Structural damage and phase stability of Al0.3CoCrFeNi high entropy alloy under high temperature ion irradiation

An initially single phase high entropy alloy (HEA) Al0.3CoCrFeNi was irradiated by 3 MeV Au ions to a fluence of 6 × 1015 cm−2 (∼31 dpa at damage peak) at four different temperatures ranging from 250 °C to 650 °C. Transmission electron microscopy (TEM) and Atom probe tomography (APT) were employed t...

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Published inActa materialia Vol. 188; pp. 1 - 15
Main Authors Yang, Tengfei, Guo, Wei, Poplawsky, Jonathan D., Li, Dongyue, Wang, Ling, Li, Yao, Hu, Wangyu, Crespillo, Miguel L., Yan, Zhanfeng, Zhang, Yong, Wang, Yugang, Zinkle, Steven J.
Format Journal Article
LanguageEnglish
Published United States Elsevier Ltd 15.04.2020
Elsevier
Subjects
High entropy alloy
Irradiation effect
MATERIALS SCIENCE
Phase stability
Structural damage
Phase stability
Irradiation effect
High entropy alloy
Structural damage
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Abstract An initially single phase high entropy alloy (HEA) Al0.3CoCrFeNi was irradiated by 3 MeV Au ions to a fluence of 6 × 1015 cm−2 (∼31 dpa at damage peak) at four different temperatures ranging from 250 °C to 650 °C. Transmission electron microscopy (TEM) and Atom probe tomography (APT) were employed to study the evolution of structural damage and phase stability with irradiation temperature. Al0.3CoCrFeNi exhibited a similar evolution of irradiation-induced defects with temperature as compared with conventional FCC alloys. At 250 °C and 350 °C, most of the visible irradiation-induced defects were faulted 1/3〈111〉 dislocation loops. As the irradiation temperature increased to 500 °C, perfect 1/2〈110〉 dislocation loops were observed along with the faulted loops. At the highest irradiation temperature 650 °C, only dislocation lines and networks could be observed. Regarding phase stability, the 3 MeV Au irradiation was observed to suppress the precipitation of (Ni, Al)-enriched nano clusters and the L12 ordered structure at irradiation temperatures 250 °C to 500 °C whereas precipitation of the B2 ordered structure was accelerated at 650 °C. This resulted in qualitatively opposite precipitation behavior between the ion irradiated damage region and unirradiated region at 500 °C and 650 °C. The opposite phase stability of the ion-irradiated damage region and unirradiated region at different temperatures is attributed to the competing effects of ballistic dissolution vs irradiation enhanced diffusion on precipitation. [Display omitted]
AbstractList In this study, an initially single phase high entropy alloy (HEA) Al0.3CoCrFeNi was irradiated by 3 MeV Au ions to a fluence of 6 × 1015 cm–2 (~31 dpa at damage peak) at four different temperatures ranging from 250 °C to 650 °C. Transmission electron microscopy (TEM) and Atom probe tomography (APT) were employed to study the evolution of structural damage and phase stability with irradiation temperature. Al0.3CoCrFeNi exhibited a similar evolution of irradiation-induced defects with temperature as compared with conventional FCC alloys. At 250 °C and 350 °C, most of the visible irradiation-induced defects were faulted 1/3$\langle{111}\rangle$ dislocation loops. As the irradiation temperature increased to 500 °C, perfect 1/2$\langle{110}\rangle$ dislocation loops were observed along with the faulted loops. At the highest irradiation temperature 650 °C, only dislocation lines and networks could be observed. Regarding phase stability, the 3 MeV Au irradiation was observed to suppress the precipitation of (Ni, Al)-enriched nano clusters and the L12 ordered structure at irradiation temperatures 250 °C to 500 °C whereas precipitation of the B2 ordered structure was accelerated at 650 °C. This resulted in qualitatively opposite precipitation behavior between the ion irradiated damage region and unirradiated region at 500 °C and 650 °C. The opposite phase stability of the ion-irradiated damage region and unirradiated region at different temperatures is attributed to the competing effects of ballistic dissolution vs irradiation enhanced diffusion on precipitation.
An initially single phase high entropy alloy (HEA) Al0.3CoCrFeNi was irradiated by 3 MeV Au ions to a fluence of 6 × 1015 cm−2 (∼31 dpa at damage peak) at four different temperatures ranging from 250 °C to 650 °C. Transmission electron microscopy (TEM) and Atom probe tomography (APT) were employed to study the evolution of structural damage and phase stability with irradiation temperature. Al0.3CoCrFeNi exhibited a similar evolution of irradiation-induced defects with temperature as compared with conventional FCC alloys. At 250 °C and 350 °C, most of the visible irradiation-induced defects were faulted 1/3〈111〉 dislocation loops. As the irradiation temperature increased to 500 °C, perfect 1/2〈110〉 dislocation loops were observed along with the faulted loops. At the highest irradiation temperature 650 °C, only dislocation lines and networks could be observed. Regarding phase stability, the 3 MeV Au irradiation was observed to suppress the precipitation of (Ni, Al)-enriched nano clusters and the L12 ordered structure at irradiation temperatures 250 °C to 500 °C whereas precipitation of the B2 ordered structure was accelerated at 650 °C. This resulted in qualitatively opposite precipitation behavior between the ion irradiated damage region and unirradiated region at 500 °C and 650 °C. The opposite phase stability of the ion-irradiated damage region and unirradiated region at different temperatures is attributed to the competing effects of ballistic dissolution vs irradiation enhanced diffusion on precipitation. [Display omitted]
Author Yang, Tengfei
Guo, Wei
Li, Yao
Poplawsky, Jonathan D.
Li, Dongyue
Hu, Wangyu
Crespillo, Miguel L.
Yan, Zhanfeng
Zinkle, Steven J.
Wang, Ling
Zhang, Yong
Wang, Yugang
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  organization: College of Materials Science and Engineering, Hunan University, Changsha 410082, China
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  surname: Crespillo
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  givenname: Zhanfeng
  surname: Yan
  fullname: Yan, Zhanfeng
  organization: State Key Laboratory of Nuclear Physics and Technology, Center for Applied Physics and Technology, Peking University, Beijing 100871, China
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  orcidid: 0000-0002-6355-9923
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  surname: Wang
  fullname: Wang, Yugang
  organization: State Key Laboratory of Nuclear Physics and Technology, Center for Applied Physics and Technology, Peking University, Beijing 100871, China
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  givenname: Steven J.
  orcidid: 0000-0003-2890-6915
  surname: Zinkle
  fullname: Zinkle, Steven J.
  email: szinkle@utk.edu
  organization: Department of Nuclear Engineering, University of Tennessee, Knoxville, TN 37996, United States
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Keywords Phase stability
Irradiation effect
High entropy alloy
Structural damage
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Snippet An initially single phase high entropy alloy (HEA) Al0.3CoCrFeNi was irradiated by 3 MeV Au ions to a fluence of 6 × 1015 cm−2 (∼31 dpa at damage peak) at four...
In this study, an initially single phase high entropy alloy (HEA) Al0.3CoCrFeNi was irradiated by 3 MeV Au ions to a fluence of 6 × 1015 cm–2 (~31 dpa at...
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SubjectTerms High entropy alloy
Irradiation effect
MATERIALS SCIENCE
Phase stability
Structural damage
Title Structural damage and phase stability of Al0.3CoCrFeNi high entropy alloy under high temperature ion irradiation
URI https://dx.doi.org/10.1016/j.actamat.2020.01.060
https://www.osti.gov/servlets/purl/1648949
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