PAN—Composite Electrospun-Fibers Decorated with Magnetite Nanoparticles

The results of the synthesis of PAN(polyacrylonitrile)-magnetite composite fibers using the electrospinning method are presented. The electrospinning installation included a rotating drum collector for collecting fibers. Magnetite nanoparticles were synthesized using chemical condensation from an ir...

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Published inMagnetochemistry Vol. 8; no. 11; p. 160
Main Authors Mansurov, Zulkhair, Smagulova, Gaukhar, Kaidar, Bayan, Imash, Aigerim, Lesbayev, Aidos
Format Journal Article
LanguageEnglish
Published Basel MDPI AG 01.11.2022
Subjects
Analysis
Aqueous solutions
Biosensors
Chemical synthesis
composite fibers
Composite materials
Diffraction
Electron microscopy
Electrospinning
Fibers
Information storage
Iron chlorides
Iron oxides
Magnetic properties
Magnetite
Methods
Morphology
Nanocomposites
Nanomaterials
Nanoparticles
PCB
Polyacrylonitrile
Polychlorinated biphenyls
Polyvinyl alcohol
Scanning microscopy
Structure
X-ray diffraction
X-rays
Kazakhstan
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Abstract The results of the synthesis of PAN(polyacrylonitrile)-magnetite composite fibers using the electrospinning method are presented. The electrospinning installation included a rotating drum collector for collecting fibers. Magnetite nanoparticles were synthesized using chemical condensation from an iron chloride solution. It was shown that homogeneous Fe3O4 magnetite nanoparticles with particle sizes of 6–16 nm could be synthesized using this method. Magnetite nanoparticles were investigated using X-ray diffraction analyses and transmission electron microscopy. Based on magnetite nanoparticles, composite PAN/magnetite fibers were obtained through electrospinning. The obtained composite fibers were investigated using scanning electron microscopy, X-ray diffraction analyses, and elemental analyses. It was shown that the magnetite nanoparticles were uniformly distributed on the surface of the fibers. A comparison of PAN fibers without any added magnetite to PAN/magnetite fibers showed that the addition of magnetite led to a decrease in the value of the fiber diameter at the same polymer concentration and under the same electrospinning process conditions.
AbstractList The results of the synthesis of PAN(polyacrylonitrile)-magnetite composite fibers using the electrospinning method are presented. The electrospinning installation included a rotating drum collector for collecting fibers. Magnetite nanoparticles were synthesized using chemical condensation from an iron chloride solution. It was shown that homogeneous Fe[sub.3] O[sub.4] magnetite nanoparticles with particle sizes of 6–16 nm could be synthesized using this method. Magnetite nanoparticles were investigated using X-ray diffraction analyses and transmission electron microscopy. Based on magnetite nanoparticles, composite PAN/magnetite fibers were obtained through electrospinning. The obtained composite fibers were investigated using scanning electron microscopy, X-ray diffraction analyses, and elemental analyses. It was shown that the magnetite nanoparticles were uniformly distributed on the surface of the fibers. A comparison of PAN fibers without any added magnetite to PAN/magnetite fibers showed that the addition of magnetite led to a decrease in the value of the fiber diameter at the same polymer concentration and under the same electrospinning process conditions.
The results of the synthesis of PAN(polyacrylonitrile)-magnetite composite fibers using the electrospinning method are presented. The electrospinning installation included a rotating drum collector for collecting fibers. Magnetite nanoparticles were synthesized using chemical condensation from an iron chloride solution. It was shown that homogeneous Fe3O4 magnetite nanoparticles with particle sizes of 6–16 nm could be synthesized using this method. Magnetite nanoparticles were investigated using X-ray diffraction analyses and transmission electron microscopy. Based on magnetite nanoparticles, composite PAN/magnetite fibers were obtained through electrospinning. The obtained composite fibers were investigated using scanning electron microscopy, X-ray diffraction analyses, and elemental analyses. It was shown that the magnetite nanoparticles were uniformly distributed on the surface of the fibers. A comparison of PAN fibers without any added magnetite to PAN/magnetite fibers showed that the addition of magnetite led to a decrease in the value of the fiber diameter at the same polymer concentration and under the same electrospinning process conditions.
Audience Academic
Author Kaidar, Bayan
Smagulova, Gaukhar
Imash, Aigerim
Mansurov, Zulkhair
Lesbayev, Aidos
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  surname: Lesbayev
  fullname: Lesbayev, Aidos
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Snippet The results of the synthesis of PAN(polyacrylonitrile)-magnetite composite fibers using the electrospinning method are presented. The electrospinning...
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SubjectTerms Analysis
Aqueous solutions
Biosensors
Chemical synthesis
composite fibers
Composite materials
Diffraction
Electron microscopy
Electrospinning
Fibers
Information storage
Iron chlorides
Iron oxides
Magnetic properties
Magnetite
Methods
Morphology
Nanocomposites
Nanomaterials
Nanoparticles
PCB
Polyacrylonitrile
Polychlorinated biphenyls
Polyvinyl alcohol
Scanning microscopy
Structure
X-ray diffraction
X-rays
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Title PAN—Composite Electrospun-Fibers Decorated with Magnetite Nanoparticles
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