Citrate sol-gel combustion preparation and photoluminescence properties of YAG：Ce phosphors
Yellow-emitting YAG：Ce3＋ nanocrystalline phosphors were prepared by citrate sol-gel combustion method using citric acid as the fuel and chelating agent. The influence of mole ratio of citric acid to metallic ions （MRCM）, pH value of the solution, calcination temperature and Ce-doped concentration on...
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| Published in | Journal of rare earths Vol. 30; no. 4; pp. 289 - 296 |
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| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.04.2012
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| Subjects | |
| Online Access | Get full text |
| ISSN | 1002-0721 2509-4963 |
| DOI | 10.1016/S1002-0721(12)60040-4 |
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| Abstract | Yellow-emitting YAG：Ce3＋ nanocrystalline phosphors were prepared by citrate sol-gel combustion method using citric acid as the fuel and chelating agent. The influence of mole ratio of citric acid to metallic ions （MRCM）, pH value of the solution, calcination temperature and Ce-doped concentration on the structures and properties of as-prepared powders were investigated in detail. Higher crystallinity and better luminescence performance powders were obtained at MRCM=2, pH=3 and the calcination temperature of 1200 ℃. The phosphors exhibited the charactefistc broadband visible luminescence of YAG：Ce. The optimum concentration of Ce3＋ was 1.0 tool.%, and the concentration quenching was derived from the reciprocity between electric dipole and electric quadrupole （d-q）. Especially, the pH value of the solution was a key factor to obtain a stable sol-gel system and then obtain pure and homogeneous rare earth ions doped YAG phosphors at a lower tem- perature. The Y3Al5O12：Ce0.03 phosphor with optimized synthesis-condition and composition had a similar luminescence intensity with the commercial phosphor YAG：Ce. |
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| AbstractList | Yellow-emitting YAG: Ce3+ nanocrystalline phosphors were prepared by citrate sol-gel combustion method using citric acid as the fuel and chelating agent. The influence of mole ratio of citric acid to metallic ions (MRCM), pH value of the solution, calcination temperature and Ce-doped concentration on the structures and properties of as-prepared powders were investigated in detail. Higher crystallinity and better luminescence performance powders were obtained at MRCM=2, pH=3 and the calcination temperature of 1200 [deg]C. The phosphors exhibited the characteristic broadband visible luminescence of YAG: Ce. The optimum concentration of Ce3+ was 1.0 mol.%, and the concentration quenching was derived from the reciprocity between electric dipole and electric quadrupole (d-q). Especially, the pH value of the solution was a key factor to obtain a stable sol-gel system and then obtain pure and homogeneous rare earth ions doped YAG phosphors at a lower temperature. The Y3Al5O12: Ce0.03 phosphor with optimized synthesis-condition and composition had a similar luminescence intensity with the commercial phosphor YAG: Ce. Yellow-emitting YAG：Ce3＋ nanocrystalline phosphors were prepared by citrate sol-gel combustion method using citric acid as the fuel and chelating agent. The influence of mole ratio of citric acid to metallic ions （MRCM）, pH value of the solution, calcination temperature and Ce-doped concentration on the structures and properties of as-prepared powders were investigated in detail. Higher crystallinity and better luminescence performance powders were obtained at MRCM=2, pH=3 and the calcination temperature of 1200 ℃. The phosphors exhibited the charactefistc broadband visible luminescence of YAG：Ce. The optimum concentration of Ce3＋ was 1.0 tool.