Influence of membrane skin morphology on CO2/N2 separation at sub-ambient temperatures
Matrimid® hollow fiber membranes with silicone rubber (PDMS) calked fused nodular selective layers display much higher CO2/N2 selectivity as well as higher CO2 permeance than those with isotropic dense selective layers at 253.15 K. Two kinds of asymmetric hollow fiber membranes were successfully spu...
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Published in | Journal of membrane science Vol. 446; pp. 433 - 439 |
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Main Authors | , , , , , , |
Format | Journal Article |
Language | English |
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Elsevier B.V
01.11.2013
Elsevier |
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Abstract | Matrimid® hollow fiber membranes with silicone rubber (PDMS) calked fused nodular selective layers display much higher CO2/N2 selectivity as well as higher CO2 permeance than those with isotropic dense selective layers at 253.15 K. Two kinds of asymmetric hollow fiber membranes were successfully spun: fibers with fused nodular skins and fibers with truly dense skins. The skin morphologies were confirmed with SEM images. CO2/N2 mixed gas permeation characterization was carried out within the temperature range of 253.15 K to 308.15 K. Permeation results showed that, at 253.15 K, the nodular-skinned fibers displayed CO2/N2 selectivity of 90.5, and CO2 permeance of 63.3GPU after standard PDMS calking; while the dense-skinned fibers displayed CO2/N2 selectivity of 52.5, and CO2 permeance of 16.6GPU. The PDMS calking had negligible effect on the dense-skinned fibers, but it was necessary for the fused nodular-skinned fibers. A hypothesis regarding the introduction of Langmuir sorption sites and a local orientation of polymer chain segments is proposed to explain the better performance of the calked nodular-skinned fibers. This work provides a promising method for improved hollow fiber membranes for the removal of CO2 from flue gas.
•Formation of asymmetric hollow fiber membranes with fused nodular selective layers.•Nodular skin has high permeance and high selectivity at sub-ambient temperatures.•Propose a hypothesis of added Langmuir sorption sites.•Propose a hypothesis of local orientation of polymer chain segments. |
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AbstractList | MatrimidARG hollow fiber membranes with silicone rubber (PDMS) calked fused nodular selective layers display much higher CO2/N2 selectivity as well as higher CO2 permeance than those with isotropic dense selective layers at 253.15 K. Two kinds of asymmetric hollow fiber membranes were successfully spun: fibers with fused nodular skins and fibers with truly dense skins. The skin morphologies were confirmed with SEM images. CO2/N2 mixed gas permeation characterization was carried out within the temperature range of 253.15 K to 308.15 K. Permeation results showed that, at 253.15 K, the nodular-skinned fibers displayed CO2/N2 selectivity of 90.5, and CO2 permeance of 63.3 GPU after standard PDMS calking; while the dense-skinned fibers displayed CO2/N2 selectivity of 52.5, and CO2 permeance of 16.6 GPU. The PDMS calking had negligible effect on the dense-skinned fibers, but it was necessary for the fused nodular-skinned fibers. A hypothesis regarding the introduction of Langmuir sorption sites and a local orientation of polymer chain segments is proposed to explain the better performance of the calked nodular-skinned fibers. This work provides a promising method for improved hollow fiber membranes for the removal of CO2 from flue gas. Matrimid® hollow fiber membranes with silicone rubber (PDMS) calked fused nodular selective layers display much higher CO₂/N₂ selectivity as well as higher CO₂ permeance than those with isotropic dense selective layers at 253.15 K. Two kinds of asymmetric hollow fiber membranes were successfully spun: fibers with fused nodular skins and fibers with truly dense skins. The skin morphologies were confirmed with SEM images. CO₂/N₂ mixed gas permeation characterization was carried out within the temperature range of 253.15 K to 308.15 K. Permeation results showed that, at 253.15 K, the nodular-skinned fibers displayed CO₂/N₂ selectivity of 90.5, and CO₂ permeance of 63.3GPU after standard PDMS calking; while the