Solvent effects in microemulsion electrokinetic chromatography
The contribution of organic solvents to the mechanisms responsible for separation in microemulsion electrokinetic chromatography (MEEKC) is reviewed. Organic solvents are needed as constituents of microemulsions for a series of reasons. (i) A water‐immiscible organic substance is used to form the ac...
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| Published in | Electrophoresis Vol. 24; no. 10; pp. 1537 - 1543 |
|---|---|
| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
WILEY-VCH Verlag
01.05.2003
WILEY‐VCH Verlag |
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| Online Access | Get full text |
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| Abstract | The contribution of organic solvents to the mechanisms responsible for separation in microemulsion electrokinetic chromatography (MEEKC) is reviewed. Organic solvents are needed as constituents of microemulsions for a series of reasons. (i) A water‐immiscible organic substance is used to form the actual oil phase of the microemulsion, (ii) a less hydrophobic solvent is commonly employed as a so‐called cosurfactant, and (iii) in many cases an organic modifier is added to influence the solubility of the analytes in the aqueous phase of the microemulsion. All these organic solvents do not only participate in the separation in their actual function, but also interact with each other and the analytes. Variations in separation selectivities triggered by changes in the nature and/or concentration of these organic solvents present in microemulsions suitable for MEEKC are discussed in this work. |
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| AbstractList | The contribution of organic solvents to the mechanisms responsible for separation in microemulsion electrokinetic chromatography (MEEKC) is reviewed. Organic solvents are needed as constituents of microemulsions for a series of reasons. (i). A water-immiscible organic substance is used to form the actual oil phase of the microemulsion, (ii). a less hydrophobic solvent is commonly employed as a so-called co-surfactant, and (iii). in many cases an organic modifier is added to influence the solubility of the analytes in the aqueous phase of the microemulsion. All these organic solvents do not only participate in the separation in their actual function, but also interact with each other and the analytes. Variations in separation selectivities triggered by changes in the nature and/or concentration of these organic solvents present in microemulsions suitable for MEEKC are discussed in this work. The contribution of organic solvents to the mechanisms responsible for separation in microemulsion electrokinetic chromatography (MEEKC) is reviewed. Organic solvents are needed as constituents of microemulsions for a series of reasons. (i) A water‐immiscible organic substance is used to form the actual oil phase of the microemulsion, (ii) a less hydrophobic solvent is commonly employed as a so‐called cosurfactant, and (iii) in many cases an organic modifier is added to influence the solubility of the analytes in the aqueous phase of the microemulsion. All these organic solvents do not only participate in the separation in their actual function, but also interact with each other and the analytes. Variations in separation selectivities triggered by changes in the nature and/or concentration of these organic solvents present in microemulsions suitable for MEEKC are discussed in this work. Abstract The contribution of organic solvents to the mechanisms responsible for separation in microemulsion electrokinetic chromatography (MEEKC) is reviewed. Organic solvents are needed as constituents of microemulsions for a series of reasons. (i) A water‐immiscible organic substance is used to form the actual oil phase of the microemulsion, (ii) a less hydrophobic solvent is commonly employed as a so‐called cosurfactant, and (iii) in many cases an organic modifier is added to influence the solubility of the analytes in the aqueous phase of the microemulsion. All these organic solvents do not only participate in the separation in their actual function, but also interact with each other and the analytes. Variations in separation selectivities triggered by changes in the nature and/or concentration of these organic solvents present in microemulsions suitable for MEEKC are discussed in this work. |
| Author | Klampfl, Christian W. |
| Author_xml | – sequence: 1 givenname: Christian W. surname: Klampfl fullname: Klampfl, Christian W. email: christian.klampfl@jku.at organization: Department of Analytical Chemistry, Johannes Kepler-University Linz, Linz, Austria |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/12761783$$D View this record in MEDLINE/PubMed |
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| SubjectTerms | Chromatography, Micellar Electrokinetic Capillary - methods Emulsions Microemulsion electrokinetic chromatography Organic Chemicals - chemistry Review Separation mechanism Solvent effects Solvents - chemistry Surface-Active Agents - chemistry |
| Title | Solvent effects in microemulsion electrokinetic chromatography |
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