Tolerant to air σ-alkane complexes by surface modification of single crystalline solid-state molecular organometallics using vapour-phase cationic polymerisation: SMOM@polymer

Vapour-phase surface-initiated cationic polymerisation of ethylvinylether occurs at single-crystals of the σ-alkane complex [Rh(Cy 2 PCH 2 CH 2 PCy 2 )(NBA)][BAr F 4 ]. This new surface interface makes these normally very air sensitive materials tolerant to air, while also allowing for onward single...

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Published inChemical communications (Cambridge, England) Vol. 56; no. 31; pp. 4328 - 4331
Main Authors Bukvic, Alexander J, Crivoi, Dana Georgiana, Garwood, Hollie G, McKay, Alasdair I, Chen, Thomas T. D, Martínez-Martínez, Antonio J, Weller, Andrew S
Format Journal Article
LanguageEnglish
Published England Royal Society of Chemistry 21.04.2020
Subjects
air
Alkanes
Cationic polymerization
Crystal lattices
Crystallography
Crystals
Organometallic compounds
Polymerization
polymers
Single crystals
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Abstract Vapour-phase surface-initiated cationic polymerisation of ethylvinylether occurs at single-crystals of the σ-alkane complex [Rh(Cy 2 PCH 2 CH 2 PCy 2 )(NBA)][BAr F 4 ]. This new surface interface makes these normally very air sensitive materials tolerant to air, while also allowing for onward single-crystal to single-crystal reactivity at metal sites within the lattice. Surface-initiated cationic polymerisation of ethylvinylether at single-crystals of the σ-alkane complex [Rh(Cy 2 PCH 2 CH 2 PCy 2 )(NBA)][BAr F 4 ] imparts air-tolerance to this highly reactive complex.
AbstractList Vapour-phase surface-initiated cationic polymerisation of ethylvinylether occurs at single-crystals of the σ-alkane complex [Rh(Cy2PCH2CH2PCy2)(NBA)][BArF4]. This new surface interface makes these normally very air sensitive materials tolerant to air, while also allowing for onward single-crystal to single-crystal reactivity at metal sites within the lattice.
Vapour-phase surface-initiated cationic polymerisation of ethylvinylether occurs at single-crystals of the σ-alkane complex [Rh(Cy₂PCH₂CH₂PCy₂)(NBA)][BArF₄]. This new surface interface makes these normally very air sensitive materials tolerant to air, while also allowing for onward single-crystal to single-crystal reactivity at metal sites within the lattice.
Vapour-phase surface-initiated cationic polymerisation of ethylvinylether occurs at single-crystals of the σ-alkane complex [Rh(Cy PCH CH PCy )(NBA)][BAr ]. This new surface interface makes these normally very air sensitive materials tolerant to air, while also allowing for onward single-crystal to single-crystal reactivity at metal sites within the lattice.
Vapour-phase surface-initiated cationic polymerisation of ethylvinylether occurs at single-crystals of the σ-alkane complex [Rh(Cy 2 PCH 2 CH 2 PCy 2 )(NBA)][BAr F 4 ]. This new surface interface makes these normally very air sensitive materials tolerant to air, while also allowing for onward single-crystal to single-crystal reactivity at metal sites within the lattice. Surface-initiated cationic polymerisation of ethylvinylether at single-crystals of the σ-alkane complex [Rh(Cy 2 PCH 2 CH 2 PCy 2 )(NBA)][BAr F 4 ] imparts air-tolerance to this highly reactive complex.
Vapour-phase surface-initiated cationic polymerisation of ethylvinylether occurs at single-crystals of the σ-alkane complex [Rh(Cy 2 PCH 2 CH 2 PCy 2 )(NBA)][BAr F 4 ]. This new surface interface makes these normally very air sensitive materials tolerant to air, while also allowing for onward single-crystal to single-crystal reactivity at metal sites within the lattice.
Vapour-phase surface-initiated cationic polymerisation of ethylvinylether occurs at single-crystals of the σ-alkane complex [Rh(Cy2PCH2CH2PCy2)(NBA)][BArF4]. This new surface interface makes these normally very air sensitive materials tolerant to air, while also allowing for onward single-crystal to single-crystal reactivity at metal sites within the lattice.Vapour-phase surface-initiated cationic polymerisation of ethylvinylether occurs at single-crystals of the σ-alkane complex [Rh(Cy2PCH2CH2PCy2)(NBA)][BArF4]. This new surface interface makes these normally very air sensitive materials tolerant to air, while also allowing for onward single-crystal to single-crystal reactivity at metal sites within the lattice.
Author McKay, Alasdair I
Garwood, Hollie G
Weller, Andrew S
Chen, Thomas T. D
Martínez-Martínez, Antonio J
Bukvic, Alexander J
Crivoi, Dana Georgiana
AuthorAffiliation Department of Chemistry
University of York
University of Oxford
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Snippet Vapour-phase surface-initiated cationic polymerisation of ethylvinylether occurs at single-crystals of the σ-alkane complex [Rh(Cy 2 PCH 2 CH 2 PCy 2...
Vapour-phase surface-initiated cationic polymerisation of ethylvinylether occurs at single-crystals of the σ-alkane complex [Rh(Cy PCH CH PCy )(NBA)][BAr ]....
Vapour-phase surface-initiated cationic polymerisation of ethylvinylether occurs at single-crystals of the σ-alkane complex [Rh(Cy2PCH2CH2PCy2)(NBA)][BArF4]....
Vapour-phase surface-initiated cationic polymerisation of ethylvinylether occurs at single-crystals of the σ-alkane complex [Rh(Cy₂PCH₂CH₂PCy₂)(NBA)][BArF₄]....
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SubjectTerms air
Alkanes
Cationic polymerization
Crystal lattices
Crystallography
Crystals
Organometallic compounds
Polymerization
polymers
Single crystals
Title Tolerant to air σ-alkane complexes by surface modification of single crystalline solid-state molecular organometallics using vapour-phase cationic polymerisation: SMOM@polymer
URI https://www.ncbi.nlm.nih.gov/pubmed/32191244
https://www.proquest.com/docview/2390192052
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https://www.proquest.com/docview/2986161765
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