A green, efficient, closed-loop direct regeneration technology for reconstructing of the LiNi0.5Co0.2Mn0.3O2 cathode material from spent lithium-ion batteries
Lithium nickel manganese cobalt oxide in the spent lithium ion batteries (LIBs) contains a lot of lithium, nickel, cobalt and manganese. However, how to effectively recover these valuable metals under the premise of reducing environmental pollution is still a challenge. In this work, a green, effici...
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| Published in | Journal of hazardous materials Vol. 410; p. 124610 |
|---|---|
| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
15.05.2021
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| Subjects | |
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| Abstract | Lithium nickel manganese cobalt oxide in the spent lithium ion batteries (LIBs) contains a lot of lithium, nickel, cobalt and manganese. However, how to effectively recover these valuable metals under the premise of reducing environmental pollution is still a challenge. In this work, a green, efficient, closed-loop direct regeneration technology is proposed to reconstruct LiNi0.5Co0.2Mn0.3O2 (NCM523) cathode materials from spent LIBs. Firstly, the failure mechanism of NCM523 cathode materials in the spent LIBs is analyzed deeply. It is found that the spent NCM523 material has problems such as the dissolution of lithium and transition metals, surface interface failure and structural transformation, resulting in serious deterioration of electrochemical performance. Then NCM523 material was directly regenerated by supplementing metal ions, granulation, ion doping and heat treatment. Meanwhile, PO43− polyanions were doped into the regenerated NCM material in the recovery process, showing excellent electrochemical performance with discharge capacity of 189.8 mAh g−1 at 0.1 C. The recovery process proposed in this study puts forward a new strategy for the recovery various lithium nickel cobalt manganese oxide (e.g., LiNi1/3Co1/3Mn1/3O2, LiNi0.5Co0.2Mn0.3O2, LiNi0.6Co0.2Mn0.2O2 and LiNi0.8Co0.1Mn0.1O2) and accelerates the industrialization of spent lithium ion battery recycling.
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•A direct regeneration technology is proposed to reconstruct NCM523 cathode materials from spent LIBs.•The failure behaviors of the LiNi0.5Co0.2Mn0.3O2 of spent LIBs were analyzed in depth.•The specific discharge capacity of the reconstructed RNCMP-2 material is as high as 189.8 mAh g−1 at 0.1 C rate. |
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| AbstractList | Lithium nickel manganese cobalt oxide in the spent lithium ion batteries (LIBs) contains a lot of lithium, nickel, cobalt and manganese. However, how to effectively recover these valuable metals under the premise of reducing environmental pollution is still a challenge. In this work, a green, efficient, closed-loop direct regeneration technology is proposed to reconstruct LiNi0.5Co0.2Mn0.3O2 (NCM523) cathode materials from spent LIBs. Firstly, the failure mechanism of NCM523 cathode materials in the spent LIBs is analyzed deeply. It is found that the spent NCM523 material has problems such as the dissolution of lithium and transition metals, surface interface failure and structural transformation, resulting in serious deterioration of electrochemical performance. Then NCM523 material was directly regenerated by supplementing metal ions, granulation, ion doping and heat treatment. Meanwhile, PO43− polyanions were doped into the regenerated NCM material in the recovery process, showing excellent electrochemical performance with discharge capacity of 189.8 mAh g−1 at 0.1 C. The recovery process proposed in this study puts forward a new strategy for the recovery various lithium nickel cobalt manganese oxide (e.g., LiNi1/3Co1/3Mn1/3O2, LiNi0.5Co0.2Mn0.3O2, LiNi0.6Co0.2Mn0.2O2 and LiNi0.8Co0.1Mn0.1O2) and accelerates the industrialization of spent lithium ion battery recycling.
