Measuring the viscosity of films by thermomechanical analysis: application to metal organic precursor films of functional oxides
We have developed a new method to measure the viscosity of micrometric films by thermomechanical analysis with a hemispherical probe of millimetric diameter. The loading curve (displacement vs. time) recorded as the probe tip crosses the whole film at constant load until it touches the substrate is...
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Published in | Journal of thermal analysis and calorimetry Vol. 148; no. 9; pp. 3427 - 3438 |
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Main Authors | , , , , , , |
Format | Journal Article |
Language | English |
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01.05.2023
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Abstract | We have developed a new method to measure the viscosity of micrometric films by thermomechanical analysis with a hemispherical probe of millimetric diameter. The loading curve (displacement vs. time) recorded as the probe tip crosses the whole film at constant load until it touches the substrate is fitted to a theoretical curve shape that has been obtained after solving the problem of liquid flow under the probe tip. The method has been validated by measuring the viscosity of rosin films. It has been applied to analyze the thermal evolution of unstable liquid films that appear on Ba propionate, Ce(III) propionate and a low-fluorine precursor film of YBa
2
Cu
3
O
6+x
. During pyrolysis of the last two films, viscosity first diminishes due to heating and then it increases as solid oxide particles are formed inside the liquid. |
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AbstractList | We have developed a new method to measure the viscosity of micrometric films by thermomechanical analysis with a hemispherical probe of millimetric diameter. The loading curve (displacement vs. time) recorded as the probe tip crosses the whole film at constant load until it touches the substrate is fitted to a theoretical curve shape that has been obtained after solving the problem of liquid flow under the probe tip. The method has been validated by measuring the viscosity of rosin films. It has been applied to analyze the thermal evolution of unstable liquid films that appear on Ba propionate, Ce(III) propionate and a low-fluorine precursor film of YBa
2
Cu
3
O
6+x
. During pyrolysis of the last two films, viscosity first diminishes due to heating and then it increases as solid oxide particles are formed inside the liquid. We have developed a new method to measure the viscosity of micrometric films by thermomechanical analysis with a hemispherical probe of millimetric diameter. The loading curve (displacement vs. time) recorded as the probe tip crosses the whole film at constant load until it touches the substrate is fitted to a theoretical curve shape that has been obtained after solving the problem of liquid flow under the probe tip. The method has been validated by measuring the viscosity of rosin films. It has been applied to analyze the thermal evolution of unstable liquid films that appear on Ba propionate, Ce(III) propionate and a low-fluorine precursor film of YBa2Cu3O6+x. During pyrolysis of the last two films, viscosity first diminishes due to heating and then it increases as solid oxide particles are formed inside the liquid. We have developed a new method to measure the viscosity of micrometric films by thermomechanical analysis with a hemispherical probe of millimetric diameter. The loading curve (displacement vs. time) recorded as the probe tip crosses the whole film at constant load until it touches the substrate is fitted to a theoretical curve shape that has been obtained after solving the problem of liquid flow under the probe tip. The method has been validated by measuring the viscosity of rosin films. It has been applied to analyze the thermal evolution of unstable liquid films that appear on Ba propionate, Ce(III) propionate and a low-fluorine precursor film of YBa.sub.2Cu.sub.3O.sub.6+x. During pyrolysis of the last two films, viscosity first diminishes due to heating and then it increases as solid oxide particles are formed inside the liquid. Abstract We have developed a new method to measure the viscosity of micrometric films by thermomechanical analysis with a hemispherical probe of millimetric diameter. The loading curve (displacement vs. time) recorded as the probe tip crosses the whole film at constant load until it touches the substrate is fitted to a theoretical curve shape that has been obtained after solving the problem of liquid flow under the probe tip. The method has been validated by measuring the viscosity of rosin films. It has been applied to analyze the thermal evolution of unstable liquid films that appear on Ba propionate, Ce(III) propionate and a low-fluorine precursor film of YBa 2 Cu 3 O 6+x . During pyrolysis of the last two films, viscosity first diminishes due to heating and then it increases as solid oxide particles are formed inside the liquid. |
Audience | Academic |
Author | Puig, Teresa Farjas, Jordi Villarejo, Bohores Obradors, Xavier Roura-Grabulosa, Pere López-Olmedo, Joan Pere Ricart, Susagna |
Author_xml | – sequence: 1 givenname: Pere orcidid: 0000-0003-4964-1362 surname: Roura-Grabulosa fullname: Roura-Grabulosa, Pere email: pere.roura@udg.cat organization: GRMT, Department of Physics, University of Girona – sequence: 2 givenname: Jordi surname: Farjas fullname: Farjas, Jordi organization: GRMT, Department of Physics, University of Girona – sequence: 3 givenname: Joan Pere surname: López-Olmedo fullname: López-Olmedo, Joan Pere organization: Unitat d’Anàlisi Tèrmica (STR), University of Girona – sequence: 4 givenname: Bohores surname: Villarejo fullname: Villarejo, Bohores organization: Institut de Ciència de Materials de Barcelona, ICMAB – CSIC – sequence: 5 givenname: Susagna surname: Ricart fullname: Ricart, Susagna organization: Institut de Ciència de Materials de Barcelona, ICMAB – CSIC – sequence: 6 givenname: Xavier surname: Obradors fullname: Obradors, Xavier organization: Institut de Ciència de Materials de Barcelona, ICMAB – CSIC – sequence: 7 givenname: Teresa surname: Puig fullname: Puig, Teresa organization: Institut de Ciència de Materials de Barcelona, ICMAB – CSIC |
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Keywords | Viscosity Thin films Pyrolysis TMA YBCO Functional oxides |
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Snippet | We have developed a new method to measure the viscosity of micrometric films by thermomechanical analysis with a hemispherical probe of millimetric diameter.... Abstract We have developed a new method to measure the viscosity of micrometric films by thermomechanical analysis with a hemispherical probe of millimetric... |
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SubjectTerms | Analytical Chemistry Chemistry Chemistry and Materials Science Diameters Fluorine Inorganic Chemistry Liquid flow Measurement Measurement Science and Instrumentation Oxides Physical Chemistry Polymer Sciences Precursors Pyrolysis Rosin Substrates Thermal evolution Thermomechanical analysis Viscosity |
Title | Measuring the viscosity of films by thermomechanical analysis: application to metal organic precursor films of functional oxides |
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