In situ observation of NiS nanoparticles depositing on single TiO2 mesocrystal for enhanced photocatalytic hydrogen evolution activity
[Display omitted] •Deposition of NiS on TiO2 mesocrystal (TMC) was in situ monitored via single-particle photoluminescence (PL) spectroscopy.•The variations of PL intensity and lifetime on individual TMC particle was detected before and after NiS photodeposition.•The interfacial electron injection k...
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| Published in | Applied catalysis. B, Environmental Vol. 254; pp. 594 - 600 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Amsterdam
Elsevier B.V
05.10.2019
Elsevier BV |
| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
•Deposition of NiS on TiO2 mesocrystal (TMC) was in situ monitored via single-particle photoluminescence (PL) spectroscopy.•The variations of PL intensity and lifetime on individual TMC particle was detected before and after NiS photodeposition.•The interfacial electron injection kinetics from TMC to NiS in individual TMC/NiS particle was investigated.•TMC/NiS heterostructure exhibited 71 folds enhanced H2 evolution compared with TMC.
For photocatalysis, clarifications of charge carrier migration route and kinetics on individual particles by photoluminescence (PL) are of great importance because they play significant roles on unveiling the precise information of structure-activity relationships and closely relate to the photocatalytic activities of those semiconductors on targeted functions. Here, photodeposition process of NiS nanoparticles on single TiO2 mesocrystal (TMC) as co-catalyst is in situ monitored by PL images and spectra using a confocal single-particle PL microscopy, which provides straightforward results on understanding the photoexcited electrons transfer in both individual TMC and TMC/NiS nanoparticles. Through the changes in PL intensity and decay lifetime, preferential trapping site for NiS nanoparticles on TMC is identified and efficient electron interfacial migration from TMC to NiS nanoparticles is demonstrated, which lead to an almost 71 folds enhancement on the photocatalytic H2 evolution under 365-nm photoirradiation compared to pure TMC particles. |
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| AbstractList | For photocatalysis, clarifications of charge carrier migration route and kinetics on individual particles by photoluminescence (PL) are of great importance because they play significant roles on unveiling the precise information of structure-activity relationships and closely relate to the photocatalytic activities of those semiconductors on targeted functions. Here, photodeposition process of NiS nanoparticles on single TiO2 mesocrystal (TMC) as co-catalyst is in situ monitored by PL images and spectra using a confocal single-particle PL microscopy, which provides straightforward results on understanding the photoexcited electrons transfer in both individual TMC and TMC/NiS nanoparticles. Through the changes in PL intensity and decay lifetime, preferential trapping site for NiS nanoparticles on TMC is identified and efficient electron interfacial migration from TMC to NiS nanoparticles is demonstrated, which lead to an almost 71 folds enhancement on the photocatalytic H2 evolution under 365-nm photoirradiation compared to pure TMC particles. [Display omitted] •Deposition of NiS on TiO2 mesocrystal (TMC) was in situ monitored via single-particle photoluminescence (PL) spectroscopy.•The variations of PL intensity and lifetime on individual TMC particle was detected before and after NiS photodeposition.•The interfacial electron injection kinetics from TMC to NiS in individual TMC/NiS particle was investigated.•TMC/NiS heterostructure exhibited 71 folds enhanced H2 evolution compared with TMC. For photocatalysis, clarifications of charge carrier migration route and kinetics on individual particles by photoluminescence (PL) are of great importance because they play significant roles on unveiling the precise information of structure-activity relationships and closely relate to the photocatalytic activities of those semiconductors on targeted functions. Here, photodeposition process of NiS nanoparticles on single TiO2 mesocrystal (TMC) as co-catalyst is in situ monitored by PL images and spectra using a confocal single-particle PL microscopy, which provides straightforward results on understanding the photoexcited electrons transfer in both individual TMC and TMC/NiS nanoparticles. Through the changes in PL intensity and decay lifetime, preferential trapping site for NiS nanoparticles on TMC is identified and efficient electron interfacial migration from TMC to NiS nanoparticles is demonstrated, which lead to an almost 71 folds enhancement on the photocatalytic H2 evolution under 365-nm photoirradiation compared to pure TMC particles. |
| Author | Fujitsuka, Mamoru Shi, Xiaowei Kim, Sooyeon Majima, Tetsuro |
| Author_xml | – sequence: 1 givenname: Xiaowei surname: Shi fullname: Shi, Xiaowei organization: The Institute of Scientific and Industrial Research (SANKEN), Osaka University, Mihogaoka 8-1, Ibaraki, Osaka, 567-0047, Japan – sequence: 2 givenname: Sooyeon surname: Kim fullname: Kim, Sooyeon organization: The Institute of Scientific and Industrial Research (SANKEN), Osaka University, Mihogaoka 8-1, Ibaraki, Osaka, 567-0047, Japan – sequence: 3 givenname: Mamoru surname: Fujitsuka fullname: Fujitsuka, Mamoru organization: The Institute of Scientific and Industrial Research (SANKEN), Osaka University, Mihogaoka 8-1, Ibaraki, Osaka, 567-0047, Japan – sequence: 4 givenname: Tetsuro orcidid: 0000-0003-1805-1677 surname: Majima fullname: Majima, Tetsuro email: majima@sanken.osaka-u.ac.jp organization: The Institute of Scientific and Industrial Research (SANKEN), Osaka University, Mihogaoka 8-1, Ibaraki, Osaka, 567-0047, Japan |
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•Deposition of NiS on TiO2 mesocrystal (TMC) was in situ monitored via single-particle photoluminescence (PL) spectroscopy.•The variations of... For photocatalysis, clarifications of charge carrier migration route and kinetics on individual particles by photoluminescence (PL) are of great importance... |
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| SubjectTerms | Current carriers Heterostructure Hydrogen evolution In situ Migration Nanoparticles Particle physics Photocatalysis Photodeposition Photoluminescence Photons Reaction kinetics Structure-activity relationships Titanium dioxide |
| Title | In situ observation of NiS nanoparticles depositing on single TiO2 mesocrystal for enhanced photocatalytic hydrogen evolution activity |
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