[Display omitted]
•A direct regeneration technology is proposed to reconstruct NCM523 cathode materials from spent LIBs.•The failure behaviors of the LiNi0.5Co0.2Mn0.3O2 of spent LIBs were analyzed in depth.•The specific discharge capacity of the reconstructed RNCMP-2 material is as high as 189.8 mAh g−1 at 0.1 C rate. Lithium nickel manganese cobalt oxide in the spent lithium ion batteries (LIBs) contains a lot of lithium, nickel, cobalt and manganese. However, how to effectively recover these valuable metals under the premise of reducing environmental pollution is still a challenge. In this work, a green, efficient, closed-loop direct regeneration technology is proposed to reconstruct LiNi₀.₅Co₀.₂Mn₀.₃O₂ (NCM523) cathode materials from spent LIBs. Firstly, the failure mechanism of NCM523 cathode materials in the spent LIBs is analyzed deeply. It is found that the spent NCM523 material has problems such as the dissolution of lithium and transition metals, surface interface failure and structural transformation, resulting in serious deterioration of electrochemical performance. Then NCM523 material was directly regenerated by supplementing metal ions, granulation, ion doping and heat treatment. Meanwhile, PO₄³⁻ polyanions were doped into the regenerated NCM material in the recovery process, showing excellent electrochemical performance with discharge capacity of 189.8 mAh g⁻¹ at 0.1 C. The recovery process proposed in this study puts forward a new strategy for the recovery various lithium nickel cobalt manganese oxide (e.g., LiNi₁/₃Co₁/₃Mn₁/₃O₂, LiNi₀.₅Co₀.₂Mn₀.₃O₂, LiNi₀.₆Co₀.₂Mn₀.₂O₂ and LiNi₀.₈Co₀.₁Mn₀.₁O₂) and accelerates the industrialization of spent lithium ion battery recycling. Lithium nickel manganese cobalt oxide in the spent lithium ion batteries (LIBs) contains a lot of lithium, nickel, cobalt and manganese. However, how to effectively recover these valuable metals under the premise of reducing environmental pollution is still a challenge. In this work, a green, efficient, closed-loop direct regeneration technology is proposed to reconstruct LiNi0.5Co0.2Mn0.3O2 (NCM523) cathode materials from spent LIBs. Firstly, the failure mechanism of NCM523 cathode materials in the spent LIBs is analyzed deeply. It is found that the spent NCM523 material has problems such as the dissolution of lithium and transition metals, surface interface failure and structural transformation, resulting in serious deterioration of electrochemical performance. Then NCM523 material was directly regenerated by supplementing metal ions, granulation, ion doping and heat treatment. Meanwhile, PO43- polyanions were doped into the regenerated NCM material in the recovery process, showing excellent electrochemical performance with discharge capacity of 189.8 mAh g-1 at 0.1 C. The recovery process proposed in this study puts forward a new strategy for the recovery various lithium nickel cobalt manganese oxide (e.g., LiNi1/3Co1/3Mn1/3O2, LiNi0.5Co0.2Mn0.3O2, LiNi0.6Co0.2Mn0.2O2 and LiNi0.8Co0.1Mn0.1O2) and accelerates the industrialization of spent lithium ion battery recycling.Lithium nickel manganese cobalt oxide in the spent lithium ion batteries (LIBs) contains a lot of lithium, nickel, cobalt and manganese. However, how to effectively recover these valuable metals under the premise of reducing environmental pollution is still a challenge. In this work, a green, efficient, closed-loop direct regeneration technology is proposed to reconstruct LiNi0.5Co0.2Mn0.3O2 (NCM523) cathode materials from spent LIBs. Firstly, the failure mechanism of NCM523 cathode materials in the spent LIBs is analyzed deeply. It is found that the spent NCM523 material has problems such as the dissolution of lithium and transition metals, surface interface failure and structural transformation, resulting in serious deterioration of electrochemical performance. Then NCM523 material was directly regenerated by supplementing metal ions, granulation, ion doping and heat treatment. Meanwhile, PO43- polyanions were doped into the regenerated NCM material in the recovery process, showing excellent electrochemical performance with discharge capacity of 189.8 mAh g-1 at 0.1 C. The recovery process proposed in this study puts forward a new strategy for the recovery various lithium nickel cobalt manganese oxide (e.g., LiNi1/3Co1/3Mn1/3O2, LiNi0.5Co0.2Mn0.3O2, LiNi0.6Co0.2Mn0.2O2 and LiNi0.8Co0.1Mn0.1O2) and accelerates the industrialization of spent lithium ion battery recycling. |
