phase transition can be attributed to the unique structure and morphology with enough active sites and ions diffusion channels during cycles. Such findings reveal a bright idea to prepare high-performance cathode materials for LIBs. V 6 O 13 thin films were deposited on indium-doped tin oxide (ITO) conductive glass by a concise low-temperature liquid-phase deposition method and through heat treatment. The obtained films were directly used as electrodes without adding any other media. The results indicate that the film annealed at 400 °C exhibited an excellent cycling performance, which remained at 82.7% of capacity after 100 cycles. The film annealed at 400 °C with diffusion coefficients of 6.08 × 10 −12 cm 2 ·s −1 (Li + insertion) and 5.46 × 10 −12 cm 2 ·s −1 (Li + extraction) in the V 6 O 13 film electrode. The high diffusion coefficients could be ascribed to the porous morphology composed of ultrathin nanosheets. Moreover, the film endured phase transitions during electrochemical cycling, the V 6 O 13 partially transformed to Li 0.6 V 1.67 O 3.67 , Li 3 VO 4 , and VO 2 with the insertion of Li + into the lattice, and Li 0.6 V 1.67 O 3.67 , Li 3 VO 4 , and VO 2 partially reversibly transformed backwards to V 6 O 13 with the extraction of Li + from the lattice. The phase transition can be attributed to the unique structure and morphology with enough active sites and ions diffusion channels during cycles. Such findings reveal a bright idea to prepare high-performance cathode materials for LIBs. |
Author | Xu, Haiyan Li, Fei Li, Dongcai Liu, Fanglin Wang, Aiguo Sun, Daosheng |
AuthorAffiliation | 1 Anhui Key Laboratory of Advanced Building Materials, Anhui Jianzhu University, Hefei 230022, China 2 Key Laboratory of Functional Molecule Design and Interface Process, Anhui Jianzhu University, Hefei 230601, China |
AuthorAffiliation_xml | – name: 2 Key Laboratory of Functional Molecule Design and Interface Process, Anhui Jianzhu University, Hefei 230601, China – name: 1 Anhui Key Laboratory of Advanced Building Materials, Anhui Jianzhu University, Hefei 230022, China |
Author_xml | – sequence: 1 givenname: Fei surname: Li fullname: Li, Fei – sequence: 2 givenname: Haiyan orcidid: 0000-0002-9795-1181 surname: Xu fullname: Xu, Haiyan – sequence: 3 givenname: Fanglin surname: Liu fullname: Liu, Fanglin – sequence: 4 givenname: Dongcai surname: Li fullname: Li, Dongcai – sequence: 5 givenname: Aiguo surname: Wang fullname: Wang, Aiguo – sequence: 6 givenname: Daosheng surname: Sun fullname: Sun, Daosheng |
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Snippet | V6O13 thin films were deposited on indium-doped tin oxide (ITO) conductive glass by a concise low-temperature liquid-phase deposition method and through heat... V 6 O 13 thin films were deposited on indium-doped tin oxide (ITO) conductive glass by a concise low-temperature liquid-phase deposition method and through... |
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SubjectTerms | Annealing Cathodes Cycles Diffusion Electrochemical analysis Electrode materials Electrodes Electrolytes film electrodes Heat Heat treatment Indium tin oxides Insertion Liquid phase deposition Liquid phases Low temperature Morphology nanosheet Nanosheets phase transition Phase transitions Spectrum analysis Temperature Thin films V6O13 Vanadium oxides |
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Title | Synthesis and Electrochemical Performance of V6O13 Nanosheets Film Cathodes for LIBs |
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