In-depth quantitative analysis of the microstructures produced by Surface Mechanical Attrition Treatment (SMAT)
Electron BackScattered Diffraction (EBSD) maps are used to characterize quantitatively the graded microstructure formed by Surface Mechanical Attrition Treatment (SMAT) and applied here to the 316L stainless steel. In particular, the analysis of GNDs - coupled with relevant and reliable criteria - w...
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| Published in | Materials characterization Vol. 83; pp. 129 - 138 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
New York, NY
Elsevier
01.09.2013
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| Subjects | |
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| Abstract | Electron BackScattered Diffraction (EBSD) maps are used to characterize quantitatively the graded microstructure formed by Surface Mechanical Attrition Treatment (SMAT) and applied here to the 316L stainless steel. In particular, the analysis of GNDs - coupled with relevant and reliable criteria - was used to depict the thickness of each zone identified in the SMAT-affected layers: (i) the "ultrafine grain" (UFG) zone present at the extreme top surface, (ii), the "transition zone" where grains were fragmented under the heavy plastic deformation and, finally, (iii) the "deformed zone" where initial grains are simply deformed. The interest of this procedure is illustrated through the comparative analysis of the effect of some SMAT processing parameters (amplitude of vibration and treatment duration). The UFG and transition zones are more significantly modified than the overall affected thickness under our tested conditions. |
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| AbstractList | Electron BackScattered Diffraction (EBSD) maps are used to characterize quantitatively the graded microstructure formed by Surface Mechanical Attrition Treatment (SMAT) and applied here to the 316L stainless steel. In particular, the analysis of GNDs - coupled with relevant and reliable criteria - was used to depict the thickness of each zone identified in the SMAT-affected layers: (i) the ``ultrafine grain'' (UFG) zone present at the extreme top surface, (ii), the ``transition zone'' where grains were fragmented under the heavy plastic deformation and, finally, (iii) the ``deformed zone'' where initial grains are simply deformed. The interest of this procedure is illustrated through the comparative analysis of the effect of some SMAT processing parameters (amplitude of vibration and treatment duration). The UFG and transition zones are more significantly modified than the overall affected thickness under our tested conditions. Electron BackScattered Diffraction (EBSD) maps are used to characterize quantitatively the graded microstructure formed by Surface Mechanical Attrition Treatment (SMAT) and applied here to the 316L stainless steel. In particular, the analysis of GNDs – coupled with relevant and reliable criteria – was used to depict the thickness of each zone identified in the SMAT-affected layers: (i) the “ultrafine grain” (UFG) zone present at the extreme top surface, (ii), the “transition zone” where grains were fragmented under the heavy plastic deformation and, finally, (iii) the “deformed zone” where initial grains are simply deformed. The interest of this procedure is illustrated through the comparative analysis of the effect of some SMAT processing parameters (amplitude of vibration and treatment duration). The UFG and transition zones are more significantly modified than the overall affected thickness under our tested conditions. - Highlights: • EBSD maps are used to characterize quantitatively the microstructure of SMAT treated samples. • Calculation of the GND density to quantify strain gradients • A new method to depict the different zone thicknesses in the SMAT affected layer • Effects of SMAT processing parameters on the surface microstructure evolution. |
| Author | BEAUSIR, B GROSDIDIER, T SAMIH, Y BOLLE, B |
| Author_xml | – sequence: 1 givenname: Y surname: SAMIH fullname: SAMIH, Y organization: Université de Lorraine, Laboratoire d'Etude des Microstructures et de Mécanique des Matériaux (LEM3), CNRS UMR 7239, Metz 57045, France – sequence: 2 givenname: B surname: BEAUSIR fullname: BEAUSIR, B organization: Université de Lorraine, Laboratoire d'Etude des Microstructures et de Mécanique des Matériaux (LEM3), CNRS UMR 7239, Metz 57045, France – sequence: 3 givenname: B surname: BOLLE fullname: BOLLE, B organization: Université de Lorraine, Laboratoire d'Etude des Microstructures et de Mécanique des Matériaux (LEM3), CNRS UMR 7239, Metz 57045, France – sequence: 4 givenname: T surname: GROSDIDIER fullname: GROSDIDIER, T organization: Université de Lorraine, Laboratoire d'Etude des Microstructures et de Mécanique des Matériaux (LEM3), CNRS UMR 7239, Metz 57045, France |
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| Keywords | Grain size Chemical analysis Electron diffraction Mechanical properties Surface treatments Plastic deformation SMAT Stainless steels EBSD Mechanical treatment Stainless steel Microstructure GND Grain refinement Quantitative chemical analysis |
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| SubjectTerms | Applied sciences Attrition Austenitic stainless steels BACKSCATTERING Chemical Sciences Cross-disciplinary physics: materials science; rheology Deformation DENSITY Electron back scatter diffraction ELECTRON DIFFRACTION Engineering Sciences Exact sciences and technology GRAIN REFINEMENT Grains Heat resistant steels LAYERS Material chemistry MATERIALS SCIENCE Mechanical properties and methods of testing. Rheology. Fracture mechanics. Tribology Metals. Metallurgy MICROSTRUCTURE Phase diagrams and microstructures developed by solidification and solid-solid phase transformations Physics PLASTICITY Quantitative analysis Solidification STAINLESS STEELS SURFACES THICKNESS Vibration |
| Title | In-depth quantitative analysis of the microstructures produced by Surface Mechanical Attrition Treatment (SMAT) |
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