Construction of hierarchically porous monoliths from covalent organic frameworks (COFs) and their application for bisphenol A removal
[Display omitted] •A method is developed to shape COF powder into monoliths.•The crystallinity and micropore of COF in monolith are well remained.•COF-based monoliths feature a hierarchically porous structure.•COF-based monoliths exhibit good removal performance for bisphenol A. Subject to synthetic...
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| Published in | Journal of hazardous materials Vol. 355; pp. 145 - 153 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Netherlands
Elsevier B.V
05.08.2018
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| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
•A method is developed to shape COF powder into monoliths.•The crystallinity and micropore of COF in monolith are well remained.•COF-based monoliths feature a hierarchically porous structure.•COF-based monoliths exhibit good removal performance for bisphenol A.
Subject to synthetic conditions, covalent organic frameworks (COFs) are usually in powder form. Herein, taking an azine-linked COF as an example, detailed characterizations indicated that accessible aldehyde groups and hydrazine groups (CNNH2, 88 μmol g−1) concurrently existed on its surface. Intrigued by such feature, we have developed an approach based on ring-opening polymerization to shape COF powder into monoliths. The crystallinity and micropore of COF in monoliths were well remained, meanwhile, the ring-opening polymerization remarkably generated macropores ranging from 0.43 to 3.51 μm, indicating a hierarchically porous structure. The BET surface area of resultant monoliths with different COF mass fractions of 16%, 28% and 43% ranged from 105 to 281 m2 g−1. Due to the π–π interaction and hydrogen bond interaction, COF-based monoliths exhibited strong retention and rapid adsorption for bisphenol A (BPA) in aqueous medium. When 29 mL BPA solution (22.8 mg L−1) passed through COF-based monolith (28%), the adsorption capacity was up to 61.3 mg g−1. Furthermore, the COF-based monolith demonstrated excellent cycle use for catalyzing Suzuki-Miyaura coupling reaction after being coordinated with palladium acetate. |
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| AbstractList | Subject to synthetic conditions, covalent organic frameworks (COFs) are usually in powder form. Herein, taking an azine-linked COF as an example, detailed characterizations indicated that accessible aldehyde groups and hydrazine groups (CNNH2, 88 μmol g-1) concurrently existed on its surface. Intrigued by such feature, we have developed an approach based on ring-opening polymerization to shape COF powder into monoliths. The crystallinity and micropore of COF in monoliths were well remained, meanwhile, the ring-opening polymerization remarkably generated macropores ranging from 0.43 to 3.51 μm, indicating a hierarchically porous structure. The BET surface area of resultant monoliths with different COF mass fractions of 16%, 28% and 43% ranged from 105 to 281 m2 g-1. Due to the π-π interaction and hydrogen bond interaction, COF-based monoliths exhibited strong retention and rapid adsorption for bisphenol A (BPA) in aqueous medium. When 29 mL BPA solution (22.8 mg L-1) passed through COF-based monolith (28%), the adsorption capacity was up to 61.3 mg g-1. Furthermore, the COF-based monolith demonstrated excellent cycle use for catalyzing Suzuki-Miyaura coupling reaction after being coordinated with palladium acetate.Subject to synthetic conditions, covalent organic frameworks (COFs) are usually in powder form. Herein, taking an azine-linked COF as an example, detailed characterizations indicated that accessible aldehyde groups and hydrazine groups (CNNH2, 88 μmol g-1) concurrently existed on its surface. Intrigued by such feature, we have developed an approach based on ring-opening polymerization to shape COF powder into monoliths. The crystallinity and micropore of COF in monoliths were well remained, meanwhile, the ring-opening polymerization remarkably generated macropores ranging from 0.43 to 3.51 μm, indicating a hierarchically porous structure. The BET surface area of resultant monoliths with different COF mass fractions of 16%, 28% and 43% ranged from 105 to 281 m2 g-1. Due to the π-π interaction and hydrogen bond interaction, COF-based monoliths exhibited strong retention and rapid adsorption for bisphenol A (BPA) in aqueous medium. When 29 mL BPA solution (22.8 mg L-1) passed through COF-based monolith (28%), the adsorption capacity was up to 61.3 mg g-1. Furthermore, the COF-based monolith demonstrated excellent cycle use for catalyzing Suzuki-Miyaura coupling reaction after being coordinated with palladium acetate. Subject to synthetic conditions, covalent organic frameworks (COFs) are usually in powder form. Herein, taking an azine-linked COF as an example, detailed characterizations indicated that accessible aldehyde groups and hydrazine groups (CNNH₂, 88 μmol g⁻¹) concurrently existed on its surface. Intrigued by such feature, we have developed an approach based on ring-opening polymerization to shape COF powder into monoliths. The crystallinity and micropore of COF in monoliths were well remained, meanwhile, the ring-opening polymerization remarkably generated macropores ranging from 0.43 to 3.51 μm, indicating a hierarchically porous structure. The BET surface area of resultant monoliths with different COF mass fractions of 16%, 28% and 43% ranged from 105 to 281 m² g⁻¹. Due