Potentiometric sensor for sorbic acid determination in food products
The construction, evaluation and application of a new potentiometric sensor, namely, Pt|Hg|Hg 2(SOB) 2 |Graphite, where SOB stands for sorbate ion, are described. This electrode has a wide linear dynamic range between 5.0 × 10 −7 and 1.0 × 10 −2 mol L −1 with a near-Nernstian slope of (−58.6 ± 1.3)...
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Published in | Food chemistry Vol. 115; no. 4; pp. 1563 - 1567 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
Published |
Kidlington
Elsevier Ltd
15.08.2009
[Amsterdam]: Elsevier Science Elsevier |
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Abstract | The construction, evaluation and application of a new potentiometric sensor, namely, Pt|Hg|Hg
2(SOB)
2 |Graphite, where SOB stands for sorbate ion, are described. This electrode has a wide linear dynamic range between 5.0
×
10
−7 and 1.0
×
10
−2
mol
L
−1 with a near-Nernstian slope of (−58.6
±
1.3) mV decade
−1 and a detection limit of 4.3
×
10
−7
mol
L
−1. The potentiometric response is independent of the pH of the solution in the pH range 6.0–9.0. The electrode is easily constructed at a relatively low-cost with fast response time (within 15–30
s) and can be used for a period of 4
months without significant change in its performance characteristics. The proposed sensor displayed good selectivities over a variety of other anions (carboxylates and inorganic anions). The potentiometric sensor was successfully applied to the determination of sorbic acid in real food samples, that is, soft drinks, skim yogurts, jams and sauces. |
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AbstractList | The construction, evaluation and application of a new potentiometric sensor, namely, Pt|Hg|Hg
2(SOB)
2 |Graphite, where SOB stands for sorbate ion, are described. This electrode has a wide linear dynamic range between 5.0
×
10
−7 and 1.0
×
10
−2
mol
L
−1 with a near-Nernstian slope of (−58.6
±
1.3) mV decade
−1 and a detection limit of 4.3
×
10
−7
mol
L
−1. The potentiometric response is independent of the pH of the solution in the pH range 6.0–9.0. The electrode is easily constructed at a relatively low-cost with fast response time (within 15–30
s) and can be used for a period of 4
months without significant change in its performance characteristics. The proposed sensor displayed good selectivities over a variety of other anions (carboxylates and inorganic anions). The potentiometric sensor was successfully applied to the determination of sorbic acid in real food samples, that is, soft drinks, skim yogurts, jams and sauces. The construction, evaluation and application of a new potentiometric sensor, namely, Pt|Hg|Hg₂(SOB)₂ |Graphite, where SOB stands for sorbate ion, are described. This electrode has a wide linear dynamic range between 5.0x10⁻⁷ and 1.0x10⁻² molL⁻¹ with a near-Nernstian slope of (-58.6±1.3) mV decade⁻¹ and a detection limit of 4.3x10⁻⁷ molL⁻¹. The potentiometric response is independent of the pH of the solution in the pH range 6.0-9.0. The electrode is easily constructed at a relatively low-cost with fast response time (within 15-30s) and can be used for a period of 4months without significant change in its performance characteristics. The proposed sensor displayed good selectivities over a variety of other anions (carboxylates and inorganic anions). The potentiometric sensor was successfully applied to the determination of sorbic acid in real food samples, that is, soft drinks, skim yogurts, jams and sauces. |
Author | Pezza, Leonardo Santini, Alberto O. Pezza, Helena R. Carloni-Filho, João Sequinel, Rodrigo |
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CitedBy_id | crossref_primary_10_1016_j_talanta_2011_03_027 crossref_primary_10_1016_j_aca_2012_04_033 crossref_primary_10_1016_j_talanta_2013_07_065 crossref_primary_10_2116_analsci_25_1295 crossref_primary_10_1016_j_snb_2017_09_144 crossref_primary_10_2139_ssrn_4118578 crossref_primary_10_1039_D1AY01212F crossref_primary_10_1002_jssc_201800705 crossref_primary_10_1016_j_foodchem_2014_01_041 crossref_primary_10_1016_j_talo_2022_100146 crossref_primary_10_1080_00032719_2011_644738 |
Cites_doi | 10.1016/S0963-9969(00)00014-4 10.1080/02652039009373936 10.1016/S0021-9673(01)95756-5 10.1016/S0021-9673(98)01035-8 10.1039/an9871201269 10.1016/j.foodchem.2005.09.022 10.1016/S0021-9673(03)00246-2 10.1016/S0003-2670(01)00794-2 10.1016/S0003-2670(00)85640-8 10.1021/cr940394a 10.1016/0308-8146(95)90793-7 10.1016/0021-9673(92)80337-T 10.1351/pac199466122527 10.1111/j.1398-9995.1987.tb00386.x 10.1039/an9901501219 10.1080/02652039009373932 10.1002/elan.1140030802 10.1016/S0021-9673(00)00404-0 10.1016/j.chroma.2004.10.105 |
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Keywords | Sorbate-sensitive electrode Potentiometry Skim yogurts Sauces Jams Soft drinks Dairy product Yogurt Electrodes Sauce Jam Soft drink Food |
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2 |Graphite, where SOB stands for sorbate ion, are... The construction, evaluation and application of a new potentiometric sensor, namely, Pt|Hg|Hg₂(SOB)₂ |Graphite, where SOB stands for sorbate ion, are... |
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SubjectTerms | analytical methods Biological and medical sciences detection electrodes food analysis food composition Food industries food preservatives Fundamental and applied biological sciences. Psychology Jams Milk and cheese industries. Ice creams Non alcoholic beverage industries and mineral waters potentiometric sensor Potentiometry rapid methods Sauces sensors Skim yogurts Soft drinks Sorbate-sensitive electrode sorbic acid |
Title | Potentiometric sensor for sorbic acid determination in food products |
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