Synthesis and characterization of Fe-doped TiO2 films by electrophoretic method and its photocatalytic activity toward methyl orange

In this study the cathodic electrophoretic deposition method has been developed and used to prepare Fe-doped TiO2 films to enhance the photocatalytic activity. X-ray diffraction (XRD) showed that the photocatalysts were predominantly in well-crystallized anatase phase, scanning electron microscope (...

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Published in	Solid state sciences Vol. 16; pp. 16 - 20
Main Authors	Zhang, Yanrong, Li, Qian
Format	Journal Article
Language	English
Published	Issy-les-Moulineaux Elsevier Masson SAS 01.02.2013 Elsevier Masson
Subjects	Chemistry Electrophoretic deposition Exact sciences and technology Fe-doped TiO2 film General and physical chemistry General, apparatus Low temperature Methyl orange Photocatalytic decolorization Surface physical chemistry Fe-doped TiO2 film Methyl orange Photocatalytic decolorization Electrophoretic deposition Low temperature Scanning electron microscopy Anatase Photocatalysis Fe-doped TiO Iron film X ray diffraction Molybdenum Thin film Transmission electron microscopy Iron addition Titanium oxide Catalyst activity Catalyst
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Abstract	In this study the cathodic electrophoretic deposition method has been developed and used to prepare Fe-doped TiO2 films to enhance the photocatalytic activity. X-ray diffraction (XRD) showed that the photocatalysts were predominantly in well-crystallized anatase phase, scanning electron microscope (SEM) and transmission electron microscopy (TEM) showed that the photocatalysts were in nanometer size with the diameter about 20 nm. We discussed the effects of electrophoretic voltage and the optimum content of Fe on the activity of photocatalyst. Compared to the calcined Fe-doped TiO2 film, the non-calcined Fe-doped TiO2 film showed higher photocatalytic decolorization toward methyl orange (MO). The photocatalytic degradation of MO could be described as pseudo-first order reactions. [Display omitted] ► Fe-doped TiO2 film was prepared by electrophoretic deposition method. ► Non-calcined Fe-doped TiO2 films exhibited an enhanced photocatalyst activity. ► Calcination process exerted a disaster effect on the photocatalytic activity of the non-calcined films.
AbstractList	In this study the cathodic electrophoretic deposition method has been developed and used to prepare Fe-doped TiO2 films to enhance the photocatalytic activity. X-ray diffraction (XRD) showed that the photocatalysts were predominantly in well-crystallized anatase phase, scanning electron microscope (SEM) and transmission electron microscopy (TEM) showed that the photocatalysts were in nanometer size with the diameter about 20 nm. We discussed the effects of electrophoretic voltage and the optimum content of Fe on the activity of photocatalyst. Compared to the calcined Fe-doped TiO2 film, the non-calcined Fe-doped TiO2 film showed higher photocatalytic decolorization toward methyl orange (MO). The photocatalytic degradation of MO could be described as pseudo-first order reactions. [Display omitted] ► Fe-doped TiO2 film was prepared by electrophoretic deposition method. ► Non-calcined Fe-doped TiO2 films exhibited an enhanced photocatalyst activity. ► Calcination process exerted a disaster effect on the photocatalytic activity of the non-calcined films.
Author	Li, Qian Zhang, Yanrong
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Keywords	Fe-doped TiO2 film Methyl orange Photocatalytic decolorization Electrophoretic deposition Low temperature Scanning electron microscopy Anatase Photocatalysis Fe-doped TiO Iron film X ray diffraction Molybdenum Thin film Transmission electron microscopy Iron addition Titanium oxide Catalyst activity Catalyst
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Snippet	In this study the cathodic electrophoretic deposition method has been developed and used to prepare Fe-doped TiO2 films to enhance the photocatalytic activity....
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SubjectTerms	Chemistry Electrophoretic deposition Exact sciences and technology Fe-doped TiO2 film General and physical chemistry General, apparatus Low temperature Methyl orange Photocatalytic decolorization Surface physical chemistry
Title	Synthesis and characterization of Fe-doped TiO2 films by electrophoretic method and its photocatalytic activity toward methyl orange
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