dense-skinned fibers displayed CO₂/N₂ selectivity of 52.5, and CO₂ permeance of 16.6GPU. The PDMS calking had negligible effect on the dense-skinned fibers, but it was necessary for the fused nodular-skinned fibers. A hypothesis regarding the introduction of Langmuir sorption sites and a local orientation of polymer chain segments is proposed to explain the better performance of the calked nodular-skinned fibers. This work provides a promising method for improved hollow fiber membranes for the removal of CO₂ from flue gas. Matrimid® hollow fiber membranes with silicone rubber (PDMS) calked fused nodular selective layers display much higher CO2/N2 selectivity as well as higher CO2 permeance than those with isotropic dense selective layers at 253.15 K. Two kinds of asymmetric hollow fiber membranes were successfully spun: fibers with fused nodular skins and fibers with truly dense skins. The skin morphologies were confirmed with SEM images. CO2/N2 mixed gas permeation characterization was carried out within the temperature range of 253.15 K to 308.15 K. Permeation results showed that, at 253.15 K, the nodular-skinned fibers displayed CO2/N2 selectivity of 90.5, and CO2 permeance of 63.3GPU after standard PDMS calking; while the dense-skinned fibers displayed CO2/N2 selectivity of 52.5, and CO2 permeance of 16.6GPU. The PDMS calking had negligible effect on the dense-skinned fibers, but it was necessary for the fused nodular-skinned fibers. A hypothesis regarding the introduction of Langmuir sorption sites and a local orientation of polymer chain segments is proposed to explain the better performance of the calked nodular-skinned fibers. This work provides a promising method for improved hollow fiber membranes for the removal of CO2 from flue gas. •Formation of asymmetric hollow fiber membranes with fused nodular selective layers.•Nodular skin has high permeance and high selectivity at sub-ambient temperatures.•Propose a hypothesis of added Langmuir sorption sites.•Propose a hypothesis of local orientation of polymer chain segments. |
Author | Kulkarni, Sudhir Karvan, Oguz Johnson, Justin R. Koros, William J. Liu, Lu Hasse, David J. Sanders, Edgar S. |
Author_xml | – sequence: 1 givenname: Lu surname: Liu fullname: Liu, Lu – sequence: 2 givenname: Edgar S. surname: Sanders fullname: Sanders, Edgar S. – sequence: 3 givenname: Justin R. surname: Johnson fullname: Johnson, Justin R. – sequence: 4 givenname: Oguz surname: Karvan fullname: Karvan, Oguz – sequence: 5 givenname: Sudhir surname: Kulkarni fullname: Kulkarni, Sudhir – sequence: 6 givenname: David J. surname: Hasse fullname: Hasse, David J. – sequence: 7 givenname: William J. surname: Koros fullname: Koros, William J. email: bill.koros@chbe.gatech.edu |
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Keywords | CO2/N2 separation Asymmetric hollow fiber membrane Langmuir sorption site Sub-ambient temperature Nodular skin Polymeric membrane Separation CO N Sorption Adsorption Morphology Hollow fiber Asymmetric membrane |
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Snippet | Matrimid® hollow fiber membranes with silicone rubber (PDMS) calked fused nodular selective layers display much higher CO2/N2 selectivity as well as higher CO2... Matrimid® hollow fiber membranes with silicone rubber (PDMS) calked fused nodular selective layers display much higher CO₂/N₂ selectivity as well as higher CO₂... MatrimidARG hollow fiber membranes with silicone rubber (PDMS) calked fused nodular selective layers display much higher CO2/N2 selectivity as well as higher... |
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SubjectTerms | Applied sciences artificial membranes Asymmetric hollow fiber membrane Carbon dioxide Chemistry CO2/N2 separation Colloidal state and disperse state Exact sciences and technology Exchange resins and membranes Fibers Flue gases Forms of application and semi-finished materials General and physical chemistry Langmuir sorption site Membranes Morphology Nodular skin Polymer industry, paints, wood Reluctance rubber scanning electron microscopy Selectivity silicone Silicone resins sorption Sub-ambient temperature Surface physical chemistry Technology of polymers temperature |
Title | Influence of membrane skin morphology on CO2/N2 separation at sub-ambient temperatures |
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