Supramolecular Stacks of Bis(imidazolyl)porphyrin through Metal Coordination
cis- and trans-bis(1-methyl-2-imidazolyl)tetraethyltetramethylporphyrin Mg complexes were prepared. 1H NMR, absorption, and fluorescence spectra suggest that Mg has a high tendency toward dimer formation through coordination from imidazolyl to metal in a similar way to Zn, and accepts further the si...
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| Published in | Bulletin of the Chemical Society of Japan Vol. 69; no. 12; pp. 3563 - 3569 |
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| Main Authors | , |
| Format | Journal Article |
| Language | English |
| Published |
TOKYO
The Chemical Society of Japan
01.12.1996
Chemical Soc Japan Chemical Society of Japan |
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| Abstract | cis- and trans-bis(1-methyl-2-imidazolyl)tetraethyltetramethylporphyrin Mg complexes were prepared. 1H NMR, absorption, and fluorescence spectra suggest that Mg has a high tendency toward dimer formation through coordination from imidazolyl to metal in a similar way to Zn, and accepts further the sixth coordination, which never occurred in Zn complexes. Propagation of the organization from a dimer to a trimer for trans-Mg complex starts at such a low concentration level as 10−5 M (1 M = 1 mol dm−3) and a 2 × 10−3 M solution organized the system to a 2.34 mer on average. |
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| AbstractList | Abstract
cis- and trans-bis(1-methyl-2-imidazolyl)tetraethyltetramethylporphyrin Mg complexes were prepared. 1H NMR, absorption, and fluorescence spectra suggest that Mg has a high tendency toward dimer formation through coordination from imidazolyl to metal in a similar way to Zn, and accepts further the sixth coordination, which never occurred in Zn complexes. Propagation of the organization from a dimer to a trimer for trans-Mg complex starts at such a low concentration level as 10−5 M (1 M = 1 mol dm−3) and a 2 × 10−3 M solution organized the system to a 2.34 mer on average. cis- and trans-bis(1-methyl-2-imidazolyl)tetraethyltetramethylporphyrin Mg complexes were prepared. 1H NMR, absorption, and fluorescence spectra suggest that Mg has a high tendency toward dimer formation through coordination from imidazolyl to metal in a similar way to Zn, and accepts further the sixth coordination, which never occurred in Zn complexes. Propagation of the organization from a dimer to a trimer for trans-Mg complex starts at such a low concentration level as 10-5 M (1 M = 1 mol dm-3) and a 2 × 10-3 M solution organized the system to a 2.34 mer on average. cis- and trans-bis(1-methyl-2-imidazolyl)tetraethyltetramethylporphyrin Mg complexes were prepared. 1H NMR, absorption, and fluorescence spectra suggest that Mg has a high tendency toward dimer formation through coordination from imidazolyl to metal in a similar way to Zn, and accepts further the sixth coordination, which never occurred in Zn complexes. Propagation of the organization from a dimer to a trimer for trans-Mg complex starts at such a low concentration level as 10−5 M (1 M = 1 mol dm−3) and a 2 × 10−3 M solution organized the system to a 2.34 mer on average. cis- and trans-bis(1-methyl-2-imidazolyl)tetraethyltetramethylprophyrin Mg complexes were prepared. H-1 NMR, absorption, and fluorescence spectra suggest that Mg has a high tendency toward dimer formation through coordination from imidazolyl to metal in a similar way to Zn, and accepts further the sixth coordination, which never occurred in Zn complexes. Propagation of the organization from a dimer to a trimer for trans-Mg complex starts at such a low concentration level as 10(-5) M (1 M=1 mol dm(-3)) and a 2x10(-3) M solution organized the system to a 2.34 mer on average. |
| Author | Miyaji, Hidekazu Kobuke, Yoshiaki |
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| Keywords | NETWORK LIGHT-HARVESTING COMPLEX PORPHYRIN BUILDING-BLOCKS |
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| Snippet | cis- and trans-bis(1-methyl-2-imidazolyl)tetraethyltetramethylporphyrin Mg complexes were prepared. 1H NMR, absorption, and fluorescence spectra suggest that... cis- and trans-bis(1-methyl-2-imidazolyl)tetraethyltetramethylprophyrin Mg complexes were prepared. H-1 NMR, absorption, and fluorescence spectra suggest that... Abstract cis- and trans-bis(1-methyl-2-imidazolyl)tetraethyltetramethylporphyrin Mg complexes were prepared. 1H NMR, absorption, and fluorescence spectra... |
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| SubjectTerms | Chemistry Chemistry, Multidisciplinary Physical Sciences Science & Technology |
| Title | Supramolecular Stacks of Bis(imidazolyl)porphyrin through Metal Coordination |
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