Synthesis of popcorn-shaped gallium-platinum (GaPt3) nanoparticles as highly efficient and stable electrocatalysts for hydrogen evolution reaction
The hydrogen evolution reaction (HER) holds great promise for clean energy, where electrocatalysts for HER perform as the cathode reaction of water splitting is the critical reaction process on fuel cell. In spite of the rapid growth of alternative materials, platinum (Pt)-based or platinum alloy ma...
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| Published in | Electrochimica acta Vol. 297; pp. 288 - 296 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
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Oxford
Elsevier Ltd
20.02.2019
Elsevier BV |
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| Abstract | The hydrogen evolution reaction (HER) holds great promise for clean energy, where electrocatalysts for HER perform as the cathode reaction of water splitting is the critical reaction process on fuel cell. In spite of the rapid growth of alternative materials, platinum (Pt)-based or platinum alloy materials are still the most efficient catalysts for HER. Here, we report a hot-solvent synthesis for producing pop-corn shaped gallium-platinum (GaPt3) nanoparticles, which exhibits intermetallic behavior with abundant uneven surfaces that guarantee the extensive catalytic active edge sites. The electrochemical catalytic activity of GaPt3-based electrode towards HER was demonstrated for the first time, resulting an outstanding performance of only 27 mV overpotential to achieve the 10 mA/cm2 current density and a Tafel slope of 43.3 mV/dec. (vs. RHE) in acidic media, which is rather superior to that of commercial Pt catalysts and a relatively low overpotential (<80 mV) was obtained even operated at large area (5 cm2). Moreover, cycling tests for 10000-cycle CV sweep (−0.3 to 0.2 V vs. RHE) and durability test for 48 h were applied and the performance remains still, thus giving the confirmation to the long-lasting feature of GaPt3 nanoparticles.
The GaPt3 nanoparticles with pop-corn like appearance were prepared via hot-solvent synthesis for the first time, exhibit high-performance catalytic and long-lasting properties as HER electrodes. [Display omitted] |
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| AbstractList | The hydrogen evolution reaction (HER) holds great promise for clean energy, where electrocatalysts for HER perform as the cathode reaction of water splitting is the critical reaction process on fuel cell. In spite of the rapid growth of alternative materials, platinum (Pt)-based or platinum alloy materials are still the most efficient catalysts for HER. Here, we report a hot-solvent synthesis for producing pop-corn shaped gallium-platinum (GaPt3) nanoparticles, which exhibits intermetallic behavior with abundant uneven surfaces that guarantee the extensive catalytic active edge sites. The electrochemical catalytic activity of GaPt3-based electrode towards HER was demonstrated for the first time, resulting an outstanding performance of only 27 mV overpotential to achieve the 10 mA/cm2 current density and a Tafel slope of 43.3 mV/dec. (vs. RHE) in acidic media, which is rather superior to that of commercial Pt catalysts and a relatively low overpotential (<80 mV) was obtained even operated at large area (5 cm2). Moreover, cycling tests for 10000-cycle CV sweep (−0.3 to 0.2 V vs. RHE) and durability test for 48 h were applied and the performance remains still, thus giving the confirmation to the long-lasting feature of GaPt3 nanoparticles.
The GaPt3 nanoparticles with pop-corn like appearance were prepared via hot-solvent synthesis for the first time, exhibit high-performance catalytic and long-lasting properties as HER electrodes. [Display omitted] The hydrogen evolution reaction (HER) holds great promise for clean energy, where electrocatalysts for HER perform as the cathode reaction of water splitting is the critical reaction process on fuel cell. In spite of the rapid growth of alternative materials, platinum (Pt)-based or platinum alloy materials are still the most efficient catalysts for HER. Here, we report a hot-solvent synthesis for producing pop-corn shaped gallium-platinum (GaPt3) nanoparticles, which exhibits intermetallic behavior with abundant uneven surfaces that guarantee the extensive catalytic active edge sites. The electrochemical catalytic activity of GaPt3-based electrode towards HER was demonstrated for the first time, resulting an outstanding performance of only 27 mV overpotential to achieve the 10 mA/cm2 current density and a Tafel slope of 43.3 mV/dec. (vs. RHE) in acidic media, which is rather superior to that of commercial Pt catalysts and a relatively low overpotential (<80 mV) was obtained even operated at large area (5 cm2). Moreover, cycling tests for 10000-cycle CV sweep (−0.3 to 0.2 V vs. RHE) and durability test for 48 h were applied and the performance remains still, thus giving the confirmation to the long-lasting feature of GaPt3 nanoparticles. |
| Author | Chen, Kuan-Ting Tuan, Hsing-Yu Lim, Suh-Ciuan Chan, Cheng-Ying |
| Author_xml | – sequence: 1 givenname: Suh-Ciuan surname: Lim fullname: Lim, Suh-Ciuan – sequence: 2 givenname: Cheng-Ying surname: Chan fullname: Chan, Cheng-Ying – sequence: 3 givenname: Kuan-Ting surname: Chen fullname: Chen, Kuan-Ting – sequence: 4 givenname: Hsing-Yu surname: Tuan fullname: Tuan, Hsing-Yu email: hytuan@che.nthu.edu.tw |
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| SubjectTerms | Catalysis Catalysts Catalytic activity Cathodic cleaning Chemical synthesis Clean energy Corn Electrocatalysts Fuel cell Fuel cells Gallium Hydrogen evolution reaction Hydrogen evolution reactions Nanoparticles Platinum Platinum alloy Platinum base alloys Popcorn-shaped Water splitting |
| Title | Synthesis of popcorn-shaped gallium-platinum (GaPt3) nanoparticles as highly efficient and stable electrocatalysts for hydrogen evolution reaction |
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