Effect of layer structures of gold nanoparticle films on surface enhanced Raman scattering

Using a method of collecting nanoparticles at a water/hexane interface in a close-packed monolayer film and transferring such films onto a solid substrate, three-dimensional multilayer films of nanoparticles were formed. The packed nanoparticles were gold nanospheres (NS) with a 26 nm diameter or go...

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Published in	Analytica chimica acta Vol. 649; no. 1; pp. 111 - 116
Main Authors	Oh, Min Kyung, Yun, Sukang, Kim, Seong Kyu, Park, Sungho
Format	Journal Article
Language	English
Published	Amsterdam Elsevier B.V 01.09.2009 Elsevier
Subjects	Analytical chemistry Chemistry Exact sciences and technology Extinction spectroscopy Gold film Nanoparticle Plasmon Spectrometric and optical methods Surface enhanced Raman scattering Gold film Extinction spectroscopy Plasmon Nanoparticle Surface enhanced Raman scattering Water Monolayer Structure effect Gold Multilayer Surface Enhanced Raman Spectrometry Hexane
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Abstract	Using a method of collecting nanoparticles at a water/hexane interface in a close-packed monolayer film and transferring such films onto a solid substrate, three-dimensional multilayer films of nanoparticles were formed. The packed nanoparticles were gold nanospheres (NS) with a 26 nm diameter or gold nanorods (NR) with a 31 nm diameter and 74 nm length. We investigated variations in the surface enhanced Raman scattering (SERS) intensities from such nanoparticle films as the layer compositions were changed. The films stacked with NR layers generated much higher SERS intensity than those of NS layers. The SERS intensities from both kinds of films increased as the number of layers were increased. However, when the NR layer and NS layer were stacked alternately, SERS intensity varied in a zigzag fashion. It was found that the structure of top layer plays a distinguishable role in generating strong SERS enhancement while the lower layers contribute to SERS with less dependency on structures. Interlayer coupling as well as intralayer coupling was considered in order to explain the observations.
AbstractList	Using a method of collecting nanoparticles at a water/hexane interface in a close-packed monolayer film and transferring such films onto a solid substrate, three-dimensional multilayer films of nanoparticles were formed. The packed nanoparticles were gold nanospheres (NS) with a 26 nm diameter or gold nanorods (NR) with a 31 nm diameter and 74 nm length. We investigated variations in the surface enhanced Raman scattering (SERS) intensities from such nanoparticle films as the layer compositions were changed. The films stacked with NR layers generated much higher SERS intensity than those of NS layers. The SERS intensities from both kinds of films increased as the number of layers were increased. However, when the NR layer and NS layer were stacked alternately, SERS intensity varied in a zigzag fashion. It was found that the structure of top layer plays a distinguishable role in generating strong SERS enhancement while the lower layers contribute to SERS with less dependency on structures. Interlayer coupling as well as intralayer coupling was considered in order to explain the observations. Using a method of collecting nanoparticles at a water/hexane interface in a close-packed monolayer film and transferring such films onto a solid substrate, three-dimensional multilayer films of nanoparticles were formed. The packed nanoparticles were gold nanospheres (NS) with a 26 nm diameter or gold nanorods (NR) with a 31 nm diameter and 74 nm length. We investigated variations in the surface enhanced Raman scattering (SERS) intensities from such nanoparticle films as the layer compositions were changed. The films stacked with NR layers generated much higher SERS intensity than those of NS layers. The SERS intensities from both kinds of films increased as the number of layers were increased. However, when the NR layer and NS layer were stacked alternately, SERS intensity varied in a zigzag fashion. It was found that the structure of top layer plays a distinguishable role in generating strong SERS enhancement while the lower layers contribute to SERS with less dependency on structures. Interlayer coupling as well as intralayer coupling was considered in order to explain the observations.
Author	Kim, Seong Kyu Park, Sungho Yun, Sukang Oh, Min Kyung
Author_xml	– sequence: 1 givenname: Min Kyung surname: Oh fullname: Oh, Min Kyung organization: Department of Chemistry, Sungkyunkwan University, Suwon 440-746, Republic of Korea – sequence: 2 givenname: Sukang surname: Yun fullname: Yun, Sukang organization: Department of Chemistry, Sungkyunkwan University, Suwon 440-746, Republic of Korea – sequence: 3 givenname: Seong Kyu surname: Kim fullname: Kim, Seong Kyu email: skkim@skku.edu organization: Department of Chemistry, Sungkyunkwan University, Suwon 440-746, Republic of Korea – sequence: 4 givenname: Sungho surname: Park fullname: Park, Sungho email: spark72@skku.edu organization: Department of Chemistry, Sungkyunkwan University, Suwon 440-746, Republic of Korea
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Keywords	Gold film Extinction spectroscopy Plasmon Nanoparticle Surface enhanced Raman scattering Water Monolayer Structure effect Gold Multilayer Surface Enhanced Raman Spectrometry Hexane
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Snippet	Using a method of collecting nanoparticles at a water/hexane interface in a close-packed monolayer film and transferring such films onto a solid substrate,...
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SubjectTerms	Analytical chemistry Chemistry Exact sciences and technology Extinction spectroscopy Gold film Nanoparticle Plasmon Spectrometric and optical methods Surface enhanced Raman scattering
Title	Effect of layer structures of gold nanoparticle films on surface enhanced Raman scattering
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