Optical and magnetic properties of Mg-doped ZnFe2O4 nanoparticles prepared by rapid microwave combustion method
[Display omitted] •Nano-sized Mg-doped ZnFe2O4 was synthesized by the microwave combustion method.•The as-synthesized samples showed good optical and magnetic properties.•Investigated the effect of Mg-doping on ZnFe2O4 systematically.•Mg concentration increases in ZnFe2O4, the ferromagnetic nature i...
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| Published in | Superlattices and microstructures Vol. 64; pp. 118 - 131 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
01.12.2013
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| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
•Nano-sized Mg-doped ZnFe2O4 was synthesized by the microwave combustion method.•The as-synthesized samples showed good optical and magnetic properties.•Investigated the effect of Mg-doping on ZnFe2O4 systematically.•Mg concentration increases in ZnFe2O4, the ferromagnetic nature increases.
Mg-doped ZnFe2O4 samples were prepared by a microwave combustion method. The obtained samples were characterized by powder X-ray diffraction (XRD), high resolution scanning electron microscopy (HR-SEM), energy dispersive X-ray analysis, UV–Visible diffuse reflectance spectra (DRS), photoluminescence (PL) spectra and vibrating sample magnetometer (VSM). XRD results confirm the formation of cubic spinel-type structure with an average crystallite size in the range of 15–43nm. Lattice parameter decreases with increasing Mg concentration, due to the smaller ionic radius of Mg2+ ion. The HR-SEM images show the morphology of the samples as spherical shaped particles in agglomeration. The broad visible emission band is observed in the entire PL spectrum. The estimated band gap energy is found to decrease with increasing Mg content (2.15–1.42eV). The magnetization showed an increasing trend with increasing Mg concentration (x=0.5), due to the rearrangement of cations at tetrahedral and octahedral sites. |
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| AbstractList | [Display omitted]
•Nano-sized Mg-doped ZnFe2O4 was synthesized by the microwave combustion method.•The as-synthesized samples showed good optical and magnetic properties.•Investigated the effect of Mg-doping on ZnFe2O4 systematically.•Mg concentration increases in ZnFe2O4, the ferromagnetic nature increases.
Mg-doped ZnFe2O4 samples were prepared by a microwave combustion method. The obtained samples were characterized by powder X-ray diffraction (XRD), high resolution scanning electron microscopy (HR-SEM), energy dispersive X-ray analysis, UV–Visible diffuse reflectance spectra (DRS), photoluminescence (PL) spectra and vibrating sample magnetometer (VSM). XRD results confirm the formation of cubic spinel-type structure with an average crystallite size in the range of 15–43nm. Lattice parameter decreases with increasing Mg concentration, due to the smaller ionic radius of Mg2+ ion. The HR-SEM images show the morphology of the samples as spherical shaped particles in agglomeration. The broad visible emission band is observed in the entire PL spectrum. The estimated band gap energy is found to decrease with increasing Mg content (2.15–1.42eV). The magnetization showed an increasing trend with increasing Mg concentration (x=0.5), due to the rearrangement of cations at tetrahedral and octahedral sites. Mg-doped ZnFe2O4 samples were prepared by a microwave combustion method. The obtained samples were characterized by powder X-ray diffraction (XRD), high resolution scanning electron microscopy (HR-SEM), energy dispersive X-ray analysis, UV-Visible diffuse reflectance spectra (DRS), photoluminescence (PL) spectra and vibrating sample magnetometer (VSM). XRD results confirm the formation of cubic spinel-type structure with an average crystallite size in the range of 15-43 nm. Lattice parameter decreases with increasing Mg concentration, due to the smaller ionic radius of Mg2+ ion. The HR-SEM images show the morphology of the samples as spherical shaped particles in agglomeration. The broad visible emission band is observed in the entire PL spectrum. The estimated band gap energy is found to decrease with increasing Mg content (2.15-1.42 eV). The magnetization showed an increasing trend with increasing Mg concentration (x = 0.5), due to the rearrangement of cations at tetrahedral and octahedral sites. |
| Author | Judith Vijaya, J. Meganathan, C. Sundararajan, M. Bououdina, M. Kennedy, L. John Manikandan, A. |
| Author_xml | – sequence: 1 givenname: A. surname: Manikandan fullname: Manikandan, A. organization: Catalysis and Nanomaterials Research Laboratory, Department of Chemistry, Loyola College, Chennai 600 034, India – sequence: 2 givenname: J. surname: Judith Vijaya fullname: Judith Vijaya, J. email: jjvijayaloyola@yahoo.co.in organization: Catalysis and Nanomaterials Research Laboratory, Department of Chemistry, Loyola College, Chennai 600 034, India – sequence: 3 givenname: M. surname: Sundararajan fullname: Sundararajan, M. organization: Materials Division, School of Advanced Sciences, Vellore Institute of Technology University Chennai Campus, Chennai 600 127, India – sequence: 4 givenname: C. surname: Meganathan fullname: Meganathan, C. organization: Catalysis and Nanomaterials Research Laboratory, Department of Chemistry, Loyola College, Chennai 600 034, India – sequence: 5 givenname: L. John surname: Kennedy fullname: Kennedy, L. John organization: Materials Division, School of Advanced Sciences, Vellore Institute of Technology University Chennai Campus, Chennai 600 127, India – sequence: 6 givenname: M. surname: Bououdina fullname: Bououdina, M. organization: Department of Physics, College of Science, University of Bahrain, PO Box 32038, Bahrain |
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•Nano-sized Mg-doped ZnFe2O4 was synthesized by the microwave combustion method.•The as-synthesized samples showed good optical and magnetic... Mg-doped ZnFe2O4 samples were prepared by a microwave combustion method. The obtained samples were characterized by powder X-ray diffraction (XRD), high... |
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| SubjectTerms | Cations Combustion Crystallites Electron microscopy Ferrites Magnesium Magnetic properties Magnetization Microwaves Nanostructures Optical properties Spectra X-ray diffraction X-rays |
| Title | Optical and magnetic properties of Mg-doped ZnFe2O4 nanoparticles prepared by rapid microwave combustion method |
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