Gold()-doped films: new routes for efficient room temperature phosphorescent materials
The synthesis of four novel gold( i )-phosphane complexes coordinated to 9-phenanthrene chromophore has been carried out through the reaction of 9-phenanthreneboronic acid and the corresponding AuClPR 3 (PR 3 = PPh 3 for triphenylphosphane ( 1a ); 1,4-bis(diphenylphosphanyl)butane or dppb ( 2b ); bi...
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| Published in | Dalton transactions : an international journal of inorganic chemistry Vol. 5; no. 11; pp. 386 - 3815 |
|---|---|
| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
England
Royal Society of Chemistry
21.03.2021
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| Subjects | |
| Online Access | Get full text |
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| Abstract | The synthesis of four novel gold(
i
)-phosphane complexes coordinated to 9-phenanthrene chromophore has been carried out through the reaction of 9-phenanthreneboronic acid and the corresponding AuClPR
3
(PR
3
= PPh
3
for triphenylphosphane (
1a
); 1,4-bis(diphenylphosphanyl)butane or dppb (
2b
); bis(diphenylphosphanyl)acetylene or dppa (
2c
); (AuCl)
2
(diphos) (diphos = bis(diphenylphosphanyl)methane or dppm (
3
)) sources. The X-ray crystal structures of compounds
1a
and
2b
show the existence of MOF-like intermolecular assemblies that contain empty inner cavities in the absence of aurophilic contacts. In contrast, the formation of a tetranuclear complex with intramolecular aurophilic interactions was evidenced for
3
. Photophysical characterization indicates dual emission in all gold(
i
) complexes when oxygen is removed from the sample, while only fluorescence emission is recorded for the uncoordinated ligand. The introduction of the compounds within PMMA and Zeonex was assayed, and luminescent films containing gold(
i
) complexes where phosphorescence is the sole pathway for emission are obtained, instead of the dual emission (with significant fluorescence contribution) recorded in solution.
The synthesis of four novel gold(
i
)-phosphane complexes coordinated to 9-phenanthrene has been carried out and their inclusion within organic matrixes showed the formation of new pure room temperature phosphorescence materials. |
|---|---|
| AbstractList | The synthesis of four novel gold(
i
)-phosphane complexes coordinated to 9-phenanthrene chromophore has been carried out through the reaction of 9-phenanthreneboronic acid and the corresponding AuClPR
3
(PR
3
= PPh
3
for triphenylphosphane (
1a
); 1,4-bis(diphenylphosphanyl)butane or dppb (
2b
); bis(diphenylphosphanyl)acetylene or dppa (
2c
); (AuCl)
2
(diphos) (diphos = bis(diphenylphosphanyl)methane or dppm (
3
)) sources. The X-ray crystal structures of compounds
1a
and
2b
show the existence of MOF-like intermolecular assemblies that contain empty inner cavities in the absence of aurophilic contacts. In contrast, the formation of a tetranuclear complex with intramolecular aurophilic interactions was evidenced for
3
. Photophysical characterization indicates dual emission in all gold(
i
) complexes when oxygen is removed from the sample, while only fluorescence emission is recorded for the uncoordinated ligand. The introduction of the compounds within PMMA and Zeonex was assayed, and luminescent films containing gold(
i
) complexes where phosphorescence is the sole pathway for emission are obtained, instead of the dual emission (with significant fluorescence contribution) recorded in solution.
The synthesis of four novel gold(
i
)-phosphane complexes coordinated to 9-phenanthrene has been carried out and their inclusion within organic matrixes showed the formation of new pure room temperature phosphorescence materials. The synthesis of four novel gold( i )-phosphane complexes coordinated to 9-phenanthrene chromophore has been carried out through the reaction of 9-phenanthreneboronic acid and the corresponding AuClPR 3 (PR 3 = PPh 3 for triphenylphosphane ( 1a ); 1,4-bis(diphenylphosphanyl)butane or dppb ( 2b ); bis(diphenylphosphanyl)acetylene or dppa ( 2c ); (AuCl) 2 (diphos) (diphos = bis(diphenylphosphanyl)methane or dppm ( 3 )) sources. The X-ray crystal structures of compounds 1a and 2b show the existence of MOF-like intermolecular assemblies that contain empty inner cavities in the absence of aurophilic contacts. In contrast, the formation of a tetranuclear complex with intramolecular aurophilic interactions was evidenced for 3 . Photophysical characterization indicates dual emission in all gold( i ) complexes when oxygen is removed from the sample, while only fluorescence emission is recorded for the uncoordinated ligand. The introduction of the compounds within PMMA and Zeonex was assayed, and luminescent films containing gold( i ) complexes where phosphorescence is the sole pathway for emission are obtained, instead of the dual emission (with significant fluorescence contribution) recorded in solution. The synthesis of four novel gold(i)-phosphane complexes coordinated