Adsorption of 2-mercaptopyridine and 4-mercaptopyridine on a silver surfaces investigated by SERS spectroscopy
In this study, the 2-mercaptopyridine (2-MPY) and 4-mercaptopyridine (4-MPY) on to silver mirror and silver sol substrates have been studied by surface enhanced Raman scattering (SERS). The surface enhanced properties of 2-MPY and 4-MPY showed that the substrate of silver mirror was superior to the...
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| Published in | Journal of industrial and engineering chemistry (Seoul, Korea) Vol. 18; no. 6; pp. 2141 - 2146 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
25.11.2012
한국공업화학회 |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1226-086X 1876-794X |
| DOI | 10.1016/j.jiec.2012.06.009 |
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| Abstract | In this study, the 2-mercaptopyridine (2-MPY) and 4-mercaptopyridine (4-MPY) on to silver mirror and silver sol substrates have been studied by surface enhanced Raman scattering (SERS). The surface enhanced properties of 2-MPY and 4-MPY showed that the substrate of silver mirror was superior to the sliver sol. The silver mirror and silver sol substrates were prepared by Tollen's and gamma irradiation method respectively. UV-visible spectra indicate that Ag nanoparticles were produced by this method. Considerable differences were found in the SERS spectra of 2-MPY and 4-MPY molecules onto silver mirror and silver sol substrates. From the analysis of the SERS data, it was evidenced that 2-MPY was chemisorbed through its S atom to Ag surfaces at a perpendicular orientation, whereas 4-MPY was bonded to Ag surface via the S atom and N atom assuming a tilted orientation. |
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| AbstractList | In this study, the 2-mercaptopyridine (2-MPY) and 4-mercaptopyridine (4-MPY) on to silver mirror and silver sol substrates have been studied by surface enhanced Raman scattering (SERS). The surface enhanced properties of 2-MPY and 4-MPY showed that the substrate of silver mirror was superior to the sliver sol. The silver mirror and silver sol substrates were prepared by Tollen's and gamma irradiation method respectively. UV-visible spectra indicate that Ag nanoparticles were produced by this method. Considerable differences were found in the SERS spectra of 2-MPY and 4-MPY molecules onto silver mirror and silver sol substrates. From the analysis of the SERS data, it was evidenced that 2-MPY was chemisorbed through its S atom to Ag surfaces at a perpendicular orientation, whereas 4-MPY was bonded to Ag surface via the S atom and N atom assuming a tilted orientation. In this study, the 2-mercaptopyridine (2-MPY) and 4-mercaptopyridine (4-MPY) on to silver mirror and silver sol substrates have been studied by surface enhanced Raman scattering (SERS). The surface enhanced properties of 2-MPY and 4-MPY showed that the substrate of silver mirror was superior to the sliver sol. The silver mirror and silver sol substrates were prepared by Tollen’s and gamma irradiation method respectively. UV-visible spectra indicate that Ag nanoparticles were produced by this method. Considerable differences were found in the SERS spectra of 2-MPY and 4-MPY molecules onto silver mirror and silver sol substrates. From the analysis of the SERS data, it was evidenced that 2-MPY was chemisorbed through its S atom to Ag surfaces at a perpendicular orientation, whereas 4-MPY was bonded to Ag surface via the S atom and N atom assuming a tilted orientation. KCI Citation Count: 27 |
| Author | Lee, Chul Jae Do, Won Hui Jung, Maeng Joon Kim, Dong Yeub |
| Author_xml | – sequence: 1 givenname: Won Hui surname: Do fullname: Do, Won Hui organization: Department of Chemistry, Kyungpook National University, Daegu 702-701, Republic of Korea – sequence: 2 givenname: Chul Jae surname: Lee fullname: Lee, Chul Jae organization: School of Chemical Industry, Yeungnam College of Science & Technology, Daegu 705-703, Republic of Korea – sequence: 3 givenname: Dong Yeub surname: Kim fullname: Kim, Dong Yeub organization: School of Chemical Industry, Yeungnam College of Science & Technology, Daegu 705-703, Republic of Korea – sequence: 4 givenname: Maeng Joon surname: Jung fullname: Jung, Maeng Joon email: jmj@knu.ac.kr organization: School of Nano & Materials Science Engineering, Kyungpook National University, Sangju 742-711, Republic of Korea |
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| Cites_doi | 10.1016/S1383-5866(03)00003-0 10.1021/la011554y 10.1021/ac060807v 10.1021/la001700k 10.1016/j.jcis.2005.03.017 10.1016/S0022-0728(77)80224-6 10.1103/RevModPhys.57.783 10.1016/0009-2614(74)85388-1 10.1021/cr9502357 10.1016/0039-6028(83)90345-X 10.1366/000370207781540105 10.1016/S1386-1425(02)00074-4 10.1021/ja00276a005 10.1016/j.jcis.2004.02.084 10.5012/bkcs.2006.27.4.545 10.1016/j.electacta.2005.08.007 10.1021/ja00457a071 10.1021/ja00079a021 |
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| Keywords | Gamma irradiation 2-Mercaptopyridine 4-Mercaptopyridine SERS Tollen's method |
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| SubjectTerms | 2-Mercaptopyridine 4-Mercaptopyridine Chemical bonds Gamma irradiation Nanoparticles Orientation Raman scattering SERS Silver Slivers Spectra Surface chemistry Tollen's method 화학공학 |
| Title | Adsorption of 2-mercaptopyridine and 4-mercaptopyridine on a silver surfaces investigated by SERS spectroscopy |
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