Performance, methanol tolerance and stability of Fe-aminobenzimidazole derived catalyst for direct methanol fuel cells
Highly active and durable non-platinum group metals (non-PGM) catalyst based on iron-nitrogen-carbon (Fe-N-C) for the oxygen reduction reaction (ORR) derived from pyrolyzed Fe-aminobenzimidazole (Fe-ABZIM) was synthesized by sacrificial support method (SSM), and characterized by several physical-che...
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| Published in | Journal of power sources Vol. 319; pp. 235 - 246 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
01.07.2016
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| Abstract | Highly active and durable non-platinum group metals (non-PGM) catalyst based on iron-nitrogen-carbon (Fe-N-C) for the oxygen reduction reaction (ORR) derived from pyrolyzed Fe-aminobenzimidazole (Fe-ABZIM) was synthesized by sacrificial support method (SSM), and characterized by several physical-chemical techniques: scanning electron microscopy, transmission electron microscopy, Brunauer-Emmett-Teller method and X-ray photoelectron spectroscopy. In half-cell electrochemical configuration, the Fe-ABZIM catalyst presented a significant improvement of ORR activity with respect to a recently reported non-PGM formulation based on Fe-aminoantipyrine, with an enhancement of half-wave potential of about 85 mV in O2-saturated sulfuric acid solution. To the moment, the gap with respect to a benchmark Pt/C catalyst was about 90 mV. The Fe-ABZIM catalyst showed a remarkably high tolerance to methanol, resulting in superior ORR performance compared to Pt/C at methanol concentrations higher than 0.02 M. In direct methanol fuel cell (DMFC) good performances were also obtained. A durability test (100 h) at 90 °C, feeding 5 M methanol, was carried out. A certain decrease of performance was recorded, amounting to −0.20 mW cm−2 h−1 at the very beginning of test and −0.05 mW cm−2 h−1 at the end. However, the Fe-ABZIM is more adequate than previously reported formulations in terms of both ORR activity and stability.
•Non-PGM catalyst (Fe-N-C) was synthesized from iron and aminobenzimidazole.•High ORR activity and remarkable tolerance to the presence of methanol.•High performance of non-PGM catalyst in DMFC even at high methanol concentration.•Remarkable durability compared to state of the art best Fe-N-C catalysts. |
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| AbstractList | Highly active and durable non-platinum group metals (non-PGM) catalyst based on iron-nitrogen-carbon (Fe-N-C) for the oxygen reduction reaction (ORR) derived from pyrolyzed Fe-aminobenzimidazole (Fe-ABZIM) was synthesized by sacrificial support method (SSM), and characterized by several physical-chemical techniques: scanning electron microscopy, transmission electron microscopy, Brunauer-Emmett-Teller method and X-ray photoelectron spectroscopy. In half-cell electrochemical configuration, the Fe-ABZIM catalyst presented a significant improvement of ORR activity with respect to a recently reported non-PGM formulation based on Fe-aminoantipyrine, with an enhancement of half-wave potential of about 85 mV in O2-saturated sulfuric acid solution. To the moment, the gap with respect to a benchmark Pt/C catalyst was about 90 mV. The Fe-ABZIM catalyst showed a remarkably high tolerance to methanol, resulting in superior ORR performance compared to Pt/C at methanol concentrations higher than 0.02 M. In direct methanol fuel cell (DMFC) good performances were also obtained. A durability test (100 h) at 90 °C, feeding 5 M methanol, was carried out. A certain decrease of performance was recorded, amounting to −0.20 mW cm−2 h−1 at the very beginning of test and −0.05 mW cm−2 h−1 at the end. However, the Fe-ABZIM is more adequate than previously reported formulations in terms of both ORR activity and stability.
•Non-PGM catalyst (Fe-N-C) was synthesized from iron and aminobenzimidazole.•High ORR activity and remarkable tolerance to the presence of methanol.•High performance of non-PGM catalyst in DMFC even at high methanol concentration.•Remarkable durability compared to state of the art best Fe-N-C catalysts. Highly active and durable non-platinum group metals (non-PGM) catalyst based on iron-nitrogen-carbon (Fe-N-C) for the oxygen reduction reaction (ORR) derived from pyrolyzed Fe-aminobenzimidazole (Fe-ABZIM) was synthesized by sacrificial support method (SSM), and characterized by several physical-chemical techniques: scanning electron microscopy, transmission electron microscopy, Brunauer-Emmett-Teller method and X-ray photoelectron spectroscopy. In half-cell electrochemical configuration, the Fe-ABZIM catalyst presented a significant improvement of ORR activity with respect to a recently reported non-PGM formulation based on Fe-aminoantipyrine, with an enhancement of half-wave potential of about 85 mV in O sub(2)-saturated sulfuric acid solution. To the moment, the gap with respect to a benchmark Pt/C catalyst was about 90 mV. The Fe-ABZIM catalyst showed a remarkably high tolerance to methanol, resulting in superior ORR performance compared to Pt/C at methanol concentrations higher than 0.02 M. In direct methanol fuel cell (DMFC) good performances were also obtained. A durability test (100 h) at 90 degree C, feeding 5 M methanol, was carried out. A certain decrease of performance was recorded, amounting to -0.20 mW cm super(-2) h super(-1) at the very beginning of test and -0.05 mW cm super(-2) h super(-1) at the end. However, the Fe-ABZIM is more adequate than previously reported formulations in terms of both ORR activity and stability. |
| Author | Sebastián, David Artyushkova, Kateryna Aricò, Antonino S. Baglio, Vincenzo Serov, Alexey Atanassov, Plamen |
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| SubjectTerms | Catalysts DMFC Durability Electrocatalysts Fe-N-C Formulations Fuel cells Methanol tolerance Methyl alcohol Non-PGM ORR Platinum Stability Tolerances |
| Title | Performance, methanol tolerance and stability of Fe-aminobenzimidazole derived catalyst for direct methanol fuel cells |
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