TFE Terpolymers: Once Promising – Are There Still Perspectives in the 21st Century: Synthesis, Characterization, and Properties‐Part I

Polytetrafluoroethylene (PTFE) exhibits outstanding properties such as high‐temperature stability, low surface tension, and chemical resistance against most solvents, strong acids, and bases. However, these traits make it challenging to subject PTFE to standard polymer processing procedures, such as...

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Published inMacromolecular rapid communications. Vol. 45; no. 18; pp. e2400294 - n/a
Main Authors Ok, Salim, Steinhart, Martin, Scheler, Ulrich, Améduri, Bruno
Format Journal Article
LanguageEnglish
Published Germany Wiley Subscription Services, Inc 01.09.2024
Wiley-VCH Verlag
Subjects
Acid resistance
characterization
Chemical Sciences
Copolymerization
Fluoropolymers
Melting point
Melting points
Microstructural analysis
Microstructure
Polymers
Polytetrafluoroethylene
Propylene
Surface stability
Surface tension
Synthesis
Terpolymers
Tetrafluoroethylene
TFE‐based terpolymers
Thermoforming
synthesis
characterization
TFE‐based terpolymers
TFE-based terpolymers
Online AccessGet full text
ISSN1022-1336
1521-3927
1521-3927
DOI10.1002/marc.202400294

