Facile and Green Synthesis of Graphene-Based Conductive Adhesives via Liquid Exfoliation Process
In this study, we report a facile and green process to synthesize high-quality and few-layer graphene (FLG) derived from graphite via a liquid exfoliation process. The corresponding characterizations of FLG, such as scanning electron microscopy (SEM), transmission electron microscope (TEM), atomic f...
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| Published in | Nanomaterials (Basel, Switzerland) Vol. 9; no. 1; p. 38 |
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| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
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28.12.2018
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| Abstract | In this study, we report a facile and green process to synthesize high-quality and few-layer graphene (FLG) derived from graphite via a liquid exfoliation process. The corresponding characterizations of FLG, such as scanning electron microscopy (SEM), transmission electron microscope (TEM), atomic force microscopy (AFM) and Raman spectroscopy, were carried out. The results of SEM show that the lateral size of as-synthesized FLG is 1–5 μm. The results of TEM and AFM indicate more than 80% of graphene layers is <10 layers. The most surprising thing is that D/G ratio of graphite and FLG are 0.15 and 0.19, respectively. The result of the similar D/G ratio demonstrates that little structural defects were created via the liquid exfoliation process. Electronic conductivity tests and resistance of composite film, in terms of different contents of graphite/polyvinylidene difluoride (PVDF) and FLG/PVDF, were carried out. Dramatically, the FLG/PVDF composite demonstrates superior performance compared to the graphite/PVDF composite at the same ratio. In addition, the post-sintering process plays an important role in improving electronic conductivity by 85%. The composition-optimized FLG/PVDF thin film exhibits 81.9 S·cm−1. These results indicate that the developed FLG/PVDF composite adhesives could be a potential candidate for conductive adhesive applications. |
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| AbstractList | In this study, we report a facile and green process to synthesize high-quality and few-layer graphene (FLG) derived from graphite via a liquid exfoliation process. The corresponding characterizations of FLG, such as scanning electron microscopy (SEM), transmission electron microscope (TEM), atomic force microscopy (AFM) and Raman spectroscopy, were carried out. The results of SEM show that the lateral size of as-synthesized FLG is 1-5 μm. The results of TEM and AFM indicate more than 80% of graphene layers is <10 layers. The most surprising thing is that D/G ratio of graphite and FLG are 0.15 and 0.19, respectively. The result of the similar D/G ratio demonstrates that little structural defects were created via the liquid exfoliation process. Electronic conductivity tests and resistance of composite film, in terms of different contents of graphite/polyvinylidene difluoride (PVDF) and FLG/PVDF, were carried out. Dramatically, the FLG/PVDF composite demonstrates superior performance compared to the graphite/PVDF composite at the same ratio. In addition, the post-sintering process plays an important role in improving electronic conductivity by 85%. The composition-optimized FLG/PVDF thin film exhibits 81.9 S·cm−1. These results indicate that the developed FLG/PVDF composite adhesives could be a potential candidate for conductive adhesive applications. In this study, we report a facile and green process to synthesize high-quality and few-layer graphene (FLG) derived from graphite via a liquid exfoliation process. The corresponding characterizations of FLG, such as scanning electron microscopy (SEM), transmission electron microscope (TEM), atomic force microscopy (AFM) and Raman spectroscopy, were carried out. The results of SEM show that the lateral size of as-synthesized FLG is 1⁻5 μm. The results of TEM and AFM indicate more than 80% of graphene layers is <10 layers. The most surprising thing is that D/G ratio of graphite and FLG are 0.15 and 0.19, respectively. The result of the similar D/G ratio demonstrates that little structural defects were created via the liquid exfoliation process. Electronic conductivity tests and resistance of composite film, in terms of different contents