A novel positively charged composite nanofiltration membrane based on polyethyleneimine with a tunable active layer structure developed via interfacial polymerization
A novel positively charged composite nanofiltration (NF) membrane with tunable active layer structure was successfully developed via interfacial polymerization on a polysulfone (PSF) ultrafiltration (UF) membrane surface, using polyethyleneimine (PEI) as the monomer of the aqueous phase, and a mixtu...
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| Published in | RSC advances Vol. 9; no. 19; pp. 10796 - 10806 |
|---|---|
| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
England
Royal Society of Chemistry
08.04.2019
The Royal Society of Chemistry |
| Subjects | |
| Online Access | Get full text |
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| Abstract | A novel positively charged composite nanofiltration (NF) membrane with tunable active layer structure was successfully developed
via
interfacial polymerization on a polysulfone (PSF) ultrafiltration (UF) membrane surface, using polyethyleneimine (PEI) as the monomer of the aqueous phase, and a mixture of isophthaloyl dichloride (IPC) and tri-mesoyl chloride (TMC) as the monomer of the organic phase. Interestingly, a synergetic effect of the mass ratio of IPC and TMC was observed on the pore size and the structure of the active layer of the resultant polyamide (PA)/polysulfone (PSF) composite NF membrane. The rejection (
R
) to the inorganic electrolytes increased with the mass ratio of IPC to TMC, while the permeate flux (
F
) escalated up to a 1 : 1 mixing ratio of IPC to TMC and dropped at higher mixing ratios. The rejection to different inorganic electrolytes decreased in the order of ZnCl
2
, MgCl
2
, CaCl
2
, CuCl
2
, MgSO
4
, NaCl, and Na
2
SO
4
. At ambient temperature and 0.4 MPa, the optimized membrane demonstrated
R
and
F
to 1 g L
−1
MgCl
2
aqueous solution as 98.1% and 27.6 L m
−2
h
−1
, respectively. Its rejection to various dyes reduced significantly in the order of cationic red X-GTL (100%), rhodamine B (94.2%), cationic gold yellow X-GL (93.5%), and brilliant blue KN-R (43.9%), in agreement with the decrease in the molecular weight (
M
w
) and the overall charges of the dye. |
|---|---|
| AbstractList | A novel positively charged composite nanofiltration (NF) membrane with tunable active layer structure was successfully developed via interfacial polymerization on a polysulfone (PSF) ultrafiltration (UF) membrane surface, using polyethyleneimine (PEI) as the monomer of the aqueous phase, and a mixture of isophthaloyl dichloride (IPC) and tri-mesoyl chloride (TMC) as the monomer of the organic phase. Interestingly, a synergetic effect of the mass ratio of IPC and TMC was observed on the pore size and the structure of the active layer of the resultant polyamide (PA)/polysulfone (PSF) composite NF membrane. The rejection (R) to the inorganic electrolytes increased with the mass ratio of IPC to TMC, while the permeate flux (F) escalated up to a 1 : 1 mixing ratio of IPC to TMC and dropped at higher mixing ratios. The rejection to different inorganic electrolytes decreased in the order of ZnCl2, MgCl2, CaCl2, CuCl2, MgSO4, NaCl, and Na2SO4. At ambient temperature and 0.4 MPa, the optimized membrane demonstrated R and F to 1 g L-1 MgCl2 aqueous solution as 98.1% and 27.6 L m-2 h-1, respectively. Its rejection to various dyes reduced significantly in the order of cationic red X-GTL (100%), rhodamine B (94.2%), cationic gold yellow X-GL (93.5%), and brilliant blue KN-R (43.9%), in agreement with the decrease in the molecular weight (M w) and the overall charges of the dye.A novel positively charged composite nanofiltration (NF) membrane with tunable active layer structure was successfully developed via interfacial polymerization on a polysulfone (PSF) ultrafiltration (UF) membrane surface, using polyethyleneimine (PEI) as the monomer of the aqueous phase, and a mixture of isophthaloyl