Effect of loading content of copper oxides on performance of Mn-Cu mixed oxide catalysts for catalytic combustion of benzene
A series of Mn-Cu mixed oxide catalysts were prepared by precipitation method. The catalysts were characterized by N2 adsorp- tion-desorption, H2-TPR and XPS. When the loading ratio of manganese oxides to copper oxides was 8：2 or 7：3, the catalysts possessed better catalytic activity, and benzene wa...
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| Published in | Journal of rare earths Vol. 30; no. 9; pp. 871 - 877 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
01.09.2012
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| Online Access | Get full text |
| ISSN | 1002-0721 2509-4963 |
| DOI | 10.1016/S1002-0721(12)60148-3 |
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| Abstract | A series of Mn-Cu mixed oxide catalysts were prepared by precipitation method. The catalysts were characterized by N2 adsorp- tion-desorption, H2-TPR and XPS. When the loading ratio of manganese oxides to copper oxides was 8：2 or 7：3, the catalysts possessed better catalytic activity, and benzene was converted completely at 558 K. Results of H2-TPR showed that the loading of a small amount of copper oxides decreased the reduction temperature of catalysts. Results of XPS showed that the loading of a small amount of copper oxides increased the proportion of manganese and defective oxygen on the surface of catalysts, and stabilized manganese at higher oxidation state. And the catalyst with the loading ratio 7：3 was a little worse than 8：2, since the interaction between manganese oxides and copper oxides is too strong, copper oxides migrate to the surface of catalysts and manganese oxides in excess are immerged. |
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| AbstractList | A series of Mn-Cu mixed oxide catalysts were prepared by precipitation method. The catalysts were characterized by N2 adsorp- tion-desorption, H2-TPR and XPS. When the loading ratio of manganese oxides to copper oxides was 8：2 or 7：3, the catalysts possessed better catalytic activity, and benzene was converted completely at 558 K. Results of H2-TPR showed that the loading of a small amount of copper oxides decreased the reduction temperature of catalysts. Results of XPS showed that the loading of a small amount of copper oxides increased the proportion of manganese and defective oxygen on the surface of catalysts, and stabilized manganese at higher oxidation state. And the catalyst with the loading ratio 7：3 was a little worse than 8：2, since the interaction between manganese oxides and copper oxides is too strong, copper oxides migrate to the surface of catalysts and manganese oxides in excess are immerged. A series of Mn-Cu mixed oxide catalysts were prepared by precipitation method. The catalysts were characterized by N(2) adsorp-tion-desorption, H(2)-TPR and XPS. When the loading ratio of manganese oxides to copper oxides was 8: 2 or 7: 3, the catalysts possessed better catalytic activity, and benzene was converted completely at 558 K. Results of H(2)-TPR showed that the loading of a small amount of copper oxides decreased the reduction temperature of catalysts. Results of XPS showed that the loading of a small amount of copper oxides increased the proportion of manganese and defective oxygen on the surface of catalysts, and stabilized manganese at higher oxidation state. And the catalyst with the loading ratio 7: 3 was a little worse than 8: 2, since the interaction between manganese oxides and copper oxides is too strong, copper oxides migrate to the surface of catalysts and manganese oxides in excess are immerged. A series of Mn-Cu mixed oxide catalysts were prepared by precipitation method. The catalysts were characterized by N2 adsorption-desorption, H2-TPR and XPS. When the loading ratio of manganese oxides to copper oxides was 8:2 or 7:3, the catalysts possessed better catalytic activity, and benzene was converted completely at 558 K. Results of H2-TPR showed that the loading of a small amount of copper oxides decreased the reduction temperature of catalysts. Results of XPS showed that the loading of a small amount of copper oxides increased the proportion of manganese and defective oxygen on the surface of catalysts, and stabilized manganese at higher oxidation state. And the catalyst with the loading ratio 7:3 was a little worse than 8:2, since the interaction between manganese oxides and copper oxides is too strong, copper oxides migrate to the surface of catalysts and manganese oxides in excess are immerged. |
| Author | CAO Hongyan LI Xiaoshuang CHEN Yaoqiang GONG Maochu WANG Jianli |
| AuthorAffiliation | Key Laboratory of Green Chemistry ＆ Technology of Ministry of Education, College of Chemistry, Sichuan University, Chengdu 610064, China |
| Author_xml | – sequence: 1 givenname: Hongyan surname: CAO fullname: CAO, Hongyan – sequence: 2 givenname: Xiaoshuang surname: LI fullname: LI, Xiaoshuang – sequence: 3 givenname: Yaoqiang surname: CHEN fullname: CHEN, Yaoqiang – sequence: 4 givenname: Maochu surname: GONG fullname: GONG, Maochu – sequence: 5 givenname: Jianli surname: WANG fullname: WANG, Jianli email: wangjianli@scu.edu.cn |
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| Keywords | catalytic combustion Mn-Cu mixed oxide catalysts benzene rare earths |
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| Notes | Mn-Cu mixed oxide catalysts; catalytic combustion; benzene; rare earths A series of Mn-Cu mixed oxide catalysts were prepared by precipitation method. The catalysts were characterized by N2 adsorp- tion-desorption, H2-TPR and XPS. When the loading ratio of manganese oxides to copper oxides was 8：2 or 7：3, the catalysts possessed better catalytic activity, and benzene was converted completely at 558 K. Results of H2-TPR showed that the loading of a small amount of copper oxides decreased the reduction temperature of catalysts. Results of XPS showed that the loading of a small amount of copper oxides increased the proportion of manganese and defective oxygen on the surface of catalysts, and stabilized manganese at higher oxidation state. And the catalyst with the loading ratio 7：3 was a little worse than 8：2, since the interaction between manganese oxides and copper oxides is too strong, copper oxides migrate to the surface of catalysts and manganese oxides in excess are immerged. 11-2788/TF ObjectType-Article-2 SourceType-Scholarly Journals-1 ObjectType-Feature-1 content type line 23 |
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| Snippet | A series of Mn-Cu mixed oxide catalysts were prepared by precipitation method. The catalysts were characterized by N2 adsorp- tion-desorption, H2-TPR and XPS.... A series of Mn-Cu mixed oxide catalysts were prepared by precipitation method. The catalysts were characterized by N2 adsorption-desorption, H2-TPR and XPS.... A series of Mn-Cu mixed oxide catalysts were prepared by precipitation method. The catalysts were characterized by N(2) adsorp-tion-desorption, H(2)-TPR and... |
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| SubjectTerms | Benzene Catalysis CATALYSTS catalytic combustion COMBUSTION COPPER OXIDE Copper oxides Manganese Manganese oxides Mn-Cu mixed oxide catalysts OXIDES Rare earth metals rare earths X RAY SPECTROSCOPY X-ray photoelectron spectroscopy 催化剂性能 催化燃烧 加载 复合氧化物催化剂 氧化铜催化剂 铜复合氧化物 铜氧化物 锰铜 |
| Title | Effect of loading content of copper oxides on performance of Mn-Cu mixed oxide catalysts for catalytic combustion of benzene |
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