Effects of microstructure of carbon nanofibers for amperometric detection of hydrogen peroxide
Carbon nanofibers (CNFs) with three microstructures, including platelet-carbon nanofibers (PCNFs), fish-bone-carbon nanofibers (FCNFs), and tube-carbon nanofibers (TCNFs), were synthesized, characterized, and evaluated for electrochemical sensing of hydrogen peroxide. The CNFs studied here show micr...
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Published in | Analytica chimica acta Vol. 597; no. 2; pp. 238 - 244 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
Published |
Amsterdam
Elsevier B.V
10.08.2007
Elsevier |
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Abstract | Carbon nanofibers (CNFs) with three microstructures, including platelet-carbon nanofibers (PCNFs), fish-bone-carbon nanofibers (FCNFs), and tube-carbon nanofibers (TCNFs), were synthesized, characterized, and evaluated for electrochemical sensing of hydrogen peroxide. The CNFs studied here show microstructures with various stacked morphologies. The sizes and graphite-layer ordering of the CNFs can be well controlled. Glassy carbon (GC) electrodes modified by CNFs were fabricated and compared for amperometric detection of hydrogen peroxide. Sensors based on PCNFs/GC, FCNFs/GC, and TCNFs/GC were used in the amperometric detection of H
2O
2 in solution by applying a potential of +0.65
V versus Ag/AgCl at the working electrode. The highest electrocatalytic performance was observed for PCNFs/GC among the three types of hydrogen peroxide sensors. The amperometric response of PCNFs/GC retained over 90% of the initial current of the first day up to 21 days. The linear range is from 1.80
×
10
−4 to 2.62
×
10
−3
M with a correlation coefficient larger than 0.999 and with a detection limit of 4.0
μM H
2O
2 (S/N
=
3). The relative standard deviation for detecting 1.80
×
10
−4
M H
2O
2 (
N
=
8) is 2.1% with an average response of 0.64
μA. The significant diversity of electrocatalytic activity of the CNFs toward the oxidation of hydrogen peroxide may result from the difference of morphologies, textural properties, and crystalline structures. |
---|---|
AbstractList | Carbon nanofibers (CNFs) with different microstructures, including platelet-carbon nanofibers (PCNFs), fish-bone-carbon nanofibers (FCNFs), and tube-carbon nanofibers (TCNFs), were synthesized, characterized, and evaluated for electrochemical sensing of hydrogen peroxide. The CNFs studied here can show several microstructures in which various stacked morphologies and their sizes and graphite-layer ordering can be well controlled. Glassy carbon (GC) electrodes modified by CNFs were fabricated and compared for amperometric detection of hydrogen peroxide. Sensors of PCNFs/GC, FCNFs/GC, and TCNFs/GC were used in the amperometric detection of H2O2 in a solution of 0.05 M phosphate buffered saline solution (pH 7.4). Carbon nanofibers (CNFs) with three microstructures, including platelet-carbon nanofibers (PCNFs), fish-bone-carbon nanofibers (FCNFs), and tube-carbon nanofibers (TCNFs), were synthesized, characterized, and evaluated for electrochemical sensing of hydrogen peroxide. The CNFs studied here show microstructures with various stacked morphologies. The sizes and graphite-layer ordering of the CNFs can be well controlled. Glassy carbon (GC) electrodes modified by CNFs were fabricated and compared for amperometric detection of hydrogen peroxide. Sensors based on PCNFs/GC, FCNFs/GC, and TCNFs/GC were used in the amperometric detection of H 2O 2 in solution by applying a potential of +0.65 V versus Ag/AgCl at the working electrode. The highest electrocatalytic performance was observed for PCNFs/GC among the three types of hydrogen peroxide sensors. The amperometric response of PCNFs/GC retained over 90% of the initial current of the first day up to 21 days. The linear range is from 1.80 × 10 −4 to 2.62 × 10 −3 M with a correlation coefficient larger than 0.999 and with a detection limit of 4.0 μM H 2O 2 (S/N = 3). The relative standard deviation for detecting 1.80 × 10 −4 M H 2O 2 ( N = 8) is 2.1% with an average response of 0.64 μA. The significant diversity of electrocatalytic activity of the CNFs toward the oxidation of hydrogen peroxide may result from the difference of morphologies, textural properties, and crystalline structures. Carbon nanofibers (CNFs) with three microstructures, including platelet-carbon nanofibers (PCNFs), fish-bone-carbon nanofibers (FCNFs), and tube-carbon nanofibers (TCNFs), were synthesized, characterized, and evaluated for electrochemical sensing of hydrogen peroxide. The CNFs studied here show microstructures with various stacked morphologies. The sizes and graphite-layer ordering of the CNFs can be well controlled. Glassy carbon (GC) electrodes modified by CNFs were fabricated and compared for amperometric detection of hydrogen peroxide. Sensors based on PCNFs/GC, FCNFs/GC, and TCNFs/GC were used in the amperometric detection