| ArticleNumber | 124610 |
| Author | Li, Yahao Pan, Qichang Li, Yu Wang, Hongqiang Li, Qingyu Huang, Youguo Zheng, Fenghua Fan, Xiaoping Tan, Chunlei Chen, Zhiqiang |
| Author_xml | – sequence: 1 givenname: Xiaoping surname: Fan fullname: Fan, Xiaoping organization: Guangxi Key Laboratory of Low Carbon Energy Materials, School of Chemical and Pharmaceutical Science, Guangxi Normal University, Guilin 541004, China – sequence: 2 givenname: Chunlei surname: Tan fullname: Tan, Chunlei organization: Guangxi Key Laboratory of Low Carbon Energy Materials, School of Chemical and Pharmaceutical Science, Guangxi Normal University, Guilin 541004, China – sequence: 3 givenname: Yu surname: Li fullname: Li, Yu organization: Guangxi Key Laboratory of Low Carbon Energy Materials, School of Chemical and Pharmaceutical Science, Guangxi Normal University, Guilin 541004, China – sequence: 4 givenname: Zhiqiang surname: Chen fullname: Chen, Zhiqiang organization: Guangxi Key Laboratory of Low Carbon Energy Materials, School of Chemical and Pharmaceutical Science, Guangxi Normal University, Guilin 541004, China – sequence: 5 givenname: Yahao surname: Li fullname: Li, Yahao email: liyahao66@126.com organization: State Key Laboratory of Silicon Materials, Key Laboratory of Advanced Materials and Applications for Batteries of Zhejiang Province, and Department of Materials Science and Engineering, Zhejiang University, Hangzhou 310027, China – sequence: 6 givenname: Youguo surname: Huang fullname: Huang, Youguo organization: Guangxi Key Laboratory of Low Carbon Energy Materials, School of Chemical and Pharmaceutical Science, Guangxi Normal University, Guilin 541004, China – sequence: 7 givenname: Qichang surname: Pan fullname: Pan, Qichang organization: Guangxi Key Laboratory of Low Carbon Energy Materials, School of Chemical and Pharmaceutical Science, Guangxi Normal University, Guilin 541004, China – sequence: 8 givenname: Fenghua surname: Zheng fullname: Zheng, Fenghua email: zhengfh870627@163.com organization: Guangxi Key Laboratory of Low Carbon Energy Materials, School of Chemical and Pharmaceutical Science, Guangxi Normal University, Guilin 541004, China – sequence: 9 givenname: Hongqiang surname: Wang fullname: Wang, Hongqiang organization: Guangxi Key Laboratory of Low Carbon Energy Materials, School of Chemical and Pharmaceutical Science, Guangxi Normal University, Guilin 541004, China – sequence: 10 givenname: Qingyu surname: Li fullname: Li, Qingyu organization: Guangxi Key Laboratory of Low Carbon Energy Materials, School of Chemical and Pharmaceutical Science, Guangxi Normal University, Guilin 541004, China |
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| Snippet | Lithium nickel manganese cobalt oxide in the spent lithium ion batteries (LIBs) contains a lot of lithium, nickel, cobalt and manganese. However, how to... |
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| SubjectTerms | Cathode material cathodes cobalt cobalt oxide electrochemistry heat treatment industrialization LiNi0.5Co0.2Mn0.3O2 lithium lithium batteries manganese manganese monoxide nickel pollution Reconstructing Regeneration technology Spent lithium-ion batteries |
| Title | A green, efficient, closed-loop direct regeneration technology for reconstructing of the LiNi0.5Co0.2Mn0.3O2 cathode material from spent lithium-ion batteries |
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