to the π–π interaction and hydrogen bond interaction, COF-based monoliths exhibited strong retention and rapid adsorption for bisphenol A (BPA) in aqueous medium. When 29 mL BPA solution (22.8 mg L⁻¹) passed through COF-based monolith (28%), the adsorption capacity was up to 61.3 mg g⁻¹. Furthermore, the COF-based monolith demonstrated excellent cycle use for catalyzing Suzuki-Miyaura coupling reaction after being coordinated with palladium acetate. Subject to synthetic conditions, covalent organic frameworks (COFs) are usually in powder form. Herein, taking an azine-linked COF as an example, detailed characterizations indicated that accessible aldehyde groups and hydrazine groups (CNNH , 88 μmol g ) concurrently existed on its surface. Intrigued by such feature, we have developed an approach based on ring-opening polymerization to shape COF powder into monoliths. The crystallinity and micropore of COF in monoliths were well remained, meanwhile, the ring-opening polymerization remarkably generated macropores ranging from 0.43 to 3.51 μm, indicating a hierarchically porous structure. The BET surface area of resultant monoliths with different COF mass fractions of 16%, 28% and 43% ranged from 105 to 281 m g . Due to the π-π interaction and hydrogen bond interaction, COF-based monoliths exhibited strong retention and rapid adsorption for bisphenol A (BPA) in aqueous medium. When 29 mL BPA solution (22.8 mg L ) passed through COF-based monolith (28%), the adsorption capacity was up to 61.3 mg g . Furthermore, the COF-based monolith demonstrated excellent cycle use for catalyzing Suzuki-Miyaura coupling reaction after being coordinated with palladium acetate. [Display omitted] •A method is developed to shape COF powder into monoliths.•The crystallinity and micropore of COF in monolith are well remained.•COF-based monoliths feature a hierarchically porous structure.•COF-based monoliths exhibit good removal performance for bisphenol A. Subject to synthetic conditions, covalent organic frameworks (COFs) are usually in powder form. Herein, taking an azine-linked COF as an example, detailed characterizations indicated that accessible aldehyde groups and hydrazine groups (CNNH2, 88 μmol g−1) concurrently existed on its surface. Intrigued by such feature, we have developed an approach based on ring-opening polymerization to shape COF powder into monoliths. The crystallinity and micropore of COF in monoliths were well remained, meanwhile, the ring-opening polymerization remarkably generated macropores ranging from 0.43 to 3.51 μm, indicating a hierarchically porous structure. The BET surface area of resultant monoliths with different COF mass fractions of 16%, 28% and 43% ranged from 105 to 281 m2 g−1. Due to the π–π interaction and hydrogen bond interaction, COF-based monoliths exhibited strong retention and rapid adsorption for bisphenol A (BPA) in aqueous medium. When 29 mL BPA solution (22.8 mg L−1) passed through COF-based monolith (28%), the adsorption capacity was up to 61.3 mg g−1. Furthermore, the COF-based monolith demonstrated excellent cycle use for catalyzing Suzuki-Miyaura coupling reaction after being coordinated with palladium acetate. |
| Author | Chen, Lianfang Ou, Junjie Ye, Mingliang Liu, Zhongshan Wang, Hongwei |
| Author_xml | – sequence: 1 givenname: Zhongshan surname: Liu fullname: Liu, Zhongshan organization: Key Laboratory of Separation Science for Analytical Chemistry, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023, China – sequence: 2 givenname: Hongwei surname: Wang fullname: Wang, Hongwei organization: Key Laboratory of Separation Science for Analytical Chemistry, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023, China – sequence: 3 givenname: Junjie surname: Ou fullname: Ou, Junjie email: junjieou@dicp.ac.cn organization: Key Laboratory of Separation Science for Analytical Chemistry, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023, China – sequence: 4 givenname: Lianfang surname: Chen fullname: Chen, Lianfang organization: Key Laboratory of Separation Science for Analytical Chemistry, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023, China – sequence: 5 givenname: Mingliang surname: Ye fullname: Ye, Mingliang email: mingliang@dicp.ac.cn organization: Key Laboratory of Separation Science for Analytical Chemistry, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023, China |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/29783155$$D View this record in MEDLINE/PubMed |
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| Keywords | Covalent organic framework Hierarchically porous monolith Ring-opening polymerization Bisphenol A removal Hydrazine |
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•A method is developed to shape COF powder into monoliths.•The crystallinity and micropore of COF in monolith are well remained.•COF-based... Subject to synthetic conditions, covalent organic frameworks (COFs) are usually in powder form. Herein, taking an azine-linked COF as an example, detailed... |
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| SubjectTerms | acetates adsorption aldehydes bisphenol A Bisphenol A removal Covalent organic framework crystal structure Hierarchically porous monolith Hydrazine hydrogen bonding macropores palladium polymerization Ring-opening polymerization surface area Suzuki reaction |
| Title | Construction of hierarchically porous monoliths from covalent organic frameworks (COFs) and their application for bisphenol A removal |
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