to 9-phenanthrene chromophore has been carried out through the reaction of 9-phenanthreneboronic acid and the corresponding AuClPR3 (PR3 = PPh3 for triphenylphosphane (1a); 1,4-bis(diphenylphosphanyl)butane or dppb (2b); bis(diphenylphosphanyl)acetylene or dppa (2c); (AuCl)2(diphos) (diphos = bis(diphenylphosphanyl)methane or dppm (3)) sources. The X-ray crystal structures of compounds 1a and 2b show the existence of MOF-like intermolecular assemblies that contain empty inner cavities in the absence of aurophilic contacts. In contrast, the formation of a tetranuclear complex with intramolecular aurophilic interactions was evidenced for 3. Photophysical characterization indicates dual emission in all gold(i) complexes when oxygen is removed from the sample, while only fluorescence emission is recorded for the uncoordinated ligand. The introduction of the compounds within PMMA and Zeonex was assayed, and luminescent films containing gold(i) complexes where phosphorescence is the sole pathway for emission are obtained, instead of the dual emission (with significant fluorescence contribution) recorded in solution. The synthesis of four novel gold(i)-phosphane complexes coordinated to 9-phenanthrene chromophore has been carried out through the reaction of 9-phenanthreneboronic acid and the corresponding AuClPR (PR = PPh for triphenylphosphane (1a); 1,4-bis(diphenylphosphanyl)butane or dppb (2b); bis(diphenylphosphanyl)acetylene or dppa (2c); (AuCl) (diphos) (diphos = bis(diphenylphosphanyl)methane or dppm (3)) sources. The X-ray crystal structures of compounds 1a and 2b show the existence of MOF-like intermolecular assemblies that contain empty inner cavities in the absence of aurophilic contacts. In contrast, the formation of a tetranuclear complex with intramolecular aurophilic interactions was evidenced for 3. Photophysical characterization indicates dual emission in all gold(i) complexes when oxygen is removed from the sample, while only fluorescence emission is recorded for the uncoordinated ligand. The introduction of the compounds within PMMA and Zeonex was assayed, and luminescent films containing gold(i) complexes where phosphorescence is the sole pathway for emission are obtained, instead of the dual emission (with significant fluorescence contribution) recorded in solution. |
| Author | Choi, Hyeonho Rissanen, Kari Jung, Yongsik de Aquino, Araceli Lima, João Carlos Ferrer, Montserrat Caparrós, Francisco J Truong, Khai-Nghi Rodríguez, Laura |
| AuthorAffiliation | Department of Chemistry Departament de Química Inorgànica i Orgànica. Secció de Química Inorgànica LAQV-REQUIMTE Universidade Nova de Lisboa University of Jyvaskyla Universitat de Barcelona Institut de Nanociència i Nanotecnologia (IN2UB). Universitat de Barcelona Departamento de Química Samsung Advanced Institute of Technology Samsung Electronics Co. Ltd |
| AuthorAffiliation_xml | – name: Departament de Química Inorgànica i Orgànica. Secció de Química Inorgànica – name: Universitat de Barcelona – name: Institut de Nanociència i Nanotecnologia (IN2UB). Universitat de Barcelona – name: Department of Chemistry – name: Samsung Advanced Institute of Technology – name: LAQV-REQUIMTE – name: Samsung Electronics Co. Ltd – name: Universidade Nova de Lisboa – name: University of Jyvaskyla – name: Departamento de Química |
| Author_xml | – sequence: 1 givenname: Araceli surname: de Aquino fullname: de Aquino, Araceli – sequence: 2 givenname: Francisco J surname: Caparrós fullname: Caparrós, Francisco J – sequence: 3 givenname: Khai-Nghi surname: Truong fullname: Truong, Khai-Nghi – sequence: 4 givenname: Kari surname: Rissanen fullname: Rissanen, Kari – sequence: 5 givenname: Montserrat surname: Ferrer fullname: Ferrer, Montserrat – sequence: 6 givenname: Yongsik surname: Jung fullname: Jung, Yongsik – sequence: 7 givenname: Hyeonho surname: Choi fullname: Choi, Hyeonho – sequence: 8 givenname: João Carlos surname: Lima fullname: Lima, João Carlos – sequence: 9 givenname: Laura surname: Rodríguez fullname: Rodríguez, Laura |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/33704345$$D View this record in MEDLINE/PubMed |
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| Snippet | The synthesis of four novel gold(
i
)-phosphane complexes coordinated to 9-phenanthrene chromophore has been carried out through the reaction of... The synthesis of four novel gold(i)-phosphane complexes coordinated to 9-phenanthrene chromophore has been carried out through the reaction of... |
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| SubjectTerms | Acetylene Chromophores Crystal structure Crystallography Doped films Emission Fluorescence Gold Phenanthrene Phosphorescence Room temperature |
| Title | Gold()-doped films: new routes for efficient room temperature phosphorescent materials |
| URI | https://www.ncbi.nlm.nih.gov/pubmed/33704345 https://www.proquest.com/docview/2503620474/abstract/ https://search.proquest.com/docview/2500374640 |
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