of graphite/polyvinylidene difluoride (PVDF) and FLG/PVDF, were carried out. Dramatically, the FLG/PVDF composite demonstrates superior performance compared to the graphite/PVDF composite at the same ratio. In addition, the post-sintering process plays an important role in improving electronic conductivity by 85%. The composition-optimized FLG/PVDF thin film exhibits 81.9 S·cm-1. These results indicate that the developed FLG/PVDF composite adhesives could be a potential candidate for conductive adhesive applications.In this study, we report a facile and green process to synthesize high-quality and few-layer graphene (FLG) derived from graphite via a liquid exfoliation process. The corresponding characterizations of FLG, such as scanning electron microscopy (SEM), transmission electron microscope (TEM), atomic force microscopy (AFM) and Raman spectroscopy, were carried out. The results of SEM show that the lateral size of as-synthesized FLG is 1⁻5 μm. The results of TEM and AFM indicate more than 80% of graphene layers is <10 layers. The most surprising thing is that D/G ratio of graphite and FLG are 0.15 and 0.19, respectively. The result of the similar D/G ratio demonstrates that little structural defects were created via the liquid exfoliation process. Electronic conductivity tests and resistance of composite film, in terms of different contents of graphite/polyvinylidene difluoride (PVDF) and FLG/PVDF, were carried out. Dramatically, the FLG/PVDF composite demonstrates superior performance compared to the graphite/PVDF composite at the same ratio. In addition, the post-sintering process plays an important role in improving electronic conductivity by 85%. The composition-optimized FLG/PVDF thin film exhibits 81.9 S·cm-1. These results indicate that the developed FLG/PVDF composite adhesives could be a potential candidate for conductive adhesive applications. In this study, we report a facile and green process to synthesize high-quality and few-layer graphene (FLG) derived from graphite via a liquid exfoliation process. The corresponding characterizations of FLG, such as scanning electron microscopy (SEM), transmission electron microscope (TEM), atomic force microscopy (AFM) and Raman spectroscopy, were carried out. The results of SEM show that the lateral size of as-synthesized FLG is 1–5 μm. The results of TEM and AFM indicate more than 80% of graphene layers is <10 layers. The most surprising thing is that D/G ratio of graphite and FLG are 0.15 and 0.19, respectively. The result of the similar D/G ratio demonstrates that little structural defects were created via the liquid exfoliation process. Electronic conductivity tests and resistance of composite film, in terms of different contents of graphite/polyvinylidene difluoride (PVDF) and FLG/PVDF, were carried out. Dramatically, the FLG/PVDF composite demonstrates superior performance compared to the graphite/PVDF composite at the same ratio. In addition, the post-sintering process plays an important role in improving electronic conductivity by 85%. The composition-optimized FLG/PVDF thin film exhibits 81.9 S·cm −1 . These results indicate that the developed FLG/PVDF composite adhesives could be a potential candidate for conductive adhesive applications. In this study, we report a facile and green process to synthesize high-quality and few-layer graphene (FLG) derived from graphite via a liquid exfoliation process. The corresponding characterizations of FLG, such as scanning electron microscopy (SEM), transmission electron microscope (TEM), atomic force microscopy (AFM) and Raman spectroscopy, were carried out. The results of SEM show that the lateral size of as-synthesized FLG is 1⁻5 μm. The results of TEM and AFM indicate more than 80% of graphene layers is <10 layers. The most surprising thing is that D/G ratio of graphite and FLG are 0.15 and 0.19, respectively. The result of the similar D/G ratio demonstrates that little structural defects were created via the liquid exfoliation process. Electronic conductivity tests and resistance of composite film, in terms of different contents of graphite/polyvinylidene difluoride (PVDF) and FLG/PVDF, were carried out. Dramatically, the FLG/PVDF composite demonstrates superior performance compared to the graphite/PVDF composite at the same ratio. In addition, the post-sintering process plays an important role in improving electronic conductivity by 85%. The composition-optimized FLG/PVDF thin film exhibits 81.9 S·cm . These results indicate that the developed FLG/PVDF composite adhesives could be a potential candidate for conductive adhesive applications. |
