A solid-phase microextraction platinized stainless steel fiber coated with a multiwalled carbon nanotube-polyaniline nanocomposite film for the extraction of thymol and carvacrol in medicinal plants and honey
•It is the first use of the EPD platinization technique, to make the surface of a stainless steel SPME fiber porous and cohesive, for tight attaching of the coating.•Using the EPD strategy, for coating of the platinized stainless steel wire by MWCNTs/PANI, resulted in an SPME fiber with substantial...
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Published in | Journal of Chromatography A Vol. 1406; pp. 87 - 93 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
Published |
Netherlands
Elsevier B.V
07.08.2015
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Abstract | •It is the first use of the EPD platinization technique, to make the surface of a stainless steel SPME fiber porous and cohesive, for tight attaching of the coating.•Using the EPD strategy, for coating of the platinized stainless steel wire by MWCNTs/PANI, resulted in an SPME fiber with substantial durability, long lifetime, and acceptable efficiency.•Comparison of the proposed novel fiber, with commercial fibers, has established its preferences.•Thymol and carvacrol was successfully extracted by the proposed nanocomposite fiber, through a DI-SPME strategy, from aqueous real samples.
A mechanically hard and cohesive porous fiber, with large surface area, for more strong attachment of the coating was provided by platinizing a stainless steel wire. Then, the platinized stainless steel fiber was coated with a multiwalled carbon nanotube/polyaniline (MWCNT/PANI) nanocomposite using electrophoretic deposition (EPD) method and applied for the extraction of thymol and carvacrol with direct-immersion solid-phase microextraction (DI-SPME) method followed by high-performance liquid chromatography-ultraviolet detection (HPLC-UV) quantification. To provide a larger coarse surface for the tightened attachment of coating on the fiber, a stainless steel wire was platinized using a suitable optimized EPD method. Different experimental parameters were studied and the optimal conditions were obtained as: pH of the sample solution: 2; extraction time: 60min; salt content in the sample solution: 1% w/v NaNO3; desorption time: 60min; type and volume of the desorption solvent: acetonitrile, 100μL. Under the optimized conditions, limits of detection (LODs) were 0.6 and 0.8μgmL−1 for thymol and carvacrol, respectively. Linear dynamic range (LDR) for the calibration curves of both analytes were 1–80μgmL−1. Relative standard deviation (RSD%, n=6) was 6.8 for thymol and 12.7 for carvacrol. The proposed fiber was successfully applied for the recovery and determination of thymol and carvacrol in thyme, savory, and honey samples. |
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AbstractList | A mechanically hard and cohesive porous fiber, with large surface area, for more strong attachment of the coating was provided by platinizing a stainless steel wire. Then, the platinized stainless steel fiber was coated with a multiwalled carbon nanotube/polyaniline (MWCNT/PANI) nanocomposite using electrophoretic deposition (EPD) method and applied for the extraction of thymol and carvacrol with direct-immersion solid-phase microextraction (DI-SPME) method followed by high-performance liquid chromatography-ultraviolet detection (HPLC-UV) quantification. To provide a larger coarse surface for the tightened attachment of coating on the fiber, a stainless steel wire was platinized using a suitable optimized EPD method. Different experimental parameters were studied and the optimal conditions were obtained as: pH of the sample solution: 2; extraction time: 60min; salt content in the sample solution: 1% w/v NaNO3; desorption time: 60min; type and volume of the desorption solvent: acetonitrile, 100μL. Under the optimized conditions, limits of detection (LODs) were 0.6 and 0.8μgmL(-1) for thymol and carvacrol, respectively. Linear dynamic range (LDR) for the calibration curves of both analytes were 1-80μgmL(-1). Relative standard deviation (RSD%, n=6) was 6.8 for thymol and 12.7 for carvacrol. The proposed fiber was successfully applied for the recovery and determination of thymol and carvacrol in thyme, savory, and honey samples. •It is the first use of the EPD platinization technique, to make the surface of a stainless steel SPME fiber porous and cohesive, for tight attaching of the coating.