%, and the concentration quenching was derived from the reciprocity between electric dipole and electric quadrupole （d-q）. Especially, the pH value of the solution was a key factor to obtain a stable sol-gel system and then obtain pure and homogeneous rare earth ions doped YAG phosphors at a lower tem- perature. The Y3Al5O12：Ce0.03 phosphor with optimized synthesis-condition and composition had a similar luminescence intensity with the commercial phosphor YAG：Ce. Yellow-emitting YAG:Ce3+ nanocrystalline phosphors were prepared by citrate sol-gel combustion method using citric acid as the fuel and chelating agent. The influence of mole ratio of citric acid to metallic ions (MRCM), pH value of the solution, calcination temperature and Ce-doped concentration on the structures and properties of as-prepared powders were investigated in detail. Higher crystallinity and better luminescence performance powders were obtained at MRCM=2, pH=3 and the calcination temperature of 1200 °C. The phosphors exhibited the characteristic broadband visible luminescence of YAG:Ce. The optimum concentration of Ce3+ was 1.0 mol.%, and the concentration quenching was derived from the reciprocity between electric dipole and electric quadrupole (d-q). Especially, the pH value of the solution was a key factor to obtain a stable sol-gel system and then obtain pure and homogeneous rare earth ions doped YAG phosphors at a lower temperature. The Y3Al5O12:Ce0.03 phosphor with optimized synthesis-condition and composition had a similar luminescence intensity with the commercial phosphor YAG:Ce. |
| Author | 张乐 陆洲 朱金振 杨浩 韩朋德 陈雁 张其土 |
| AuthorAffiliation | College of Materials Science and Engineering, Nanjing University of Technology, Nanjing 210009, China |
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| Copyright | 2012 The Chinese Society of Rare Earths |
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| Keywords | concentration quenching YAG:Ce sol-gel combustion method photoluminescence phosphors rare earths |
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| Notes | 11-2788/TF ZHANG Le , LU Zhou , ZHU Jinzhen , YANG Hao, HAN Pengde, CHEN Yan , ZHANG Qitu （College of Materials Science and Engineering, Nanjing University of Technology, Nanjing 210009, China） Yellow-emitting YAG：Ce3＋ nanocrystalline phosphors were prepared by citrate sol-gel combustion method using citric acid as the fuel and chelating agent. The influence of mole ratio of citric acid to metallic ions （MRCM）, pH value of the solution, calcination temperature and Ce-doped concentration on the structures and properties of as-prepared powders were investigated in detail. Higher crystallinity and better luminescence performance powders were obtained at MRCM=2, pH=3 and the calcination temperature of 1200 ℃. The phosphors exhibited the charactefistc broadband visible luminescence of YAG：Ce. The optimum concentration of Ce3＋ was 1.0 tool.%, and the concentration quenching was derived from the reciprocity between electric dipole and electric quadrupole （d-q）. Especially, the pH value of the solution was a key factor to obtain a stable sol-gel system and then obtain pure and homogeneous rare earth ions doped YAG phosphors at a lower tem- perature. The Y3Al5O12：Ce0.03 phosphor with optimized synthesis-condition and composition had a similar luminescence intensity with the commercial phosphor YAG：Ce. YAG：Ce; sol-gel combustion method; photoluminescence; phosphors; concentration quenching; rare earths ObjectType-Article-2 SourceType-Scholarly Journals-1 ObjectType-Feature-1 content type line 23 |
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| Snippet | Yellow-emitting YAG：Ce3＋ nanocrystalline phosphors were prepared by citrate sol-gel combustion method using citric acid as the fuel and chelating agent. The... Yellow-emitting YAG:Ce3+ nanocrystalline phosphors were prepared by citrate sol-gel combustion method using citric acid as the fuel and chelating agent. The... Yellow-emitting YAG: Ce3+ nanocrystalline phosphors were prepared by citrate sol-gel combustion method using citric acid as the fuel and chelating agent. The... |
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| SubjectTerms | Citrates Citric acid Combustion concentration quenching Luminescence Phosphors photoluminescence Rare earth metals rare earths Sol gel process sol-gel combustion method YAG YAG:Ce YAG荧光粉 光致发光特性 凝胶 制备 柠檬酸 溶胶 纳米荧光粉 |
| Title | Citrate sol-gel combustion preparation and photoluminescence properties of YAG：Ce phosphors |
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