| Author | Lai, Yi-Chin Liu, Wei-Ren Chang, Chien-Liang Hung, Wu-Ching Huang, Chia-Hung Liao, Ying-Chih Wu, Jhao-Yi Wu, Hsiao-Min |
| AuthorAffiliation | 2 Department of Chemical Engineering, National Taiwan University, No. 1, Sec. 4, Roosevelt Rd., Taipei 10617, Taiwan; yijin10221339@gmail.com 1 Department of Chemical Engineering, Chung Yuan Christian University, R&D Center for Membrane Technology, 32023, No. 200, Chun Pei Rd., Chung Li District, Taoyuan 32023, Taiwan; james19931201@gmail.com 3 National Chung Shan Institute of Science & Technology, Neighborhood, Sec. Jia’an, Zhongzheng Rd., Longtan Dist., Taoyuan 32546, Taiwan; rodin2005@yahoo.com.tw (C.-L.C.); 5000blackblue@gmail.com (W.-C.H.); prettysandy119@gmail.com (H.-M.W.) 4 Metal Industries Research and Development Centre, Kaohsiung 81160, Taiwan; chiahung@mail.mirdc.org.tw |
| AuthorAffiliation_xml | – name: 3 National Chung Shan Institute of Science & Technology, Neighborhood, Sec. Jia’an, Zhongzheng Rd., Longtan Dist., Taoyuan 32546, Taiwan; rodin2005@yahoo.com.tw (C.-L.C.); 5000blackblue@gmail.com (W.-C.H.); prettysandy119@gmail.com (H.-M.W.) – name: 1 Department of Chemical Engineering, Chung Yuan Christian University, R&D Center for Membrane Technology, 32023, No. 200, Chun Pei Rd., Chung Li District, Taoyuan 32023, Taiwan; james19931201@gmail.com – name: 2 Department of Chemical Engineering, National Taiwan University, No. 1, Sec. 4, Roosevelt Rd., Taipei 10617, Taiwan; yijin10221339@gmail.com – name: 4 Metal Industries Research and Development Centre, Kaohsiung 81160, Taiwan; chiahung@mail.mirdc.org.tw |
| Author_xml | – sequence: 1 givenname: Jhao-Yi surname: Wu fullname: Wu, Jhao-Yi – sequence: 2 givenname: Yi-Chin surname: Lai fullname: Lai, Yi-Chin – sequence: 3 givenname: Chien-Liang surname: Chang fullname: Chang, Chien-Liang – sequence: 4 givenname: Wu-Ching surname: Hung fullname: Hung, Wu-Ching – sequence: 5 givenname: Hsiao-Min surname: Wu fullname: Wu, Hsiao-Min – sequence: 6 givenname: Ying-Chih orcidid: 0000-0001-9496-4190 surname: Liao fullname: Liao, Ying-Chih – sequence: 7 givenname: Chia-Hung surname: Huang fullname: Huang, Chia-Hung – sequence: 8 givenname: Wei-Ren surname: Liu fullname: Liu, Wei-Ren |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/30597905$$D View this record in MEDLINE/PubMed |
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| CitedBy_id | crossref_primary_10_3390_ma12172793 crossref_primary_10_3390_antiox13050522 crossref_primary_10_3390_cryst10100902 crossref_primary_10_3390_nano10050926 crossref_primary_10_1007_s10854_020_03513_5 crossref_primary_10_1155_2020_7915641 |
| Cites_doi | 10.1039/B512799H 10.1021/ja807449u 10.1088/1361-6528/aa66a2 10.3390/nano6110206 10.1126/science.1157996 10.1007/978-3-319-13875-6_2 10.1002/adma.201300155 10.1016/j.microrel.2011.11.002 10.1021/cm100998e 10.1002/polb.21070 10.1038/nnano.2010.232 10.1063/1.2949074 10.1038/nnano.2008.215 10.1126/science.1110168 10.1002/macp.201200029 10.1038/nnano.2010.192 10.3390/ma11030345 10.1166/jnn.2015.9201 10.1002/anie.201201084 10.1126/science.1102896 10.1016/j.carbon.2007.02.034 10.1038/nnano.2008.199 10.1021/nl0731872 10.1016/j.ijadhadh.2004.11.008 10.1016/j.ijadhadh.2005.10.001 10.1039/c2jm00044j 10.1088/1361-6463/aac562 10.1002/polb.21695 10.1016/j.compscitech.2014.05.018 10.1016/j.compositesb.2017.10.020 10.1021/nl801827v 10.1039/C5RA08643D 10.3144/expresspolymlett.2012.68 10.1016/j.carbon.2013.07.055 10.1016/j.ijadhadh.2006.03.006 10.1016/S0026-2714(00)00033-0 10.1002/pc.10452 10.1109/6104.816098 10.1016/j.compscitech.2011.05.010 10.1016/j.polymer.2008.08.057 10.1038/nature04969 10.1103/PhysRevB.78.245403 10.1163/156856108X305471 10.1021/am200628c 10.1016/S1369-7021(06)71446-8 10.1021/nl803279t |
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| Keywords | flexiable conductive adhesives graphene liquid exfoliation polyvinylidene fluoride |
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| SubjectTerms | conductive adhesives flexiable graphene liquid exfoliation polyvinylidene fluoride |
| Title | Facile and Green Synthesis of Graphene-Based Conductive Adhesives via Liquid Exfoliation Process |
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