Control of Metal-Ion Composition in the Synthesis of Ternary II-II′-VI Nanoparticles by Using a Mixed-Metal Cluster Precursor Approach
The ternary molecular nanoclusters [ZnxCd10−xSe4(SePh)12(PnPr3)4] (x=1.8, 1 a; x=2.6, 1 b) were employed as single‐source precursors for the synthesis of high‐quality hexagonal ZnxCd1−xSe nanocrystals. The tellurium clusters [ZnxCd10−xTe4(TePh)12(PnPr3)4] (x=1.8, 2 a; x=2.6, 2 b) are equally conveni...
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| Published in | Chemistry : a European journal Vol. 12; no. 5; pp. 1547 - 1554 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
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Weinheim
WILEY-VCH Verlag
01.02.2006
WILEY‐VCH Verlag |
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| Abstract | The ternary molecular nanoclusters [ZnxCd10−xSe4(SePh)12(PnPr3)4] (x=1.8, 1 a; x=2.6, 1 b) were employed as single‐source precursors for the synthesis of high‐quality hexagonal ZnxCd1−xSe nanocrystals. The tellurium clusters [ZnxCd10−xTe4(TePh)12(PnPr3)4] (x=1.8, 2 a; x=2.6, 2 b) are equally convenient precursors for the synthesis cubic ZnxCd1−xE nanoparticles. The thermolysis of the cluster molecules in hexadecylamine provides an efficient system in which the inherent metal‐ion stoichiometry of the clusters is retained in the nanocrystalline products, whilst also affording control of particle size within the 2–5 nm range. In all cases, the nanoparticles are monodisperse, and luminescence spectra exhibit emission energies close to the absorption edge. Analysis of the optical spectra and X‐ray diffraction patterns of these materials indicates a metal‐ion concentration gradient within the structures of the nanocrystals, with ZnII ions predominantly located near the surface of the particles.
Zinc into it! Ternary Zn‐Cd‐Se and Zn‐Cd‐Te molecular nanoclusters have been employed as single‐source precursors for the synthesis of high‐quality ZnxCd1−xSe and ZnxCd1−xTe (illustrated) nanocrystals, respectively. The thermolysis of the molecular precursors in hexadecylamine solvent provides a route in which the inherent metal‐ion stoichiometry of the clusters is retained in the nanocrystalline materials. |
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| AbstractList | Abstract
The ternary molecular nanoclusters [Zn
x
Cd
10−
x
Se
4
(SePh)
12
(P
n
Pr
3
)
4
] (
x
=1.8,
1 a
;
x
=2.6,
1 b
) were employed as single‐source precursors for the synthesis of high‐quality hexagonal Zn
x
Cd
1−
x
Se nanocrystals. The tellurium clusters [Zn
x
Cd
10−
x
Te
4
(TePh)
12
(P
n
Pr
3
)
4
] (
x
=1.8,
2 a
;
x
=2.6,
2 b
) are equally convenient precursors for the synthesis cubic Zn
x
Cd
1−
x
E nanoparticles. The thermolysis of the cluster molecules in hexadecylamine provides an efficient system in which the inherent metal‐ion stoichiometry of the clusters is retained in the nanocrystalline products, whilst also affording control of particle size within the 2–5 nm range. In all cases, the nanoparticles are monodisperse, and luminescence spectra exhibit emission energies close to the absorption edge. Analysis of the optical spectra and X‐ray diffraction patterns of these materials indicates a metal‐ion concentration gradient within the structures of the nanocrystals, with Zn
II