dichloride (IPC) and tri-mesoyl chloride (TMC) as the monomer of the organic phase. Interestingly, a synergetic effect of the mass ratio of IPC and TMC was observed on the pore size and the structure of the active layer of the resultant polyamide (PA)/polysulfone (PSF) composite NF membrane. The rejection (R) to the inorganic electrolytes increased with the mass ratio of IPC to TMC, while the permeate flux (F) escalated up to a 1 : 1 mixing ratio of IPC to TMC and dropped at higher mixing ratios. The rejection to different inorganic electrolytes decreased in the order of ZnCl2, MgCl2, CaCl2, CuCl2, MgSO4, NaCl, and Na2SO4. At ambient temperature and 0.4 MPa, the optimized membrane demonstrated R and F to 1 g L-1 MgCl2 aqueous solution as 98.1% and 27.6 L m-2 h-1, respectively. Its rejection to various dyes reduced significantly in the order of cationic red X-GTL (100%), rhodamine B (94.2%), cationic gold yellow X-GL (93.5%), and brilliant blue KN-R (43.9%), in agreement with the decrease in the molecular weight (M w) and the overall charges of the dye. A novel positively charged composite nanofiltration (NF) membrane with tunable active layer structure was successfully developed interfacial polymerization on a polysulfone (PSF) ultrafiltration (UF) membrane surface, using polyethyleneimine (PEI) as the monomer of the aqueous phase, and a mixture of isophthaloyl dichloride (IPC) and tri-mesoyl chloride (TMC) as the monomer of the organic phase. Interestingly, a synergetic effect of the mass ratio of IPC and TMC was observed on the pore size and the structure of the active layer of the resultant polyamide (PA)/polysulfone (PSF) composite NF membrane. The rejection ( ) to the inorganic electrolytes increased with the mass ratio of IPC to TMC, while the permeate flux ( ) escalated up to a 1 : 1 mixing ratio of IPC to TMC and dropped at higher mixing ratios. The rejection to different inorganic electrolytes decreased in the order of ZnCl , MgCl , CaCl , CuCl , MgSO , NaCl, and Na SO . At ambient temperature and 0.4 MPa, the optimized membrane demonstrated and to 1 g L MgCl aqueous solution as 98.1% and 27.6 L m h , respectively. Its rejection to various dyes reduced significantly in the order of cationic red X-GTL (100%), rhodamine B (94.2%), cationic gold yellow X-GL (93.5%), and brilliant blue KN-R (43.9%), in agreement with the decrease in the molecular weight ( ) and the overall charges of the dye. A novel positively charged composite nanofiltration (NF) membrane with tunable active layer structure was successfully developed via interfacial polymerization on a polysulfone (PSF) ultrafiltration (UF) membrane surface, using polyethyleneimine (PEI) as the monomer of the aqueous phase, and a mixture of isophthaloyl dichloride (IPC) and tri-mesoyl chloride (TMC) as the monomer of the organic phase. Interestingly, a synergetic effect of the mass ratio of IPC and TMC was observed on the pore size and the structure of the active layer of the resultant polyamide (PA)/polysulfone (PSF) composite NF membrane. The rejection (R) to the inorganic electrolytes increased with the mass ratio of IPC to TMC, while the permeate flux (F) escalated up to a 1 : 1 mixing ratio of IPC to TMC and dropped at higher mixing ratios. The rejection to different inorganic electrolytes decreased in the order of ZnCl₂, MgCl₂, CaCl₂, CuCl₂, MgSO₄, NaCl, and Na₂SO₄. At ambient temperature and 0.4 MPa, the optimized membrane demonstrated R and F to 1 g L⁻¹ MgCl₂ aqueous solution as 98.1% and 27.6 L m⁻² h⁻¹, respectively. Its rejection to various dyes reduced significantly in the order of cationic red X-GTL (100%), rhodamine B (94.2%), cationic gold yellow X-GL (93.5%), and brilliant blue KN-R (43.9%), in agreement with the decrease in the molecular weight (Mw) and the overall charges of the dye. A novel positively charged composite nanofiltration (NF) membrane with tunable active layer structure was successfully developed via interfacial polymerization on a polysulfone (PSF) ultrafiltration (UF) membrane surface, using polyethyleneimine (PEI) as the monomer of the aqueous phase, and a mixture of isophthaloyl dichloride (IPC) and tri-mesoyl chloride (TMC) as the monomer of the organic phase. Interestingly, a synergetic effect of the mass ratio of IPC and TMC was observed on the pore size and the structure of the active layer of the resultant polyamide (PA)/polysulfone (PSF) composite NF membrane. The rejection ( R ) to the inorganic electrolytes increased with the mass ratio of IPC to TMC, while the permeate flux ( F ) escalated up to a 1 : 1 mixing ratio of IPC to TMC and dropped at higher mixing ratios. The rejection to different inorganic electrolytes decreased in the order of ZnCl 2 , MgCl 2 , CaCl 2 , CuCl 2 , MgSO 4 , NaCl, and Na 2 SO 4 . At ambient temperature and 0.4 MPa, the optimized membrane demonstrated R and F to 1 g L −1 MgCl 2 aqueous solution as 98.1% and 27.6 L m −2 h −1 , respectively. Its rejection to various dyes reduced significantly in the order of cationic red X-GTL (100%), rhodamine B (94.2%), cationic gold yellow X-GL (93.5%), and brilliant blue KN-R (43.9%), in agreement with the decrease in the molecular weight ( M w ) and the overall charges of the dye. A novel positively charged composite nanofiltration (NF) membrane with tunable active layer structure was successfully developed via interfacial polymerization on a polysulfone (PSF) ultrafiltration (UF) membrane surface, using polyethyleneimine (PEI) as the monomer of the aqueous phase, and a mixture of isophthaloyl dichloride (IPC) and tri-mesoyl chloride (TMC) as the monomer of the organic phase. Interestingly, a synergetic effect of the mass ratio of IPC and TMC was observed on the pore size and the structure of the active layer of the resultant polyamide (PA)/polysulfone (PSF) composite NF membrane. The rejection (R) to the inorganic electrolytes increased with the mass ratio of IPC to TMC, while the permeate flux (F) escalated up to a 1 : 1 mixing ratio of IPC to TMC and dropped at higher mixing ratios. The rejection to different inorganic electrolytes decreased in the order of ZnCl2, MgCl2, CaCl2, CuCl2, MgSO4, NaCl, and Na2SO4. At ambient temperature and 0.4 MPa, the optimized membrane demonstrated R and F to 1 g L−1 MgCl2 aqueous solution as 98.1% and 27.6 L m−2 h−1, respectively. Its rejection to various dyes reduced significantly in the order of cationic red X-GTL (100%), rhodamine B (94.2%), cationic gold yellow X-GL (93.5%), and brilliant blue KN-R (43.9%), in agreement with the decrease in the molecular weight (Mw) and the overall charges of the dye. A novel positively charged composite nanofiltration (NF) membrane with tunable active layer structure was successfully developed via interfacial polymerization on a polysulfone (PSF) ultrafiltration (UF) membrane surface, using polyethyleneimine (PEI) as the monomer of the aqueous phase, and a mixture of isophthaloyl dichloride (IPC) and tri-mesoyl chloride (TMC) as the monomer of the organic phase. Interestingly, a synergetic effect of the mass ratio of IPC and TMC was observed on the pore size and the structure of the active layer of the resultant polyamide (PA)/polysulfone (PSF) composite NF membrane. The rejection ( R ) to the inorganic electrolytes increased with the mass ratio of IPC to TMC, while the permeate flux ( F ) escalated up to a 1 : 1 mixing ratio of IPC to TMC and dropped at higher mixing ratios. The rejection to different inorganic electrolytes decreased in the order of ZnCl 2 , MgCl 2 , CaCl 2 , CuCl 2 , MgSO 4 , NaCl, and Na 2 SO 4 . At ambient temperature and 0.4 MPa, the optimized membrane demonstrated R and F to 1 g L −1 MgCl 2 aqueous solution as 98.1% and 27.6 L m −2 h −1 , respectively. Its rejection to various dyes reduced significantly in the order of cationic red X-GTL (100%), rhodamine B (94.2%), cationic gold yellow X-GL (93.5%), and brilliant blue KN-R (43.9%), in agreement with the decrease in the molecular weight ( M w ) and the overall charges of the dye. The tunable active layer structure was developed via interfacial polymerization, using polyethyleneimine as the monomer of the aqueous phase, and a mixture of isophthaloyl dichloride and tri-mesoyl chloride as the monomer of the organic phase. |
