Solid-state structure of thermally crystallized syndiotactic polystyrene
The solid‐state structure of syndiotactic polystyrene (s‐PS) after crystallization from the melt and the glassy state was examined by differential scanning calorimetry (DSC), density, and X‐ray diffraction analysis. It was possible to prepare semicrystalline s‐PS containing either the pure α‐ or the...
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| Published in | Journal of applied polymer science Vol. 83; no. 12; pp. 2705 - 2715 |
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| Main Authors | , , , |
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| Language | English |
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Wiley Periodicals, Inc
21.03.2002
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| Abstract | The solid‐state structure of syndiotactic polystyrene (s‐PS) after crystallization from the melt and the glassy state was examined by differential scanning calorimetry (DSC), density, and X‐ray diffraction analysis. It was possible to prepare semicrystalline s‐PS containing either the pure α‐ or the pure β‐crystalline form by melt crystallizing s‐PS from 280 or 330°C. The measurements confirmed the low density of both crystalline forms, which in the case of α‐crystalline form was smaller and in the case of β‐crystalline form was only slightly larger than the density of the glassy amorphous s‐PS. An endeavor to introduce the crystalline phase in s‐PS through cold crystallization at constant temperature above the glass transition resulted in a complex ordered phase. This ordered phase, depending on the crystallization temperature, contained the planar chain mesomorphic phase and the α‐crystalline phase with a low degree of perfection (cold crystallization in the range 120–175°C) or a mixture of the α‐ and β‐crystalline forms with a high degree of perfection (cold crystallization in the range 210–260°C). The combination of DSC and X‐ray measurements enabled us to resolve the complex ordered structure in semicrystalline s‐PS after cold crystallization. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 83: 2705–2715, 2002 |
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| AbstractList | The solid‐state structure of syndiotactic polystyrene (s‐PS) after crystallization from the melt and the glassy state was examined by differential scanning calorimetry (DSC), density, and X‐ray diffraction analysis. It was possible to prepare semicrystalline s‐PS containing either the pure α‐ or the pure β‐crystalline form by melt crystallizing s‐PS from 280 or 330°C. The measurements confirmed the low density of both crystalline forms, which in the case of α‐crystalline form was smaller and in the case of β‐crystalline form was only slightly larger than the density of the glassy amorphous s‐PS. An endeavor to introduce the crystalline phase in s‐PS through cold crystallization at constant temperature above the glass transition resulted in a complex ordered phase. This ordered phase, depending on the crystallization temperature, contained the planar chain mesomorphic phase and the α‐crystalline phase with a low degree of perfection (cold crystallization in the range 120–175°C) or a mixture of the α‐ and β‐crystalline forms with a high degree of perfection (cold crystallization in the range 210–260°C). The combination of DSC and X‐ray measurements enabled us to resolve the complex ordered structure in semicrystalline s‐PS after cold crystallization. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 83: 2705–2715, 2002 Abstract The solid‐state structure of syndiotactic polystyrene (s‐PS) after crystallization from the melt and the glassy state was examined by differential scanning calorimetry (DSC), density, and X‐ray diffraction analysis. It was possible to prepare semicrystalline s‐PS containing either the pure α‐ or the pure β‐crystalline form by melt crystallizing s‐PS from 280 or 330°C. The measurements confirmed the low density of both crystalline forms, which in the case of α‐crystalline form was smaller and in the case of β‐crystalline form was only slightly larger than the density of the glassy amorphous s‐PS. An endeavor to introduce the crystalline phase in s‐PS through cold crystallization at constant temperature above the glass transition resulted in a complex ordered phase. This ordered phase, depending on the crystallization temperature, contained the planar chain mesomorphic phase and the α‐crystalline phase with a low degree of perfection (cold crystallization in the range 120–175°C) or a mixture of the α‐ and β‐crystalline forms with a high degree of perfection (cold crystallization in the range 210–260°C). The combination of DSC and X‐ray measurements enabled us to resolve the complex ordered structure in semicrystalline s‐PS after cold crystallization. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 83: 2705–2715, 2002 The solid-state structure of syndiotactic polystyrene (s-PS) after crystallization from the melt and the glassy state was examined by differential scanning calorimetry (DSC), density, and X-ray diffraction analysis. It was possible to prepare semicrystalline s-PS containing either the pure alpha - or the pure beta -crystalline form by melt crystallizing s-PS from 280 or 330 deg C. The measurements confirmed the low density of both crystalline forms, which in the case of alpha -crystalline form was smaller and in the case of beta -crystalline form was only slightly larger than the density of the glassy amorphous s-PS. An endeavor to introduce the crystalline phase in s-PS through cold crystallization at constant temperature above the glass transition resulted in a complex ordered phase. This ordered phase, depending on the crystallization temperature, contained the planar chain mesomorphic phase and the alpha -crystalline phase with a low degree of perfection (cold crystallization in the range 120-175 deg C) or a mixture of the alpha -and beta -crystalline forms with a high degree of perfection (cold crystallization in the range 210-260 deg C). The combination of DSC and X-ray measurements enabled us to resolve the complex ordered structure in semicrystalline s-PS after cold crystallization. |
| Author | Hodge, K. Prodpran, T. Nazarenko, S. Shenogina, N. B. |
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| Cites_doi | 10.1016/0032-3861(89)90140-7 10.1021/ma00172a028 10.1016/0032-3861(88)90386-2 10.1002/pol.1962.1205816618 10.1021/ma00067a008 10.1007/BF00657401 10.1016/0040-6031(91)80095-Z 10.1021/j100892a030 10.1021/ma9712209 10.1016/0032-3861(87)90382-X 10.1295/polymj.23.1435 10.1021/ma960905q 10.1021/ma00207a050 10.1016/S0032-3861(99)00127-5 10.1016/0032-3861(92)90117-F |
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| Keywords | Structure processing relationship Melt crystallization Beta form Crystal form Styrene polymer Experimental study Syndiotactic polymer Isothermal crystallization Alpha form Polymorphism |
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| Snippet | The solid‐state structure of syndiotactic polystyrene (s‐PS) after crystallization from the melt and the glassy state was examined by differential scanning... Abstract The solid‐state structure of syndiotactic polystyrene (s‐PS) after crystallization from the melt and the glassy state was examined by differential... The solid-state structure of syndiotactic polystyrene (s-PS) after crystallization from the melt and the glassy state was examined by differential scanning... |
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| SubjectTerms | Applied sciences Crystallization Exact sciences and technology Organic polymers Physicochemistry of polymers polymorphism Properties and characterization syndiotactic polystyrene (s-PS) |
| Title | Solid-state structure of thermally crystallized syndiotactic polystyrene |
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