The thermal stability of and nature of damage in Ti alloys subject to high-strain-rate deformation

Samples of Ti-6 wt% Al-4 wt% V and Timet 550 (Ti-4 wt% Al-4 wt% Mo-2 wt% Sn-0.5 wt% Si wt%), which have been deformed at a strain rate of 5 s −1 , were annealed after thinning so that the visibility of dislocations in transmission electron microscopy could be compared before and after annealing. It...

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Published inPhilosophical magazine (Abingdon, England) Vol. 84; no. 32; pp. 3411 - 3418
Main Authors Wu †, Xinhua, Zakaria, M., Loretto, M. H.
Format Journal Article
LanguageEnglish
Published Abingdon Taylor & Francis Group 11.11.2004
Taylor and Francis
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ISSN1478-6435
1478-6443
DOI10.1080/14786430412331284450

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Abstract Samples of Ti-6 wt% Al-4 wt% V and Timet 550 (Ti-4 wt% Al-4 wt% Mo-2 wt% Sn-0.5 wt% Si wt%), which have been deformed at a strain rate of 5 s −1 , were annealed after thinning so that the visibility of dislocations in transmission electron microscopy could be compared before and after annealing. It has been found that imaging with g = 0002 produces clear images of dislocations before and after annealing, but that imaging with other diffracting vectors gives reasonable dislocation images only after annealing to at least 700°C. The sharpness of Kikuchi lines in diffraction patterns obtained from fully annealed samples, deformed at 10 −1 and 5 s −1 , has been examined. The lines are sharp for all planes in the fully annealed samples, but become more diffuse in samples deformed at 10 −1  s −1 . However, in samples deformed at 5 s −1 the Kikuchi lines from (0002) planes are sharp but the lines from all other planes are diffuse. These observations are interpreted in terms of the presence of a high density of defects, which do not distort the elastically strong (0002) planes as significantly as they distort all other planes. These observations are discussed with respect to the recent claim that a particular Ti alloy deforms by a mechanism that does not involve dislocations.
AbstractList Samples of Ti-6 wt% Al-4 wt% V and Timet 550 (Ti-4 wt% Al-4 wt% Mo-2 Wt% Sn-0.5 Wt% Siwt%), which have been deformed at a strain rate of 5 s-1, were annealed after thinning so that the visibility of dislocations in transmission electron microscopy could be compared before and after annealing. It has been found that imaging with g = 0002 produces clear images of dislocations before and after annealing, but that imaging with other diffracting vectors gives reason-able dislocation images only after annealing to at least 700 deg C. The sharpness of Kikuchi lines in diffraction patterns obtained from fully annealed samples, deformed at 10(-1) and 5 s-1, has been examined. The lines are sharp for all planes in the fully annealed samples, but become more diffuse in samples deformed at 10(-1) s-1. However, in samples deformed at 5 s-1 the Kikuchi lines from (0002) planes are sharp but the lines from all other planes are diffuse. These observations are interpreted in terms of the presence of a high density of defects, which do not distort the elastically strong (0002) planes as significantly as they distort all other planes. These observations are discussed with respect to the recent claim that a particular Ti alloy deforms by a mechanism that does not involve dislocations.
Samples of Ti-6 wt% Al-4 wt% V and Timet 550 (Ti-4 wt% Al-4 wt% Mo-2 Wt% Sn-0.5 Wt% Siwt%), which have been deformed at a strain rate of 5/s, were annealed after thinning so that the visibility of dislocations in transmission electron microscopy could be compared before and after annealing. It has been found that imaging with g = 0002 produces clear images of dislocations before and after annealing, but that imaging with other diffracting vectors gives reason-able dislocation images only after annealing to at least 700DGC. The sharpness of Kikuchi lines in diffraction patterns obtained from fully annealed samples, deformed at 10 exp -1 and 5/s, has been examined. The lines are sharp for all planes in the fully annealed samples, but become more diffuse in samples deformed at 10 exp -1/s. However, in samples deformed at 5/s the Kikuchi lines from (0002) planes are sharp but the lines from all other planes are diffuse. These observations are interpreted in terms of the presence of a high density of defects, which do not distort the elastically strong (0002) planes as significantly as they distort all other planes. These observations are discussed with respect to the recent claim that a particular Ti alloy deforms by a mechanism that does not involve dislocations.
Samples of Ti-6 wt% Al-4 wt% V and Timet 550 (Ti-4 wt% Al-4 wt% Mo-2 wt% Sn-0.5 wt% Si wt%), which have been deformed at a strain rate of 5 s −1 , were annealed after thinning so that the visibility of dislocations in transmission electron microscopy could be compared before and after annealing. It has been found that imaging with g = 0002 produces clear images of dislocations before and after annealing, but that imaging with other diffracting vectors gives reasonable dislocation images only after annealing to at least 700°C. The sharpness of Kikuchi lines in diffraction patterns obtained from fully annealed samples, deformed at 10 −1 and 5 s −1 , has been examined. The lines are sharp for all planes in the fully annealed samples, but become more diffuse in samples deformed at 10 −1  s −1 . However, in samples deformed at 5 s −1 the Kikuchi lines from (0002) planes are sharp but the lines from all other planes are diffuse. These observations are interpreted in terms of the presence of a high density of defects, which do not distort the elastically strong (0002) planes as significantly as they distort all other planes. These observations are discussed with respect to the recent claim that a particular Ti alloy deforms by a mechanism that does not involve dislocations.
Author Wu †, Xinhua
Loretto, M. H.
Zakaria, M.
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Cites_doi 10.1007/BF02651653
10.1080/1478643031000124420
10.1126/science.1081957
10.1016/S1359-6454(97)00287-5
10.1016/0001-6160(58)90048-8
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Issue 32
Keywords Annealing
Inorganic compounds
Deformation
Vanadium alloys
Ternary alloys
Experimental study
Thermal stability
Multi-element alloys
Dislocations
Tin alloys
Titanium alloys
Transmission electron microscopy
Aluminium alloys
Damage
Molybdenum alloys
Transition element alloys
Kikuchi lines
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Snippet Samples of Ti-6 wt% Al-4 wt% V and Timet 550 (Ti-4 wt% Al-4 wt% Mo-2 wt% Sn-0.5 wt% Si wt%), which have been deformed at a strain rate of 5 s −1 , were...
Samples of Ti-6 wt% Al-4 wt% V and Timet 550 (Ti-4 wt% Al-4 wt% Mo-2 Wt% Sn-0.5 Wt% Siwt%), which have been deformed at a strain rate of 5/s, were annealed...
Samples of Ti-6 wt% Al-4 wt% V and Timet 550 (Ti-4 wt% Al-4 wt% Mo-2 Wt% Sn-0.5 Wt% Siwt%), which have been deformed at a strain rate of 5 s-1, were annealed...
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SubjectTerms Condensed matter: structure, mechanical and thermal properties
Defects and impurities in crystals; microstructure
Deformation and plasticity (including yield, ductility, and superplasticity)
Exact sciences and technology
Linear defects: dislocations, disclinations
Mechanical and acoustical properties of condensed matter
Mechanical properties of solids
Physics
Structure of solids and liquids; crystallography
Title The thermal stability of and nature of damage in Ti alloys subject to high-strain-rate deformation
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