Boron nitride quantum dots decorated ultrathin porous g-C3N4: Intensified exciton dissociation and charge transfer for promoting visible-light-driven molecular oxygen activation
[Display omitted] •A novel photocatalyst constructed by BNQDs and UPCN was prepared.•Intensified exciton dissociation and charge transfer across BNQDs/UPCN heterostructure.•Higher photocatalytic efficiency toward molecular oxygen activation under visible light.•Mechanisms of enhanced photocatalytic...
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| Published in | Applied catalysis. B, Environmental Vol. 245; pp. 87 - 99 |
|---|---|
| Main Authors | , , , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Amsterdam
Elsevier B.V
15.05.2019
Elsevier BV |
| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
•A novel photocatalyst constructed by BNQDs and UPCN was prepared.•Intensified exciton dissociation and charge transfer across BNQDs/UPCN heterostructure.•Higher photocatalytic efficiency toward molecular oxygen activation under visible light.•Mechanisms of enhanced photocatalytic activities were proposed.
Graphitic carbon nitride (g-C3N4) has enormous potential for photocatalysis, but only possesses moderate activity because of excitonic effects and sluggish charge transfer. Herein, metal-free heterostructure photocatalyst constructed by boron nitride quantum dots (BNQDs) and ultrathin porous g-C3N4 (UPCN) was successfully developed for overcoming these defects. Results showed that the BNQDs loaded UPCN can simultaneously promote the dissociation of excitons and accelerate the transfer of charges owing to the negatively charged functional groups on the surface of BNQDs as well as the ultrathin and porous nanostructure of g-C3N4. Benefiting from the intensified exciton dissociation and charge transfer, the BNQDs/UPCN (BU) photocatalyst presented superior visible-light-driven molecular oxygen activation ability, such as superoxide radical (O2−) generation and hydrogen peroxide (H2O2) production. The average O2− generation rate of the optimal sample (BU-3) was estimated to be 0.25 μmol L−1 min−1, which was about 2.3 and 1.6 times than that of bulk g-C3N4 and UPCN. Moreover, the H2O2 production by BU-3 was also higher than that of bulk g-C3N4 (22.77 μmol L−1) and UPCN (36.13 μmol L−1), and reached 72.30 μmol L−1 over 60 min. This work reveals how rational combination of g-C3N4 with BNQDs can endow it with improved photocatalytic activity for molecular oxygen activation, and provides a novel metal-free and highly efficient photocatalyst for environmental remediation and energy conversion. |
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| AbstractList | [Display omitted]
•A novel photocatalyst constructed by BNQDs and UPCN was prepared.•Intensified exciton dissociation and charge transfer across BNQDs/UPCN heterostructure.•Higher photocatalytic efficiency toward molecular oxygen activation under visible light.•Mechanisms of enhanced photocatalytic activities were proposed.
Graphitic carbon nitride (g-C3N4) has enormous potential for photocatalysis, but only possesses moderate activity because of excitonic effects and sluggish charge transfer. Herein, metal-free heterostructure photocatalyst constructed by boron nitride quantum dots (BNQDs) and ultrathin porous g-C3N4 (UPCN) was successfully developed for overcoming these defects. Results showed that the BNQDs loaded UPCN can simultaneously promote the dissociation of excitons and accelerate the transfer of charges owing to the negatively charged functional groups on the surface of BNQDs as well as the ultrathin and porous nanostructure of g-C3N4. Benefiting from the intensified exciton dissociation and charge transfer, the BNQDs/UPCN (BU) photocatalyst presented superior visible-light-driven molecular oxygen activation ability, such as superoxide radical (O2−) generation and hydrogen peroxide (H2O2) production. The average O2− generation rate of the optimal sample (BU-3) was estimated to be 0.25 μmol L−1 min−1, which was about 2.3 and 1.6 times than that of bulk g-C3N4 and UPCN. Moreover, the H2O2 production by BU-3 was also higher than that of bulk g-C3N4 (22.77 μmol L−1) and UPCN (36.13 μmol L−1), and reached 72.30 μmol L−1 over 60 min. This work reveals how rational combination of g-C3N4 with BNQDs can endow it with improved photocatalytic activity for molecular oxygen activation, and provides a novel metal-free and highly efficient photocatalyst for environmental remediation and energy conversion. Graphitic carbon nitride (g-C3N4) has enormous potential for photocatalysis, but only possesses moderate activity because of excitonic effects and sluggish charge transfer. Herein, metal-free heterostructure photocatalyst constructed by boron nitride quantum dots (BNQDs) and ultrathin porous g-C3N4 (UPCN) was successfully developed for overcoming these defects. Results