Stable melt formation of 2D nitrile-based coordination polymer and hierarchical crystal-glass structuring

Crystal melting and vitrification of nitrile-based two-dimensional coordination polymer (CP) were studied. The crystal melts at 169 °C and has a wide liquid-state temperature window of over 110 °C. The crystalline state transformed to a glassy state by melt-quench or mechanical milling. The mechanic...

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Published inChemical communications (Cambridge, England) Vol. 56; no. 63; pp. 898 - 8983
Main Authors Das, Chinmoy, Ogawa, Tomohiro, Horike, Satoshi
Format Journal Article
LanguageEnglish
Published Cambridge Royal Society of Chemistry 14.08.2020
Subjects
Coordination polymers
Crystal structure
Crystallization
Glass
Mechanical milling
Melts (crystal growth)
Porosity
solvents
temperature
Vitrification
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Abstract Crystal melting and vitrification of nitrile-based two-dimensional coordination polymer (CP) were studied. The crystal melts at 169 °C and has a wide liquid-state temperature window of over 110 °C. The crystalline state transformed to a glassy state by melt-quench or mechanical milling. The mechanically induced glass showed permanent porosity, and it also showed glass-to-crystal transformation upon solvent treatment. Surface crystallization on top of the grain-boundary-free glass monolith was demonstrated. 2D nitrile-based coordination polymer crystal shows over 110 °C of windows of liquid state and it forms a glass monolith.
AbstractList Crystal melting and vitrification of nitrile-based two-dimensional coordination polymer (CP) were studied. The crystal melts at 169 °C and has a wide liquid-state temperature window of over 110 °C. The crystalline state transformed to a glassy state by melt-quench or mechanical milling. The mechanically induced glass showed permanent porosity, and it also showed glass-to-crystal transformation upon solvent treatment. Surface crystallization on top of the grain-boundary-free glass monolith was demonstrated.Crystal melting and vitrification of nitrile-based two-dimensional coordination polymer (CP) were studied. The crystal melts at 169 °C and has a wide liquid-state temperature window of over 110 °C. The crystalline state transformed to a glassy state by melt-quench or mechanical milling. The mechanically induced glass showed permanent porosity, and it also showed glass-to-crystal transformation upon solvent treatment. Surface crystallization on top of the grain-boundary-free glass monolith was demonstrated.
Crystal melting and vitrification of nitrile-based two-dimensional coordination polymer (CP) were studied. The crystal melts at 169 °C and has a wide liquid-state temperature window of over 110 °C. The crystalline state transformed to a glassy state by melt-quench or mechanical milling. The mechanically induced glass showed permanent porosity, and it also showed glass-to-crystal transformation upon solvent treatment. Surface crystallization on top of the grain-boundary-free glass monolith was demonstrated.
Crystal melting and vitrification of nitrile-based two-dimensional coordination polymer (CP) were studied. The crystal melts at 169 °C and has a wide liquid-state temperature window of over 110 °C. The crystalline state transformed to a glassy state by melt-quench or mechanical milling. The mechanically induced glass showed permanent porosity, and it also showed glass-to-crystal transformation upon solvent treatment. Surface crystallization on top of the grain-boundary-free glass monolith was demonstrated. 2D nitrile-based coordination polymer crystal shows over 110 °C of windows of liquid state and it forms a glass monolith.
Author Das, Chinmoy
Ogawa, Tomohiro
Horike, Satoshi
AuthorAffiliation Kyoto University
AIST-Kyoto University Chemical Energy Materials Open Innovation Laboratory (ChEM-OIL)
National Institute of Advanced Industrial Science and Technology (AIST)
Yoshida-Honmachi
Institute for Integrated Cell-Material Sciences
Department of Synthetic Chemistry and Biological Chemistry
Institute for Advanced Study
Graduate School of Engineering
Department of Materials Science and Engineering
School of Molecular Science and Engineering
Vidyasirimedhi Institute of Science and Technology
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Snippet Crystal melting and vitrification of nitrile-based two-dimensional coordination polymer (CP) were studied. The crystal melts at 169 °C and has a wide...
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SubjectTerms Coordination polymers
Crystal structure
Crystallization
Glass
Mechanical milling
Melts (crystal growth)
Porosity
solvents
temperature
Vitrification
Title Stable melt formation of 2D nitrile-based coordination polymer and hierarchical crystal-glass structuring
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