Interfacial improvement of carbon fiber/epoxy composites using one-step method for grafting carbon nanotubes on the fibers at ultra-low temperatures
This paper focuses on improving the out-of-plane properties of carbon fiber/epoxy composites to extend their applications. Carbon nanotubes (CNTs) were introduced on carbon fiber surface by a novel one-step chemical vapor deposition (CVD) method at ultra-low temperature and hybrid composites were fa...
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| Published in | Carbon (New York) Vol. 164; pp. 133 - 142 |
|---|---|
| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
New York
Elsevier Ltd
30.08.2020
Elsevier BV |
| Subjects | |
| Online Access | Get full text |
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| Abstract | This paper focuses on improving the out-of-plane properties of carbon fiber/epoxy composites to extend their applications. Carbon nanotubes (CNTs) were introduced on carbon fiber surface by a novel one-step chemical vapor deposition (CVD) method at ultra-low temperature and hybrid composites were fabricated by molding technology. Mechanical and dielectric tests were conducted to figure out the changes in out-of-plane properties after grafting CNTs. The results of single-fiber tensile strength indicated that both the strength and the Weibull modulus of the CNTs-coated carbon fiber increased due to the less damage caused to the fiber by catalysts at low temperature and the repairing effect of the CNTs. Compared with the properties of desized fiber based composites, both interfacial shear strength (IFSS) and interlaminar shear strength (ILSS) of CNTs-coated fiber/epoxy composites increased by 30.73% and 32.29%, respectively, as well as the dielectric properties were also improved. The fracture mechanisms of CNTs were investigated based on the morphology observation on the interface. The improved out-of-plane properties were associated with the improved stress transfer between the carbon fibers and surrounding matrix through the newly formed interphase induced by CNT layer.
TEM images of the structure of CNTs.The fracture surface in the weft direction of CNTs-coated carbon fiber/epoxy composites. [Display omitted] |
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| AbstractList | This paper focuses on improving the out-of-plane properties of carbon fiber/epoxy composites to extend their applications. Carbon nanotubes (CNTs) were introduced on carbon fiber surface by a novel one-step chemical vapor deposition (CVD) method at ultra-low temperature and hybrid composites were fabricated by molding technology. Mechanical and dielectric tests were conducted to figure out the changes in out-of-plane properties after grafting CNTs. The results of single-fiber tensile strength indicated that both the strength and the Weibull modulus of the CNTs-coated carbon fiber increased due to the less damage caused to the fiber by catalysts at low temperature and the repairing effect of the CNTs. Compared with the properties of desized fiber based composites, both interfacial shear strength (IFSS) and interlaminar shear strength (ILSS) of CNTs-coated fiber/epoxy composites increased by 30.73% and 32.29%, respectively, as well as the dielectric properties were also improved. The fracture mechanisms of CNTs were investigated based on the morphology observation on the interface. The improved out-of-plane properties were associated with the improved stress transfer between the carbon fibers and surrounding matrix through the newly formed interphase induced by CNT layer. This paper focuses on improving the out-of-plane properties of carbon fiber/epoxy composites to extend their applications. Carbon nanotubes (CNTs) were introduced on carbon fiber surface by a novel one-step chemical vapor deposition (CVD) method at ultra-low temperature and hybrid composites were fabricated by molding technology. Mechanical and dielectric tests were conducted to figure out the changes in out-of-plane properties after grafting CNTs. The results of single-fiber tensile strength indicated that both the strength and the Weibull modulus of the CNTs-coated carbon fiber increased due to the less damage caused to the fiber by catalysts at low temperature and the repairing effect of the CNTs. Compared with the properties of desized fiber based composites, both interfacial shear strength (IFSS) and interlaminar shear strength (ILSS) of CNTs-coated fiber/epoxy composites increased by 30.73% and 32.29%, respectively, as well as the dielectric properties were also improved. The fracture mechanisms of CNTs were investigated based on the morphology observation on the interface. The improved out-of-plane properties were associated with the improved stress transfer between the carbon fibers and surrounding matrix through the newly formed interphase induced by CNT layer. TEM images of the structure of CNTs.The fracture surface in the weft direction of CNTs-coated carbon fiber/epoxy composites. [Display omitted] |
| Author | Wang, Qifen Su, Shunsheng Wang, Chengguo Wei, Huazhen Yu, Meijie Wang, Yanxiang Yao, Zhiqiang Qin, Jianjie |
| Author_xml | – sequence: 1 givenname: Zhiqiang surname: Yao fullname: Yao, Zhiqiang organization: Key Laboratory for Liquid-Solid Structural Evolution & Processing of Materials (Ministry of Education), Shandong University, Jinan, 250061, China – sequence: 2 givenname: Chengguo surname: Wang fullname: Wang, Chengguo email: wangchg@sdu.edu.cn organization: Key Laboratory for Liquid-Solid Structural Evolution & Processing of Materials (Ministry of Education), Shandong University, Jinan, 250061, China – sequence: 3 givenname: Jianjie surname: Qin fullname: Qin, Jianjie organization: Carbon Fiber Engineering Research Center, School of Material Science and Engineering, Shandong University, Jinan, 250061, China – sequence: 4 givenname: Shunsheng surname: Su fullname: Su, Shunsheng organization: Carbon Fiber Engineering Research Center, School of Material Science and Engineering, Shandong University, Jinan, 250061, China – sequence: 5 givenname: Yanxiang surname: Wang fullname: Wang, Yanxiang organization: Key Laboratory for Liquid-Solid Structural Evolution & Processing of Materials (Ministry of Education), Shandong University, Jinan, 250061, China – sequence: 6 givenname: Qifen surname: Wang fullname: Wang, Qifen organization: CNGC Institute 53, Jinan, 250031, China – sequence: 7 givenname: Meijie surname: Yu fullname: Yu, Meijie email: yumeijie@sdu.edu.cn organization: Key Laboratory for Liquid-Solid Structural Evolution & Processing of Materials (Ministry of Education), Shandong University, Jinan, 250061, China – sequence: 8 givenname: Huazhen surname: Wei fullname: Wei, Huazhen organization: CNGC Institute 53, Jinan, 250031, China |
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| Snippet | This paper focuses on improving the out-of-plane properties of carbon fiber/epoxy composites to extend their applications. Carbon nanotubes (CNTs) were... |
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| StartPage | 133 |
| SubjectTerms | Carbon fiber reinforced plastics Carbon fibers Carbon nanotubes Carbon-epoxy composites catalysts Chemical vapor deposition Coated fibers Composite materials Dielectric properties epoxides Fracture mechanics Grafting Hybrid composites Interfacial shear strength Low temperature Morphology Nanotubes shear strength Stress transfer temperature Tensile strength vapors Weibull modulus Weibull statistics |
| Title | Interfacial improvement of carbon fiber/epoxy composites using one-step method for grafting carbon nanotubes on the fibers at ultra-low temperatures |
| URI | https://dx.doi.org/10.1016/j.carbon.2020.03.060 https://www.proquest.com/docview/2441886398 https://www.proquest.com/docview/2439426544 |
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