Crude glycerol-mediated liquefaction of empty fruit bunches saccharification residues for preparation of biopolyurethane

•Empty fruit bunches residue was liquefied to prepare biopolyol using crude glycerol.•Hydroxyl number of the biopolyol was 1649.3mg KOH/g.•The biomass conversion at the optimal conditions was 71.3%.•The biopolyol was a suitable monomer for biopolyurethane synthesis. In order to utilize lignin residu...

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Published inJournal of industrial and engineering chemistry (Seoul, Korea) Vol. 34; pp. 157 - 164
Main Authors Lee, Ju-Hee, Lee, Jae Hoon, Kim, Duk-Ki, Park, Chang-Ho, Yu, Ju-Hyun, Lee, Eun Yeol
Format Journal Article
LanguageEnglish
Published Elsevier B.V 25.02.2016
한국공업화학회
Subjects
Biomass
Crude glycerol
Empty fruit bunch
Fourier transforms
Fruits
Glycerols
Infrared spectroscopy
Lignol
Liquefaction
Optimization
Polyurethane
Residues
화학공학
Lignol
Crude glycerol
Empty fruit bunch
Liquefaction
Polyurethane
Online AccessGet full text
ISSN1226-086X
1876-794X
DOI10.1016/j.jiec.2015.11.007

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Abstract •Empty fruit bunches residue was liquefied to prepare biopolyol using crude glycerol.•Hydroxyl number of the biopolyol was 1649.3mg KOH/g.•The biomass conversion at the optimal conditions was 71.3%.•The biopolyol was a suitable monomer for biopolyurethane synthesis. In order to utilize lignin residue from the pretreatment of empty fruit bunch (EFB) and crude glycerol from biodiesel production, lignin residue was solvothermally liquefied using crude glycerol to produce lignol. The optimal liquefaction conditions for lignol production were determined to be 10% biomass loading, 5% acid loading, a liquefaction temperature of 170°C, and a liquefaction time of 120min. The biomass conversion at the optimal conditions was 47.9%. The lignols possess hydroxyl number of 1649.3mg KOH/g and acid number of 8.4mg KOH/g. Fourier transform infrared spectroscopy revealed that the lignol was suitable for biopolyurethane synthesis.
AbstractList •Empty fruit bunches residue was liquefied to prepare biopolyol using crude glycerol.•Hydroxyl number of the biopolyol was 1649.3mg KOH/g.•The biomass conversion at the optimal conditions was 71.3%.•The biopolyol was a suitable monomer for biopolyurethane synthesis. In order to utilize lignin residue from the pretreatment of empty fruit bunch (EFB) and crude glycerol from biodiesel production, lignin residue was solvothermally liquefied using crude glycerol to produce lignol. The optimal liquefaction conditions for lignol production were determined to be 10% biomass loading, 5% acid loading, a liquefaction temperature of 170°C, and a liquefaction time of 120min. The biomass conversion at the optimal conditions was 47.9%. The lignols possess hydroxyl number of 1649.3mg KOH/g and acid number of 8.4mg KOH/g. Fourier transform infrared spectroscopy revealed that the lignol was suitable for biopolyurethane synthesis.
In order to utilize lignin residue from the pretreatment of empty fruit bunch (EFB) and crude glycerolfrom biodiesel production, lignin residue was solvothermally liquefied using crude glycerol to producelignol. The optimal liquefaction conditions for lignol production were determined to be 10% biomassloading, 5% acid loading, a liquefaction temperature of 170 8C, and a liquefaction time of 120 min. Thebiomass conversion at the optimal conditions was 47.9%. The lignols possess hydroxyl number of1649.3 mg KOH/g and acid number of 8.4 mg KOH/g. Fourier transform infrared spectroscopy revealedthat the lignol was suitable for biopolyurethane synthesis. KCI Citation Count: 22
In order to utilize lignin residue from the pretreatment of empty fruit bunch (EFB) and crude glycerol from biodiesel production, lignin residue was solvothermally liquefied using crude glycerol to produce lignol. The optimal liquefaction conditions for lignol production were determined to be 10% biomass loading, 5% acid loading, a liquefaction temperature of 170 degree C, and a liquefaction time of 120 min. The biomass conversion at the optimal conditions was 47.9%. The lignols possess hydroxyl number of 1649.3 mg KOH/g and acid number of 8.4 mg KOH/g. Fourier transform infrared spectroscopy revealed that the lignol was suitable for biopolyurethane synthesis.
Author Lee, Ju-Hee
Yu, Ju-Hyun
Park, Chang-Ho
Lee, Eun Yeol
Kim, Duk-Ki
Lee, Jae Hoon
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  givenname: Ju-Hyun
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  email: jhyu@krict.re.kr
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  givenname: Eun Yeol
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  fullname: Lee, Eun Yeol
  email: eunylee@khu.ac.kr
  organization: Department of Chemical Engineering, Kyung Hee University, Gyeonggi-do 446-701, Republic of Korea
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Keywords Lignol
Crude glycerol
Empty fruit bunch
Liquefaction
Polyurethane
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Snippet •Empty fruit bunches residue was liquefied to prepare biopolyol using crude glycerol.•Hydroxyl number of the biopolyol was 1649.3mg KOH/g.•The biomass...
In order to utilize lignin residue from the pretreatment of empty fruit bunch (EFB) and crude glycerol from biodiesel production, lignin residue was...
In order to utilize lignin residue from the pretreatment of empty fruit bunch (EFB) and crude glycerolfrom biodiesel production, lignin residue was...
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SubjectTerms Biomass
Crude glycerol
Empty fruit bunch
Fourier transforms
Fruits
Glycerols
Infrared spectroscopy
Lignol
Liquefaction
Optimization
Polyurethane
Residues
화학공학
Title Crude glycerol-mediated liquefaction of empty fruit bunches saccharification residues for preparation of biopolyurethane
URI https://dx.doi.org/10.1016/j.jiec.2015.11.007
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