Effects of processing conditions on the properties of paraffin/melamine-urea-formaldehyde microcapsules prepared by in situ polymerization
[Display omitted] Microcapsules containing phase change material (PCM) paraffin as the internal phase and melamine-urea-formaldehyde (MUF) as the external shell were synthesized by in situ polymerization in the study. The effects of processing conditions (including core-to-shell ratio, concentration...
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| Published in | Colloids and surfaces. A, Physicochemical and engineering aspects Vol. 585; p. 124046 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
20.01.2020
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| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
Microcapsules containing phase change material (PCM) paraffin as the internal phase and melamine-urea-formaldehyde (MUF) as the external shell were synthesized by in situ polymerization in the study. The effects of processing conditions (including core-to-shell ratio, concentration of styrene/maleic anhydride (SMA), reaction temperature, reaction time, and final reaction pH) on the properties of synthesized microcapsules (microencapsulation process, morphology, mean diameter, and phase change properties) were investigated. The chemical structures, morphologies, and phase change properties of paraffin/MUF microcapsules were characterized by Fourier transform infrared spectroscopy (FTIR), field emission scanning electron microscopy (FE-SEM), differential scanning calorimetry (DSC), and thermogravimetric analyzer (TGA). Under optimal processing conditions (core-to-shell ratio of 1.5, 20 mg/mL SMA, 2-h reaction at 80 °C, and final reaction pH 5.5), the encapsulation efficiency of synthesized paraffin/MUF microcapsules reached 77.1% and the phase change latent heat values of melting and crystallization were about 134.3 J/g and 133.1 J/g, respectively. |
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| AbstractList | [Display omitted]
Microcapsules containing phase change material (PCM) paraffin as the internal phase and melamine-urea-formaldehyde (MUF) as the external shell were synthesized by in situ polymerization in the study. The effects of processing conditions (including core-to-shell ratio, concentration of styrene/maleic anhydride (SMA), reaction temperature, reaction time, and final reaction pH) on the properties of synthesized microcapsules (microencapsulation process, morphology, mean diameter, and phase change properties) were investigated. The chemical structures, morphologies, and phase change properties of paraffin/MUF microcapsules were characterized by Fourier transform infrared spectroscopy (FTIR), field emission scanning electron microscopy (FE-SEM), differential scanning calorimetry (DSC), and thermogravimetric analyzer (TGA). Under optimal processing conditions (core-to-shell ratio of 1.5, 20 mg/mL SMA, 2-h reaction at 80 °C, and final reaction pH 5.5), the encapsulation efficiency of synthesized paraffin/MUF microcapsules reached 77.1% and the phase change latent heat values of melting and crystallization were about 134.3 J/g and 133.1 J/g, respectively. Microcapsules containing phase change material (PCM) paraffin as the internal phase and melamine-urea-formaldehyde (MUF) as the external shell were synthesized by in situ polymerization in the study. The effects of processing conditions (including core-to-shell ratio, concentration of styrene/maleic anhydride (SMA), reaction temperature, reaction time, and final reaction pH) on the properties of synthesized microcapsules (microencapsulation process, morphology, mean diameter, and phase change properties) were investigated. The chemical structures, morphologies, and phase change properties of paraffin/MUF microcapsules were characterized by Fourier transform infrared spectroscopy (FTIR), field emission scanning electron microscopy (FE-SEM), differential scanning calorimetry (DSC), and thermogravimetric analyzer (TGA). Under optimal processing conditions (core-to-shell ratio of 1.5, 20 mg/mL SMA, 2-h reaction at 80 °C, and final reaction pH 5.5), the encapsulation efficiency of synthesized paraffin/MUF microcapsules reached 77.1% and the phase change latent heat values of melting and crystallization were about 134.3 J/g and 133.1 J/g, respectively. |
| ArticleNumber | 124046 |
| Author | Wang, Siqun Lyu, Shaoyi Han, Shenjie Chen, Zhilin Chen, Yanping Fu, Feng |
| Author_xml | – sequence: 1 givenname: Shenjie surname: Han fullname: Han, Shenjie organization: Research Institute of Wood Industry, Chinese Academy of Forestry, Beijing, 100091, China – sequence: 2 givenname: Yanping surname: Chen fullname: Chen, Yanping organization: Research Institute of Wood Industry, Chinese Academy of Forestry, Beijing, 100091, China – sequence: 3 givenname: Shaoyi surname: Lyu fullname: Lyu, Shaoyi organization: Research Institute of Wood Industry, Chinese Academy of Forestry, Beijing, 100091, China – sequence: 4 givenname: Zhilin surname: Chen fullname: Chen, Zhilin organization: Research Institute of Wood Industry, Chinese Academy of Forestry, Beijing, 100091, China – sequence: 5 givenname: Siqun surname: Wang fullname: Wang, Siqun email: swang@utk.edu organization: Research Institute of Wood Industry, Chinese Academy of Forestry, Beijing, 100091, China – sequence: 6 givenname: Feng surname: Fu fullname: Fu, Feng email: feng@caf.ac.cn organization: Research Institute of Wood Industry, Chinese Academy of Forestry, Beijing, 100091, China |
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Microcapsules containing phase change material (PCM) paraffin as the internal phase and melamine-urea-formaldehyde (MUF) as the external... Microcapsules containing phase change material (PCM) paraffin as the internal phase and melamine-urea-formaldehyde (MUF) as the external shell were synthesized... |
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| SubjectTerms | chemical structure crystallization differential scanning calorimetry Fourier transform infrared spectroscopy latent heat maleic anhydrides Melamine-Urea-Formaldehyde melting Microcapsule microencapsulation Phase change material polymerization Processing conditions scanning electron microscopy styrene temperature thermogravimetry |
| Title | Effects of processing conditions on the properties of paraffin/melamine-urea-formaldehyde microcapsules prepared by in situ polymerization |
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