ions predominantly located near the surface of the particles. The ternary molecular nanoclusters [Zn(x)Cd(10-x)Se4(SePh)12(PnPr3)4] (x = 1.8, 1 a; x = 2.6, 1 b) were employed as single-source precursors for the synthesis of high-quality hexagonal Zn(x)Cd(1-x)Se nanocrystals. The tellurium clusters [Zn(x)Cd(10-x)Te4(TePh)12(PnPr3)4] (x = 1.8, 2 a; x = 2.6, 2 b) are equally convenient precursors for the synthesis cubic Zn(x)Cd(1-x)E nanoparticles. The thermolysis of the cluster molecules in hexadecylamine provides an efficient system in which the inherent metal-ion stoichiometry of the clusters is retained in the nanocrystalline products, whilst also affording control of particle size within the 2-5 nm range. In all cases, the nanoparticles are monodisperse, and luminescence spectra exhibit emission energies close to the absorption edge. Analysis of the optical spectra and X-ray diffraction patterns of these materials indicates a metal-ion concentration gradient within the structures of the nanocrystals, with Zn(II) ions predominantly located near the surface of the particles. The ternary molecular nanoclusters [ZnxCd10−xSe4(SePh)12(PnPr3)4] (x=1.8, 1 a; x=2.6, 1 b) were employed as single‐source precursors for the synthesis of high‐quality hexagonal ZnxCd1−xSe nanocrystals. The tellurium clusters [ZnxCd10−xTe4(TePh)12(PnPr3)4] (x=1.8, 2 a; x=2.6, 2 b) are equally convenient precursors for the synthesis cubic ZnxCd1−xE nanoparticles. The thermolysis of the cluster molecules in hexadecylamine provides an efficient system in which the inherent metal‐ion stoichiometry of the clusters is retained in the nanocrystalline products, whilst also affording control of particle size within the 2–5 nm range. In all cases, the nanoparticles are monodisperse, and luminescence spectra exhibit emission energies close to the absorption edge. Analysis of the optical spectra and X‐ray diffraction patterns of these materials indicates a metal‐ion concentration gradient within the structures of the nanocrystals, with ZnII ions predominantly located near the surface of the particles. Zinc into it! Ternary Zn‐Cd‐Se and Zn‐Cd‐Te molecular nanoclusters have been employed as single‐source precursors for the synthesis of high‐quality ZnxCd1−xSe and ZnxCd1−xTe (illustrated) nanocrystals, respectively. The thermolysis of the molecular precursors in hexadecylamine solvent provides a route in which the inherent metal‐ion stoichiometry of the clusters is retained in the nanocrystalline materials. |
| Author | Corrigan, John F. DeGroot, Marty W. Rösner, Harald |
| Author_xml | – sequence: 1 givenname: Marty W. surname: DeGroot fullname: DeGroot, Marty W. organization: Department of Chemistry, The University of Western Ontario, London, N6 A 5B7, Canada, Fax: (+1) 519-661-3022 – sequence: 2 givenname: Harald surname: Rösner fullname: Rösner, Harald organization: Institut für Nanotechnologie, Forschungszentrum Karlsruhe in der Helmholtz-Gemeinschaft, Hermann-von-Helmholtz-Platz 1, 76344 Eggenstein-Leopoldshafen, Germany – sequence: 3 givenname: John F. surname: Corrigan fullname: Corrigan, John F. email: corrigan@uwo.ca organization: Department of Chemistry, The University of Western Ontario, London, N6 A 5B7, Canada, Fax: (+1) 519-661-3022 |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/16317798$$D View this record in MEDLINE/PubMed |
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F. (e_1_2_6_68_2) 2004 e_1_2_6_82_2 e_1_2_6_8_2 e_1_2_6_29_2 e_1_2_6_4_2 e_1_2_6_48_2 e_1_2_6_21_2 e_1_2_6_44_2 e_1_2_6_67_2 e_1_2_6_25_2 e_1_2_6_67_3 |
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| Snippet | The ternary molecular nanoclusters [ZnxCd10−xSe4(SePh)12(PnPr3)4] (x=1.8, 1 a; x=2.6, 1 b) were employed as single‐source precursors for the synthesis of... The ternary molecular nanoclusters [Zn(x)Cd(10-x)Se4(SePh)12(PnPr3)4] (x = 1.8, 1 a; x = 2.6, 1 b) were employed as single-source precursors for the synthesis... Abstract The ternary molecular nanoclusters [Zn x Cd 10− x Se 4 (SePh) 12 (P n Pr 3 ) 4 ] ( x =1.8, 1 a ; x =2.6, 1 b ) were employed as single‐source... |
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| SubjectTerms | cadmium chalcogens cluster compounds nanostructures zinc |
| Title | Control of Metal-Ion Composition in the Synthesis of Ternary II-II′-VI Nanoparticles by Using a Mixed-Metal Cluster Precursor Approach |
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