| Author | Tu, Kai Chen, Shunquan He, Yuantao Yang, Hao Zhang, Rui Zhang, Ling Jiang, Zhibin Miao, Jing |
| Author_xml | – sequence: 1 givenname: Zhibin surname: Jiang fullname: Jiang, Zhibin organization: Guangdong Key Laboratory of Membrane Materials and Membrane Separation, Guangzhou Institute of Advanced Technology, Chinese Academy of Sciences (CAS), Guangzhou 511458, PR China – sequence: 2 givenname: Jing orcidid: 0000-0003-4436-2823 surname: Miao fullname: Miao, Jing organization: Guangdong Key Laboratory of Membrane Materials and Membrane Separation, Guangzhou Institute of Advanced Technology, Chinese Academy of Sciences (CAS), Guangzhou 511458, PR China – sequence: 3 givenname: Yuantao surname: He fullname: He, Yuantao organization: Guangdong Key Laboratory of Membrane Materials and Membrane Separation, Guangzhou Institute of Advanced Technology, Chinese Academy of Sciences (CAS), Guangzhou 511458, PR China – sequence: 4 givenname: Kai surname: Tu fullname: Tu, Kai organization: Guangdong Key Laboratory of Membrane Materials and Membrane Separation, Guangzhou Institute of Advanced Technology, Chinese Academy of Sciences (CAS), Guangzhou 511458, PR China – sequence: 5 givenname: Shunquan surname: Chen fullname: Chen, Shunquan organization: Guangdong Key Laboratory of Membrane Materials and Membrane Separation, Guangzhou Institute of Advanced Technology, Chinese Academy of Sciences (CAS), Guangzhou 511458, PR China – sequence: 6 givenname: Rui surname: Zhang fullname: Zhang, Rui organization: Shandong Disk Tube Reverse Osmosis (DTRO) Membrane Engineering Laboratory, The New Water Technology, Inc. (NEWA), China – sequence: 7 givenname: Ling orcidid: 0000-0001-7289-2288 surname: Zhang fullname: Zhang, Ling organization: School of Resource and Environment, University of Jinan, Jinan 250022, PR China – sequence: 8 givenname: Hao orcidid: 0000-0003-3325-1378 surname: Yang fullname: Yang, Hao organization: Key Laboratory for Green Chemical Process of Ministry of Education, School of Environmental Ecology and Biological Engineering, Wuhan Institute of Technology, Wuhan, PR China |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/35515306$$D View this record in MEDLINE/PubMed |
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| Snippet | A novel positively charged composite nanofiltration (NF) membrane with tunable active layer structure was successfully developed
via
interfacial polymerization... A novel positively charged composite nanofiltration (NF) membrane with tunable active layer structure was successfully developed interfacial polymerization on... A novel positively charged composite nanofiltration (NF) membrane with tunable active layer structure was successfully developed via interfacial polymerization... |
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| SubjectTerms | Ambient temperature Aqueous solutions Calcium chloride Cations Chemistry Dichlorides Dyes Electrolytes Gold Magnesium chloride magnesium sulfate Mixing ratio Molecular weight Monomers Nanofiltration organochlorine compounds Polyamide resins polyamides Polyethyleneimine Polymerization Polysulfone resins Pore size Porosity Rejection Rhodamine rhodamines sodium chloride Sodium sulfate Ultrafiltration Zinc chloride |
| Title | A novel positively charged composite nanofiltration membrane based on polyethyleneimine with a tunable active layer structure developed via interfacial polymerization |
| URI | https://www.ncbi.nlm.nih.gov/pubmed/35515306 https://www.proquest.com/docview/2205382951 https://www.proquest.com/docview/2237546166 https://www.proquest.com/docview/2661082369 https://pubmed.ncbi.nlm.nih.gov/PMC9062538 |
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