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Abstract Polytetrafluoroethylene (PTFE) exhibits outstanding properties such as high‐temperature stability, low surface tension, and chemical resistance against most solvents, strong acids, and bases. However, these traits make it challenging to subject PTFE to standard polymer processing procedures, such as thermoforming and hot incremental forming. While polymer processing at temperatures above the melting point of PTFE is already demanding, the typically large molar mass of PTFE results in extremely high melt viscosities, complicating the processing of PTFE. Also, PTFE tends to decompose at temperatures close to its melting point. Therefore, fluoropolymers obtained by copolymerizing tetrafluoroethylene (TFE) with various co‐monomers are studied as alternatives to PTFE (e.g., fluorinated ethylene‐propylene (FEP)), combining its advantages with better processability. TFE terpolymers have emerged as desirable PTFE alternatives. This review provides an overview of the synthesis with various comonomers and microstructural analysis of PTFE terpolymers and the relationships between the microstructures of TFE terpolymers and their properties. PTFE decomposes at temperatures close to its melting point. Therefore, TFE terpolymers have emerged as desirable PTFE alternatives, where these TFE terpolymers combine PTFE's advantages with better processability. Currently, fluoropolymers have reached a new era. The present review summarizes the synthesis, detailed characterization, and structure‐property correlations of the fluoropolymers and ends with a future perspective on the use of fluoropolymers.
AbstractList Polytetrafluoroethylene (PTFE) exhibits outstanding properties such as high‐temperature stability, low surface tension, and chemical resistance against most solvents, strong acids, and bases. However, these traits make it challenging to subject PTFE to standard polymer processing procedures, such as thermoforming and hot incremental forming. While polymer processing at temperatures above the melting point of PTFE is already demanding, the typically large molar mass of PTFE results in extremely high melt viscosities, complicating the processing of PTFE. Also, PTFE tends to decompose at temperatures close to its melting point. Therefore, fluoropolymers obtained by copolymerizing tetrafluoroethylene (TFE) with various co‐monomers are studied as alternatives to PTFE (e.g., fluorinated ethylene‐propylene (FEP)), combining its advantages with better processability. TFE terpolymers have emerged as desirable PTFE alternatives. This review provides an overview of the synthesis with various comonomers and microstructural analysis of PTFE terpolymers and the relationships between the microstructures of TFE terpolymers and their properties. PTFE decomposes at temperatures close to its melting point. Therefore, TFE terpolymers have emerged as desirable PTFE alternatives, where these TFE terpolymers combine PTFE's advantages with better processability. Currently, fluoropolymers have reached a new era. The present review summarizes the synthesis, detailed characterization, and structure‐property correlations of the fluoropolymers and ends with a future perspective on the use of fluoropolymers.
Polytetrafluoroethylene (PTFE) exhibits outstanding properties such as high‐temperature stability, low surface tension, and chemical resistance against most solvents, strong acids, and bases. However, these traits make it challenging to subject PTFE to standard polymer processing procedures, such as thermoforming and hot incremental forming. While polymer processing at temperatures above the melting point of PTFE is already demanding, the typically large molar mass of PTFE results in extremely high melt viscosities, complicating the processing of PTFE. Also, PTFE tends to decompose at temperatures close to its melting point. Therefore, fluoropolymers obtained by copolymerizing tetrafluoroethylene (TFE) with various co‐monomers are studied as alternatives to PTFE (e.g., fluorinated ethylene‐propylene (FEP)), combining its advantages with better processability. TFE terpolymers have emerged as desirable PTFE alternatives. This review provides an overview of the synthesis with various comonomers and microstructural analysis of PTFE terpolymers and the relationships between the microstructures of TFE terpolymers and their properties.
Polytetrafluoroethylene (PTFE) exhibits outstanding properties such as high-temperature stability, low surface tension, and chemical resistance against most solvents, strong acids, and bases. However, these traits make it challenging to subject PTFE to standard polymer processing procedures, such as thermoforming and hot incremental forming. While polymer processing at temperatures above the melting point of PTFE is already demanding, the typically large molar mass of PTFE results in extremely high melt viscosities, complicating the processing of PTFE. Also, PTFE tends to decompose at temperatures close to its melting point. Therefore, fluoropolymers obtained by copolymerizing tetrafluoroethylene (TFE) with various co-monomers are studied as alternatives to PTFE (e.g., fluorinated ethylene-propylene (FEP)), combining its advantages with better processability. TFE terpolymers have emerged as desirable PTFE alternatives. This review provides an overview of the synthesis with various comonomers and microstructural analysis of PTFE terpolymers and the relationships between the microstructures of TFE terpolymers and their properties.Polytetrafluoroethylene (PTFE) exhibits outstanding properties such as high-temperature stability, low surface tension, and chemical resistance against most solvents, strong acids, and bases. However, these traits make it challenging to subject PTFE to standard polymer processing procedures, such as thermoforming and hot incremental forming. While polymer processing at temperatures above the melting point of PTFE is already demanding, the typically large molar mass of PTFE results in extremely high melt viscosities, complicating the processing of PTFE. Also, PTFE tends to decompose at temperatures close to its melting point. Therefore, fluoropolymers obtained by copolymerizing tetrafluoroethylene (TFE) with various co-monomers are studied as alternatives to PTFE (e.g., fluorinated ethylene-propylene (FEP)), combining its advantages with better processability. TFE terpolymers have emerged as desirable PTFE alternatives. This review provides an overview of the synthesis with various comonomers and microstructural analysis of PTFE terpolymers and the relationships between the microstructures of TFE terpolymers and their properties.
Author Ok, Salim
Steinhart, Martin
Améduri, Bruno
Scheler, Ulrich
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  organization: Univ. Montpellier, CNRS, ENSCM
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Keywords synthesis
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TFE‐based terpolymers
TFE-based terpolymers
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Snippet Polytetrafluoroethylene (PTFE) exhibits outstanding properties such as high‐temperature stability, low surface tension, and chemical resistance against most...
Polytetrafluoroethylene (PTFE) exhibits outstanding properties such as high-temperature stability, low surface tension, and chemical resistance against most...
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SubjectTerms Acid resistance
characterization
Chemical Sciences
Copolymerization
Fluoropolymers
Melting point
Melting points
Microstructural analysis
Microstructure
Polymers
Polytetrafluoroethylene
Propylene
Surface stability
Surface tension
Synthesis
Terpolymers
Tetrafluoroethylene
TFE‐based terpolymers
Thermoforming
Title TFE Terpolymers: Once Promising – Are There Still Perspectives in the 21st Century: Synthesis, Characterization, and Properties‐Part I
URI https://onlinelibrary.wiley.com/doi/abs/10.1002%2Fmarc.202400294
https://www.ncbi.nlm.nih.gov/pubmed/39108073
https://www.proquest.com/docview/3115379047
https://www.proquest.com/docview/3089879814
https://hal.science/hal-04671308
Volume 45
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