Preparation of ZrO2 whiskers through high pressure and high temperature method
ZrO2 whiskers have been successfully synthesized at temperature of 1800 °C and high pressure of 15 GPa, using ZrO2 powder as the starting material. After a high pressure and high temperature (HPHT) process, a bunch of long and idiomorphic ZrO2 whiskers are obtained. The grown whiskers look like need...
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| Published in | Solid state sciences Vol. 41; pp. 52 - 55 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier Masson SAS
01.03.2015
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| Abstract | ZrO2 whiskers have been successfully synthesized at temperature of 1800 °C and high pressure of 15 GPa, using ZrO2 powder as the starting material. After a high pressure and high temperature (HPHT) process, a bunch of long and idiomorphic ZrO2 whiskers are obtained. The grown whiskers look like needles, and have silky luster. They are colorless and transparent, and exhibit hexagonal, triangular, quadrilateral, and irregular shaped cross sections. Through this HPHT method, whiskers with various diameters from 10 to 20 μm, and length from 200 to 1000 μm can be produced. The aspect ratio of length to diameter can be from 10 to 100. Growth mechanism of the ZrO2 whiskers prepared under HPHT conditions are discussed, and the ZrO2 whiskers growth may undergo a vapor–solid process.
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•ZrO2 whiskers are synthesized at 15 GPa, 1800 °C.•As-prepared ZrO2 whiskers are colorless and transparent.•They exhibited some regular and irregular shaped cross sections.•The aspect ratio of ZrO2 whiskers could be from 10 to 100. |
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| AbstractList | ZrO2 whiskers have been successfully synthesized at temperature of 1800 degree C and high pressure of 15 GPa, using ZrO2 powder as the starting material. After a high pressure and high temperature (HPHT) process, a bunch of long and idiomorphic ZrO2 whiskers are obtained. The grown whiskers look like needles, and have silky luster. They are colorless and transparent, and exhibit hexagonal, triangular, quadrilateral, and irregular shaped cross sections. Through this HPHT method, whiskers with various diameters from 10 to 20 mu m, and length from 200 to 1000 mu m can be produced. The aspect ratio of length to diameter can be from 10 to 100. Growth mechanism of the ZrO2 whiskers prepared under HPHT conditions are discussed, and the ZrO2 whiskers growth may undergo a vapor-solid process. ZrO2 whiskers have been successfully synthesized at temperature of 1800 °C and high pressure of 15 GPa, using ZrO2 powder as the starting material. After a high pressure and high temperature (HPHT) process, a bunch of long and idiomorphic ZrO2 whiskers are obtained. The grown whiskers look like needles, and have silky luster. They are colorless and transparent, and exhibit hexagonal, triangular, quadrilateral, and irregular shaped cross sections. Through this HPHT method, whiskers with various diameters from 10 to 20 μm, and length from 200 to 1000 μm can be produced. The aspect ratio of length to diameter can be from 10 to 100. Growth mechanism of the ZrO2 whiskers prepared under HPHT conditions are discussed, and the ZrO2 whiskers growth may undergo a vapor–solid process. [Display omitted] •ZrO2 whiskers are synthesized at 15 GPa, 1800 °C.•As-prepared ZrO2 whiskers are colorless and transparent.•They exhibited some regular and irregular shaped cross sections.•The aspect ratio of ZrO2 whiskers could be from 10 to 100. |
| Author | He, Duanwei Wang, Haikuo Liu, Chunmei Wang, Qiming Wang, Wendan Xu, Chao Wang, Pei |
| Author_xml | – sequence: 1 givenname: Chao surname: Xu fullname: Xu, Chao organization: Institute of Atomic and Molecular Physics, Sichuan University, Chengdu 610065, China – sequence: 2 givenname: Duanwei surname: He fullname: He, Duanwei email: duanweihe@scu.edu.cn organization: Institute of Atomic and Molecular Physics, Sichuan University, Chengdu 610065, China – sequence: 3 givenname: Chunmei surname: Liu fullname: Liu, Chunmei organization: College of Physical Science and Technology, Sichuan University, Chengdu 610064, China – sequence: 4 givenname: Haikuo surname: Wang fullname: Wang, Haikuo organization: Institute of Atomic and Molecular Physics, Sichuan University, Chengdu 610065, China – sequence: 5 givenname: Pei surname: Wang fullname: Wang, Pei organization: Institute of Atomic and Molecular Physics, Sichuan University, Chengdu 610065, China – sequence: 6 givenname: Qiming surname: Wang fullname: Wang, Qiming organization: Institute of Atomic and Molecular Physics, Sichuan University, Chengdu 610065, China – sequence: 7 givenname: Wendan surname: Wang fullname: Wang, Wendan organization: Institute of Atomic and Molecular Physics, Sichuan University, Chengdu 610065, China |
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| CitedBy_id | crossref_primary_10_3390_nano13010037 crossref_primary_10_1016_j_ceramint_2018_11_135 crossref_primary_10_1016_j_apt_2021_02_006 crossref_primary_10_1016_j_vacuum_2021_110336 crossref_primary_10_1016_j_ceramint_2021_04_263 crossref_primary_10_1111_ijac_12827 crossref_primary_10_1016_j_matdes_2019_107844 crossref_primary_10_1016_j_jcrysgro_2016_12_033 crossref_primary_10_1039_D1CE01544C crossref_primary_10_1007_s12034_024_03210_7 crossref_primary_10_1016_j_jmat_2020_12_004 crossref_primary_10_1063_1_5140856 crossref_primary_10_1016_j_jmrt_2024_07_155 crossref_primary_10_1016_j_matchemphys_2020_123450 crossref_primary_10_1016_j_jmrt_2023_04_229 |
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| Snippet | ZrO2 whiskers have been successfully synthesized at temperature of 1800 °C and high pressure of 15 GPa, using ZrO2 powder as the starting material. After a... ZrO2 whiskers have been successfully synthesized at temperature of 1800 degree C and high pressure of 15 GPa, using ZrO2 powder as the starting material. After... |
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| SubjectTerms | Aspect ratio Cross sections High pressure and high temperature Luster Needles Quadrilaterals Scanning electron microscope Solid state Whiskers Zirconium dioxide ZrO2 |
| Title | Preparation of ZrO2 whiskers through high pressure and high temperature method |
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