Self‐assembly of poly(ionic liquid) functionalized mesoporous magnetic microspheres for the solid‐phase extraction of preservatives from milk samples
In this work, a novel, rapid, and simple analytical method was proposed for the detection of parabens in milk sample by gas chromatography coupled with mass spectrometry. At the same time, milk sample was pretreated by magnetic solid phase extraction, which detected up to five parabens. A series of...
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| Published in | Journal of separation science Vol. 43; no. 4; pp. 766 - 773 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
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01.02.2020
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| Abstract | In this work, a novel, rapid, and simple analytical method was proposed for the detection of parabens in milk sample by gas chromatography coupled with mass spectrometry. At the same time, milk sample was pretreated by magnetic solid phase extraction, which detected up to five parabens. A series of important parameters of magnetic solid phase extraction were investigated and optimized, such as pH value of loading buffer, amount of material, adsorption time, ionic strength, eluting solvents, and eluting time. Under the optimized conditions, the corresponding values were more than 0.9991, limits of detection and the limit of quantification were 0.1 and 0.5 ng/mL, respectively. In addition, the recoveries were achieved in range of 95–105%, the liner range were within 0.1–600 ng/mL, and the relative standard deviations were even lower than 5%. |
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| AbstractList | In this work, a novel, rapid, and simple analytical method was proposed for the detection of parabens in milk sample by gas chromatography coupled with mass spectrometry. At the same time, milk sample was pretreated by magnetic solid phase extraction, which detected up to five parabens. A series of important parameters of magnetic solid phase extraction were investigated and optimized, such as pH value of loading buffer, amount of material, adsorption time, ionic strength, eluting solvents, and eluting time. Under the optimized conditions, the corresponding values were more than 0.9991, limits of detection and the limit of quantification were 0.1 and 0.5 ng/mL, respectively. In addition, the recoveries were achieved in range of 95–105%, the liner range were within 0.1–600 ng/mL, and the relative standard deviations were even lower than 5%. In this work, a novel, rapid, and simple analytical method was proposed for the detection of parabens in milk sample by gas chromatography coupled with mass spectrometry. At the same time, milk sample was pretreated by magnetic solid phase extraction, which detected up to five parabens. A series of important parameters of magnetic solid phase extraction were investigated and optimized, such as pH value of loading buffer, amount of material, adsorption time, ionic strength, eluting solvents, and eluting time. Under the optimized conditions, the corresponding values were more than 0.9991, limits of detection and the limit of quantification were 0.1 and 0.5 ng/mL, respectively. In addition, the recoveries were achieved in range of 95-105%, the liner range were within 0.1-600 ng/mL, and the relative standard deviations were even lower than 5%.In this work, a novel, rapid, and simple analytical method was proposed for the detection of parabens in milk sample by gas chromatography coupled with mass spectrometry. At the same time, milk sample was pretreated by magnetic solid phase extraction, which detected up to five parabens. A series of important parameters of magnetic solid phase extraction were investigated and optimized, such as pH value of loading buffer, amount of material, adsorption time, ionic strength, eluting solvents, and eluting time. Under the optimized conditions, the corresponding values were more than 0.9991, limits of detection and the limit of quantification were 0.1 and 0.5 ng/mL, respectively. In addition, the recoveries were achieved in range of 95-105%, the liner range were within 0.1-600 ng/mL, and the relative standard deviations were even lower than 5%. In this work, a novel, rapid, and simple analytical method was proposed for the detection of parabens in milk sample by gas chromatography coupled with mass spectrometry. At the same time, milk sample was pretreated by magnetic solid phase extraction, which detected up to five parabens. A series of important parameters of magnetic solid phase extraction were investigated and optimized, such as pH value of loading buffer, amount of material, adsorption time, ionic strength, eluting solvents, and eluting time. Under the optimized conditions, the corresponding values were more than 0.9991, limits of detection and the limit of quantification were 0.1 and 0.5 ng/mL, respectively. In addition, the recoveries were achieved in range of 95–105%, the liner range were within 0.1–600 ng/mL, and the relative standard deviations were even lower than 5%. |
| Author | Ding, Chuan‐Fan Gao, Yiqian Tang, Keqi Yan, Yinghua Wang, Yucen |
| Author_xml | – sequence: 1 givenname: Yiqian surname: Gao fullname: Gao, Yiqian organization: Ningbo University – sequence: 2 givenname: Yucen surname: Wang fullname: Wang, Yucen organization: Ningbo Foreign Language School – sequence: 3 givenname: Yinghua orcidid: 0000-0002-0569-2881 surname: Yan fullname: Yan, Yinghua email: yanyinghua@nbu.edu.cn organization: Ningbo University – sequence: 4 givenname: Keqi surname: Tang fullname: Tang, Keqi organization: Ningbo University – sequence: 5 givenname: Chuan‐Fan surname: Ding fullname: Ding, Chuan‐Fan organization: Ningbo University |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/31746547$$D View this record in MEDLINE/PubMed |
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| CitedBy_id | crossref_primary_10_1007_s40201_021_00628_7 crossref_primary_10_1016_j_greeac_2022_100002 crossref_primary_10_20964_2021_02_22 crossref_primary_10_1002_nano_202100069 crossref_primary_10_1016_j_aca_2022_339632 crossref_primary_10_1016_j_scca_2024_100054 crossref_primary_10_1002_sscp_202000086 crossref_primary_10_1016_j_teac_2020_e00109 crossref_primary_10_1007_s00604_022_05444_w crossref_primary_10_1016_j_foodchem_2022_132843 crossref_primary_10_1016_j_trac_2021_116496 crossref_primary_10_3390_molecules29061296 crossref_primary_10_3390_separations7030037 |
| Cites_doi | 10.1016/j.electacta.2019.06.003 10.1016/j.seppur.2019.04.018 10.1002/jat.1358 10.1007/s13738-015-0626-8 10.1016/j.talanta.2018.02.022 10.1016/S0278-6915(99)00160-X 10.1002/jat.958 10.1039/C8RA02109K 10.1016/j.bios.2018.02.032 10.1039/c3cc41330f 10.1002/pca.2374 10.1002/jssc.201900089 10.1016/j.reprotox.2010.01.013 10.1016/j.chroma.2016.09.011 10.1097/00008469-200312000-00006 10.1016/j.fct.2005.01.020 10.1016/j.ab.2018.05.018 10.1016/j.microc.2010.07.005 10.1016/j.chroma.2010.09.016 10.1016/j.foodchem.2017.12.085 10.1002/jssc.201200062 10.1186/s13065-019-0587-6 10.1016/j.fct.2017.07.056 10.3390/molecules23061450 10.1016/j.cej.2019.04.062 10.1016/j.scitotenv.2011.09.040 10.1039/C7RA06682A 10.1016/j.talanta.2018.01.079 10.1016/j.talanta.2017.04.026 10.1002/jssc.201200345 10.1016/j.tox.2007.01.010 10.1039/C8PY01254G |
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| SubjectTerms | adsorption detection limit Gas chromatography gas chromatography‐mass spectrometry Ionic liquids ionic strength Ions magnetic solid phase extraction magnetism Mass spectrometry microparticles Microspheres Milk parabens porous media Preservatives solid phase extraction Solid phases standard deviation |
| Title | Self‐assembly of poly(ionic liquid) functionalized mesoporous magnetic microspheres for the solid‐phase extraction of preservatives from milk samples |
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