Design of zeolite catalysts for nitroaldol reaction under mild condition

[Display omitted] ► Henry nitroaldol reaction conditions were optimized with moderately weak base catalysts under various reaction conditions. ► Basic zeolites NaY, KL and their alkali metal impregnated form are found to be effective catalysts for nitroaldol reaction. ► Framework structure of zeolit...

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Published inApplied catalysis. A, General Vol. 433-434; pp. 122 - 127
Main Authors Devi, Rasna, Borah, Ruli, Deka, Ramesh C.
Format Journal Article
LanguageEnglish
Published AMSTERDAM Elsevier B.V 08.08.2012
Elsevier
Subjects
Base catalyst
Catalysis
Catalysts
Chemistry
Chemistry, Physical
Conversion
Environmental Sciences
Environmental Sciences & Ecology
Free energy
Hammett's constant
Henry nitroaldol reaction
Life Sciences & Biomedicine
Nuclear magnetic resonance
Physical Sciences
Science & Technology
Solvents
Spectra
Zeolite
Zeolites
β-Nitro alcohols
Hammett's constant
Zeolite
Henry nitroaldol reaction
Base catalyst
β-Nitro alcohols
KNOEVENAGEL
CONVERSION
COMPLEXES
ALDEHYDES
HENRY REACTION
beta-Nitro alcohols
NITROALKANES
CONDENSATION
SILICA
DERIVATIVES
ASYMMETRIC HENRY
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Abstract [Display omitted] ► Henry nitroaldol reaction conditions were optimized with moderately weak base catalysts under various reaction conditions. ► Basic zeolites NaY, KL and their alkali metal impregnated form are found to be effective catalysts for nitroaldol reaction. ► Framework structure of zeolites does not break after modification. ► The reaction gives nitroaldol product in good yield. NaY and KL zeolites were modified by impregnating with potassium fluoride for investigating their basicity and catalytic activity towards Henry nitroaldol reaction under different reaction conditions. Effects of solvents, temperature, catalysts and ratio of substrate versus reagents were studied to optimize the reaction conditions. The catalysts were characterized by FTIR, XRD and SEM techniques and the products were characterized by 1H NMR, 13C NMR and FTIR techniques. It was observed that NaY/KF zeolite with H2O–MeOH pair as solvent showed good conversion and selectivity at room temperature. Both XRD and FTIR study showed no change of spectral patterns for both modified and parent zeolites. We have again showed a plot of Hammett free energy linear relationship in terms of percentage yield and Hammett substituent constant.
AbstractList [Display omitted] ► Henry nitroaldol reaction conditions were optimized with moderately weak base catalysts under various reaction conditions. ► Basic zeolites NaY, KL and their alkali metal impregnated form are found to be effective catalysts for nitroaldol reaction. ► Framework structure of zeolites does not break after modification. ► The reaction gives nitroaldol product in good yield. NaY and KL zeolites were modified by impregnating with potassium fluoride for investigating their basicity and catalytic activity towards Henry nitroaldol reaction under different reaction conditions. Effects of solvents, temperature, catalysts and ratio of substrate versus reagents were studied to optimize the reaction conditions. The catalysts were characterized by FTIR, XRD and SEM techniques and the products were characterized by 1H NMR, 13C NMR and FTIR techniques. It was observed that NaY/KF zeolite with H2O–MeOH pair as solvent showed good conversion and selectivity at room temperature. Both XRD and FTIR study showed no change of spectral patterns for both modified and parent zeolites. We have again showed a plot of Hammett free energy linear relationship in terms of percentage yield and Hammett substituent constant.
NaY and KL zeolites were modified by impregnating with potassium fluoride for investigating their basicity and catalytic activity towards Henry nitroaldol reaction under different reaction conditions. Effects of solvents, temperature, catalysts and ratio of substrate versus reagents were studied to optimize the reaction conditions. The catalysts were characterized by FTIR, XRD and SEM techniques and the products were characterized by 1H NMR, 13C NMR and FTIR techniques. It was observed that NaY/KF zeolite with H2OaMeOH pair as solvent showed good conversion and selectivity at room temperature. Both XRD and FTIR study showed no change of spectral patterns for both modified and parent zeolites. We have again showed a plot of Hammett free energy linear relationship in terms of percentage yield and Hammett substituent constant.
NaY and KL zeolites were modified by impregnating with potassium fluoride for investigating their basicity and catalytic activity towards Henry nitroaldol reaction under different reaction conditions. Effects of solvents, temperature, catalysts and ratio of substrate versus reagents were studied to optimize the reaction conditions. The catalysts were characterized by FTIR, XRD and SEM techniques and the products were characterized by H-1 NMR, C-13 NMR and FTIR techniques. It was observed that NaY/KF zeolite with H2O-MeOH pair as solvent showed good conversion and selectivity at room temperature. Both XRD and FTIR study showed no change of spectral patterns for both modified and parent zeolites. We have again showed a plot of Hammett free energy linear relationship in terms of percentage yield and Hammett substituent constant. (C) 2012 Elsevier B.V. All rights reserved.
Author Borah, Ruli
Devi, Rasna
Deka, Ramesh C.
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Keywords Hammett's constant
Zeolite
Henry nitroaldol reaction
Base catalyst
β-Nitro alcohols
KNOEVENAGEL
CONVERSION
COMPLEXES
ALDEHYDES
HENRY REACTION
beta-Nitro alcohols
NITROALKANES
CONDENSATION
SILICA
DERIVATIVES
ASYMMETRIC HENRY
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Snippet [Display omitted] ► Henry nitroaldol reaction conditions were optimized with moderately weak base catalysts under various reaction conditions. ► Basic zeolites...
NaY and KL zeolites were modified by impregnating with potassium fluoride for investigating their basicity and catalytic activity towards Henry nitroaldol...
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SubjectTerms Base catalyst
Catalysis
Catalysts
Chemistry
Chemistry, Physical
Conversion
Environmental Sciences
Environmental Sciences & Ecology
Free energy
Hammett's constant
Henry nitroaldol reaction
Life Sciences & Biomedicine
Nuclear magnetic resonance
Physical Sciences
Science & Technology
Solvents
Spectra
Zeolite
Zeolites
β-Nitro alcohols
Title Design of zeolite catalysts for nitroaldol reaction under mild condition
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