showed that the BNQDs loaded UPCN can simultaneously promote the dissociation of excitons and accelerate the transfer of charges owing to the negatively charged functional groups on the surface of BNQDs as well as the ultrathin and porous nanostructure of g-C3N4. Benefiting from the intensified exciton dissociation and charge transfer, the BNQDs/UPCN (BU) photocatalyst presented superior visible-light-driven molecular oxygen activation ability, such as superoxide radical (O2−) generation and hydrogen peroxide (H2O2) production. The average O2− generation rate of the optimal sample (BU-3) was estimated to be 0.25 μmol L−1 min−1, which was about 2.3 and 1.6 times than that of bulk g-C3N4 and UPCN. Moreover, the H2O2 production by BU-3 was also higher than that of bulk g-C3N4 (22.77 μmol L−1) and UPCN (36.13 μmol L−1), and reached 72.30 μmol L−1 over 60 min. This work reveals how rational combination of g-C3N4 with BNQDs can endow it with improved photocatalytic activity for molecular oxygen activation, and provides a novel metal-free and highly efficient photocatalyst for environmental remediation and energy conversion. |
| Author | Huang, Danlian Zhang, Chen Huang, Jinhui Deng, Rui Guo, Hai Wang, Wenjun Xue, Wenjing Yang, Yang Cheng, Min Xiong, Weiping Lai, Cui Zeng, Guangming Zhou, Chengyun |
| Author_xml | – sequence: 1 givenname: Yang surname: Yang fullname: Yang, Yang organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, PR China – sequence: 2 givenname: Chen orcidid: 0000-0002-3579-6980 surname: Zhang fullname: Zhang, Chen organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, PR China – sequence: 3 givenname: Danlian surname: Huang fullname: Huang, Danlian organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, PR China – sequence: 4 givenname: Guangming orcidid: 0000-0002-4230-7647 surname: Zeng fullname: Zeng, Guangming email: zgming@hnu.edu.cn organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, PR China – sequence: 5 givenname: Jinhui surname: Huang fullname: Huang, Jinhui email: jinhui@hnu.edu.cn organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, PR China – sequence: 6 givenname: Cui surname: Lai fullname: Lai, Cui organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, PR China – sequence: 7 givenname: Chengyun surname: Zhou fullname: Zhou, Chengyun organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, PR China – sequence: 8 givenname: Wenjun surname: Wang fullname: Wang, Wenjun organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, PR China – sequence: 9 givenname: Hai surname: Guo fullname: Guo, Hai organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, PR China – sequence: 10 givenname: Wenjing surname: Xue fullname: Xue, Wenjing organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, PR China – sequence: 11 givenname: Rui surname: Deng fullname: Deng, Rui organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, PR China – sequence: 12 givenname: Min surname: Cheng fullname: Cheng, Min organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, PR China – sequence: 13 givenname: Weiping surname: Xiong fullname: Xiong, Weiping organization: College of Environmental Science and Engineering, Hunan University, Changsha, 410082, PR China |
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| ContentType | Journal Article |
| Copyright | 2018 Elsevier B.V. Copyright Elsevier BV May 15, 2019 |
| Copyright_xml | – notice: 2018 Elsevier B.V. – notice: Copyright Elsevier BV May 15, 2019 |
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| DOI | 10.1016/j.apcatb.2018.12.049 |
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| DatabaseTitleList | Materials Research Database |
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| Discipline | Engineering Chemistry Environmental Sciences |
| EISSN | 1873-3883 |
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•A novel photocatalyst constructed by BNQDs and UPCN was prepared.•Intensified exciton dissociation and charge transfer across BNQDs/UPCN... Graphitic carbon nitride (g-C3N4) has enormous potential for photocatalysis, but only possesses moderate activity because of excitonic effects and sluggish... |
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| SubjectTerms | Activation Boron Boron nitride Boron nitride quantum dots Carbon nitride Catalytic activity Charge transfer Energy conversion Environmental cleanup Exciton dissociation Excitons Functional groups H2O2 production Heterostructures Hydrogen peroxide Oxygen Photocatalysis Photocatalysts Photocatalytic molecular oxygen activation Quantum dots Superoxide Ultrathin porous g-C3N4 |
| Title | Boron nitride quantum dots decorated ultrathin porous g-C3N4: Intensified exciton dissociation and charge transfer for promoting visible-light-driven molecular oxygen activation |
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