Three-dimensional measurement of elemental distribution in minute samples by combination of in-air micro-PIXE and STIM
A technique of measuring three-dimensional (3D) distribution of trace elements in a minute sample was studied using the in-air micro-PIXE (Particle Induced X-ray Emission) system. A 3D distribution was acquired by means of reconstructing numbers of projection images of the sample obtained by micro-P...
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| Published in | Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms Vol. 267; no. 12; pp. 2125 - 2127 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
15.06.2009
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0168-583X 1872-9584 |
| DOI | 10.1016/j.nimb.2009.03.067 |
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| Abstract | A technique of measuring three-dimensional (3D) distribution of trace elements in a minute sample was studied using the in-air micro-PIXE (Particle Induced X-ray Emission) system. A 3D distribution was acquired by means of reconstructing numbers of projection images of the sample obtained by micro-PIXE analyses from different directions. This is basically the same technique as X-ray CT (Computed Tomography). However, when this technique was applied to the in-air micro-PIXE analysis, the X-ray yields should be corrected in taking account of such parameters as the X-ray production cross section, the X-ray attenuation coefficient, the energy of an incident particle, and the 3D densities of major elements in the analysis sample. In this study, STIM (Scanning Transmission Ion Microscopy)-CT was used to obtain the 3D density map of the sample. Corrected 3D distributions of sulfur and iron in a minute test sample were successfully measured with this technique in combination of STIM-CT and in-air micro-PIXE. |
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| AbstractList | A technique of measuring three-dimensional (3D) distribution of trace elements in a minute sample was studied using the in-air micro-PIXE (Particle Induced X-ray Emission) system. A 3D distribution was acquired by means of reconstructing numbers of projection images of the sample obtained by micro-PIXE analyses from different directions. This is basically the same technique as X-ray CT (Computed Tomography). However, when this technique was applied to the in-air micro-PIXE analysis, the X-ray yields should be corrected in taking account of such parameters as the X-ray production cross section, the X-ray attenuation coefficient, the energy of an incident particle, and the 3D densities of major elements in the analysis sample. In this study, STIM (Scanning Transmission Ion Microscopy)-CT was used to obtain the 3D density map of the sample. Corrected 3D distributions of sulfur and iron in a minute test sample were successfully measured with this technique in combination of STIM-CT and in-air micro-PIXE. |
| Author | Satoh, T. Oikawa, M. Kamiya, T. |
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