Formation and microstructure of nanoporous silver by dealloying rapidly solidified Zn–Ag alloys

► Nanoporous silver can be fabricated by electrochemical dealloying of Zn–Ag alloys. ► Phase constitution markedly affects electrochemical activities of Zn–Ag alloys. ► Formation of nanoporous silver is sensitive to the change of applied potentials. The electrochemical dealloying of rapidly solidifi...

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Published in	Electrochimica acta Vol. 63; pp. 302 - 311
Main Authors	Zhang, Chi, Sun, Junzhe, Xu, Junling, Wang, Xiaoguang, Ji, Hong, Zhao, Changchun, Zhang, Zhonghua
Format	Journal Article
Language	English
Published	Kidlington Elsevier Ltd 29.02.2012 Elsevier
Subjects	Alloys Applied sciences Corrosion Corrosion mechanisms Dealloying Exact sciences and technology Metals. Metallurgy Nanocomposites Nanomaterials Nanoporous silver Nanostructure Potentiodynamic polarization Potentiostatic polarization Silver Silver base alloys Zinc base alloys Zn–Ag alloys Nanoporous silver Potentiostatic polarization Zn–Ag alloys Potentiodynamic polarization Dealloying Zn-Ag alloys Transition metal Nanoporous materials Potentiodynamic method Corrosion Silver alloy Electrochemical polarization Microstructure Formation Zinc alloy Binary alloy
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ISSN	0013-4686 1873-3859
DOI	10.1016/j.electacta.2011.12.103

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Abstract	► Nanoporous silver can be fabricated by electrochemical dealloying of Zn–Ag alloys. ► Phase constitution markedly affects electrochemical activities of Zn–Ag alloys. ► Formation of nanoporous silver is sensitive to the change of applied potentials. The electrochemical dealloying of rapidly solidified (RS) Zn–Ag alloys in a 5wt.% HCl solution and 1M NaCl solution has been investigated using electrochemical measurements and microstructural analysis. The results show that the electrochemical properties of the RS Zn–Ag alloys are associated not only with the alloy composition, but with the phase constitution of the alloys. Nanoporous silver (NPS) ribbons can be fabricated through potentiostatically dealloying the RS Zn–Ag alloys in both solutions. Moreover, a minor difference in the applied potential has a significant influence on the dealloying process and formation of NPS. The critical potential and polarization behavior of the Zn–Ag alloys have also been discussed, as well as surface diffusion of Ag adatoms.
AbstractList	► Nanoporous silver can be fabricated by electrochemical dealloying of Zn–Ag alloys. ► Phase constitution markedly affects electrochemical activities of Zn–Ag alloys. ► Formation of nanoporous silver is sensitive to the change of applied potentials. The electrochemical dealloying of rapidly solidified (RS) Zn–Ag alloys in a 5wt.% HCl solution and 1M NaCl solution has been investigated using electrochemical measurements and microstructural analysis. The results show that the electrochemical properties of the RS Zn–Ag alloys are associated not only with the alloy composition, but with the phase constitution of the alloys. Nanoporous silver (NPS) ribbons can be fabricated through potentiostatically dealloying the RS Zn–Ag alloys in both solutions. Moreover, a minor difference in the applied potential has a significant influence on the dealloying process and formation of NPS. The critical potential and polarization behavior of the Zn–Ag alloys have also been discussed, as well as surface diffusion of Ag adatoms. The electrochemical dealloying of rapidly solidified (RS) Zn-Ag alloys in a 5 wt.% HCl solution and 1 M NaCl solution has been investigated using electrochemical measurements and microstructural analysis. The results show that the electrochemical properties of the RS Zn-Ag alloys are associated not only with the alloy composition, but with the phase constitution of the alloys. Nanoporous silver (NPS) ribbons can be fabricated through potentiostatically dealloying the RS Zn-Ag alloys in both solutions. Moreover, a minor difference in the applied potential has a significant influence on the dealloying process and formation of NPS. The critical potential and polarization behavior of the Zn-Ag alloys have also been discussed, as well as surface diffusion of Ag adatoms.
Author	Sun, Junzhe Wang, Xiaoguang Xu, Junling Zhao, Changchun Zhang, Chi Zhang, Zhonghua Ji, Hong
Author_xml	– sequence: 1 givenname: Chi surname: Zhang fullname: Zhang, Chi – sequence: 2 givenname: Junzhe surname: Sun fullname: Sun, Junzhe – sequence: 3 givenname: Junling surname: Xu fullname: Xu, Junling – sequence: 4 givenname: Xiaoguang surname: Wang fullname: Wang, Xiaoguang – sequence: 5 givenname: Hong surname: Ji fullname: Ji, Hong – sequence: 6 givenname: Changchun surname: Zhao fullname: Zhao, Changchun – sequence: 7 givenname: Zhonghua surname: Zhang fullname: Zhang, Zhonghua email: zh_zhang@sdu.edu.cn
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Keywords	Nanoporous silver Potentiostatic polarization Zn–Ag alloys Potentiodynamic polarization Dealloying Zn-Ag alloys Transition metal Nanoporous materials Potentiodynamic method Corrosion Silver alloy Electrochemical polarization Microstructure Formation Zinc alloy Binary alloy
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Snippet	► Nanoporous silver can be fabricated by electrochemical dealloying of Zn–Ag alloys. ► Phase constitution markedly affects electrochemical activities of Zn–Ag... The electrochemical dealloying of rapidly solidified (RS) Zn-Ag alloys in a 5 wt.% HCl solution and 1 M NaCl solution has been investigated using...
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SubjectTerms	Alloys Applied sciences Corrosion Corrosion mechanisms Dealloying Exact sciences and technology Metals. Metallurgy Nanocomposites Nanomaterials Nanoporous silver Nanostructure Potentiodynamic polarization Potentiostatic polarization Silver Silver base alloys Zinc base alloys Zn–Ag alloys
Title	Formation and microstructure of nanoporous silver by dealloying rapidly solidified Zn–Ag alloys
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