of H2O2 in solution by applying a potential of +0.65 V versus Ag/AgCl at the working electrode. The highest electrocatalytic performance was observed for PCNFs/GC among the three types of hydrogen peroxide sensors. The amperometric response of PCNFs/GC retained over 90% of the initial current of the first day up to 21 days. The linear range is from 1.80x10(-4) to 2.62x10(-3) M with a correlation coefficient larger than 0.999 and with a detection limit of 4.0 microM H2O2 (S/N = 3). The relative standard deviation for detecting 1.80x10(-4) M H2O2 (N = 8) is 2.1% with an average response of 0.64 microA. The significant diversity of electrocatalytic activity of the CNFs toward the oxidation of hydrogen peroxide may result from the difference of morphologies, textural properties, and crystalline structures. Carbon nanofibers (CNFs) with three microstructures, including platelet-carbon nanofibers (PCNFs), fish-bone-carbon nanofibers (FCNFs), and tube-carbon nanofibers (TCNFs), were synthesized, characterized, and evaluated for electrochemical sensing of hydrogen peroxide. The CNFs studied here show microstructures with various stacked morphologies. The sizes and graphite-layer ordering of the CNFs can be well controlled. Glassy carbon (GC) electrodes modified by CNFs were fabricated and compared for amperometric detection of hydrogen peroxide. Sensors based on PCNFs/GC, FCNFs/GC, and TCNFs/GC were used in the amperometric detection of H2O2 in solution by applying a potential of +0.65V versus Ag/AgCl at the working electrode. The highest electrocatalytic performance was observed for PCNFs/GC among the three types of hydrogen peroxide sensors. The amperometric response of PCNFs/GC retained over 90% of the initial current of the first day up to 21 days. The linear range is from 1.80X10-4 to 2.62X10-3M with a correlation coefficient larger than 0.999 and with a detection limit of 4.0muM H2O2 (S/N=3). The relative standard deviation for detecting 1.80X10-4M H2O2 (N=8) is 2.1% with an average response of 0.64muA. The significant diversity of electrocatalytic activity of the CNFs toward the oxidation of hydrogen peroxide may result from the difference of morphologies, textural properties, and crystalline structures. |
Author | Li, Zhizhou Lin, Yuehe Zheng, Junsheng Wang, Qingfei Cui, Xiaoli |
Author_xml | – sequence: 1 givenname: Zhizhou surname: Li fullname: Li, Zhizhou organization: Department of Materials Science, Fudan University, Shanghai 200433, China – sequence: 2 givenname: Xiaoli surname: Cui fullname: Cui, Xiaoli email: xiaolicui@fudan.edu.cn organization: Department of Materials Science, Fudan University, Shanghai 200433, China – sequence: 3 givenname: Junsheng surname: Zheng fullname: Zheng, Junsheng organization: State Key Laboratory of Chemical Engineering, East China University of Science and Technology, Shanghai 200237, China – sequence: 4 givenname: Qingfei surname: Wang fullname: Wang, Qingfei organization: College of Chemistry and Materials Science, Hebei Normal University, Shijiazhuang 050016, China – sequence: 5 givenname: Yuehe surname: Lin fullname: Lin, Yuehe email: yuehe.lin@pnl.gov organization: Pacific Northwest National Laboratory, Richland, WA 99352, USA |
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Keywords | Hydrogen peroxide oxidation Carbon nanofibers Electrocatalytic activity Hydrogen peroxide sensors Correlation coefficient Performance evaluation Hydrogen peroxide Electrochemical method Carbon electrode Chemical sensor Carbon Electrocatalysis Vertebrata Detection limit Pisces Graphite Amperometry Standard deviation Oxidation Microstructure Crystalline structure |
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Snippet | Carbon nanofibers (CNFs) with three microstructures, including platelet-carbon nanofibers (PCNFs), fish-bone-carbon nanofibers (FCNFs), and tube-carbon... Carbon nanofibers (CNFs) with different microstructures, including platelet-carbon nanofibers (PCNFs), fish-bone-carbon nanofibers (FCNFs), and tube-carbon... |
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SubjectTerms | AMPEROMETRY Analytical chemistry biosensors CARBON Carbon - chemistry Carbon nanofibers Chemistry DETECTION Electrocatalytic activity Electrochemical methods ELECTRODES Environmental Molecular Sciences Laboratory Exact sciences and technology FABRICATION FIBERS General, instrumentation Glass - chemistry HYDROGEN PEROXIDE Hydrogen Peroxide - analysis Hydrogen peroxide oxidation Hydrogen peroxide sensors INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY Microscopy, Electron, Transmission MICROSTRUCTURE NANOSCIENCE AND NANOTECHNOLOGY NANOSTRUCTURES Nanostructures - chemistry Nanostructures - ultrastructure Oxidation-Reduction Reproducibility of Results Sensitivity and Specificity Water - chemistry |
Title | Effects of microstructure of carbon nanofibers for amperometric detection of hydrogen peroxide |
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