•Using the EPD strategy, for coating of the platinized stainless steel wire by MWCNTs/PANI, resulted in an SPME fiber with substantial durability, long lifetime, and acceptable efficiency.•Comparison of the proposed novel fiber, with commercial fibers, has established its preferences.•Thymol and carvacrol was successfully extracted by the proposed nanocomposite fiber, through a DI-SPME strategy, from aqueous real samples. A mechanically hard and cohesive porous fiber, with large surface area, for more strong attachment of the coating was provided by platinizing a stainless steel wire. Then, the platinized stainless steel fiber was coated with a multiwalled carbon nanotube/polyaniline (MWCNT/PANI) nanocomposite using electrophoretic deposition (EPD) method and applied for the extraction of thymol and carvacrol with direct-immersion solid-phase microextraction (DI-SPME) method followed by high-performance liquid chromatography-ultraviolet detection (HPLC-UV) quantification. To provide a larger coarse surface for the tightened attachment of coating on the fiber, a stainless steel wire was platinized using a suitable optimized EPD method. Different experimental parameters were studied and the optimal conditions were obtained as: pH of the sample solution: 2; extraction time: 60min; salt content in the sample solution: 1% w/v NaNO3; desorption time: 60min; type and volume of the desorption solvent: acetonitrile, 100μL. Under the optimized conditions, limits of detection (LODs) were 0.6 and 0.8μgmL−1 for thymol and carvacrol, respectively. Linear dynamic range (LDR) for the calibration curves of both analytes were 1–80μgmL−1. Relative standard deviation (RSD%, n=6) was 6.8 for thymol and 12.7 for carvacrol. The proposed fiber was successfully applied for the recovery and determination of thymol and carvacrol in thyme, savory, and honey samples. |
Author | Dowlatshah, Samira Ghiasvand, Alireza Nouraei, Nadia Heidari, Nahid Yazdankhah, Fatemeh |
Author_xml | – sequence: 1 givenname: Alireza surname: Ghiasvand fullname: Ghiasvand, Alireza email: a_ghiasvand@yahoo.com – sequence: 2 givenname: Samira surname: Dowlatshah fullname: Dowlatshah, Samira – sequence: 3 givenname: Nadia surname: Nouraei fullname: Nouraei, Nadia – sequence: 4 givenname: Nahid surname: Heidari fullname: Heidari, Nahid – sequence: 5 givenname: Fatemeh surname: Yazdankhah fullname: Yazdankhah, Fatemeh |
BackLink | https://www.ncbi.nlm.nih.gov/pubmed/26138604$$D View this record in MEDLINE/PubMed |
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Keywords | Solid-phase microextraction Carvacrol Thymol HPLC Multiwalled carbon nanotube/polyaniline Electrophoretic deposition |
Language | English |
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Snippet | •It is the first use of the EPD platinization technique, to make the surface of a stainless steel SPME fiber porous and cohesive, for tight attaching of the... A mechanically hard and cohesive porous fiber, with large surface area, for more strong attachment of the coating was provided by platinizing a stainless steel... |
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SubjectTerms | Aniline Compounds - chemistry Carvacrol Chemistry Techniques, Analytical - instrumentation Chemistry Techniques, Analytical - methods Electrophoretic deposition Honey HPLC Limit of Detection Monoterpenes - isolation & purification Multiwalled carbon nanotube/polyaniline Nanocomposites - chemistry Nanotubes, Carbon - chemistry Plants, Medicinal - chemistry Solid Phase Microextraction - instrumentation Solid-phase microextraction Stainless Steel - chemistry Thymol Thymol - isolation & purification Water Pollutants, Chemical - analysis |
Title | A solid-phase microextraction platinized stainless steel fiber coated with a multiwalled carbon nanotube-polyaniline nanocomposite film for the extraction of thymol and carvacrol in medicinal plants and honey |
URI | https://dx.doi.org/10.1016/j.chroma.2015.06.052 https://www.ncbi.nlm.nih.gov/pubmed/26138604 |
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