Remote-Controllable Molecular Knob in the Mesomorphic Helical Superstructures

A programed light‐responsive chiral liquid crystal (LC) containing four photochromic azobenzene moieties covalently connected to a central bicyclic chiral core (abbreviated as AZ4ICD) is newly designed, precisely synthesized, and efficiently applied as a remote‐controllable molecular knob for the op...

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Published in	Advanced functional materials Vol. 26; no. 24; pp. 4242 - 4251
Main Authors	Kim, Dae-Yoon, Lee, Sang-A, Park, Minwook, Choi, Yu-Jin, Yoon, Won-Jin, Kim, Jin Soo, Yu, Yeon-Tae, Jeong, Kwang-Un
Format	Journal Article
Language	English
Published	Blackwell Publishing Ltd 27.06.2016
Subjects	Doping Helical helical superstructure Knobs layer structure light-responsive liquid crystal Liquid crystals Molecular structure Nematic self-assembly Superstructures Tuning
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Abstract	A programed light‐responsive chiral liquid crystal (LC) containing four photochromic azobenzene moieties covalently connected to a central bicyclic chiral core (abbreviated as AZ4ICD) is newly designed, precisely synthesized, and efficiently applied as a remote‐controllable molecular knob for the optically tunable thin film. First of all, phase evolutions and ordered structures of AZ4ICD are systematically investigated by a combination of thermal, microscopic, scattering, and simulation techniques. Wide‐angle X‐ray diffractions of oriented AZ4ICD samples indicate that the AZ4ICD molecule itself basically forms layer structures: one is a low‐ordered chiral smectic A LC phase (SmA) with 5.61 nm layer periodicity at high temperatures, and two highly ordered smectic crystal (SmCr1 and SmCr2) phases are subsequently formed at lower temperatures with the anticlinically tilted molecular packing structures. The helical superstructures of chiral nematic LC phase (N) can be spontaneously constructed by doping AZ4ICD chiral agents into the achiral nematic molecules. Due to the bent conformational geometry of AZ4ICD, the thermal window of blue LC phase (BP) is expanded by stabilizing the double twisted cylindrical building blocks. Remote‐controllable phase transformations in the mesomorphic helical superstructures are demonstrated by tuning the wavelength of light. By taking intramolecular conformations and intermolecular interactions into account, a photochromic chiral liquid crystal is synthesized that functions as a remote‐controllable molecular knob for tuning the mesomorphic helical superstructures.
AbstractList	A programed light‐responsive chiral liquid crystal (LC) containing four photochromic azobenzene moieties covalently connected to a central bicyclic chiral core (abbreviated as AZ4ICD) is newly designed, precisely synthesized, and efficiently applied as a remote‐controllable molecular knob for the optically tunable thin film. First of all, phase evolutions and ordered structures of AZ4ICD are systematically investigated by a combination of thermal, microscopic, scattering, and simulation techniques. Wide‐angle X‐ray diffractions of oriented AZ4ICD samples indicate that the AZ4ICD molecule itself basically forms layer structures: one is a low‐ordered chiral smectic A LC phase (SmA) with 5.61 nm layer periodicity at high temperatures, and two highly ordered smectic crystal (SmCr1 and SmCr2) phases are subsequently formed at lower temperatures with the anticlinically tilted molecular packing structures. The helical superstructures of chiral nematic LC phase (N) can be spontaneously constructed by doping AZ4ICD chiral agents into the achiral nematic molecules. Due to the bent conformational geometry of AZ4ICD, the thermal window of blue LC phase (BP) is expanded by stabilizing the double twisted cylindrical building blocks. Remote‐controllable phase transformations in the mesomorphic helical superstructures are demonstrated by tuning the wavelength of light. By taking intramolecular conformations and intermolecular interactions into account, a photochromic chiral liquid crystal is synthesized that functions as a remote‐controllable molecular knob for tuning the mesomorphic helical superstructures. A programed light‐responsive chiral liquid crystal (LC) containing four photochromic azobenzene moieties covalently connected to a central bicyclic chiral core (abbreviated as AZ 4 ICD) is newly designed, precisely synthesized, and efficiently applied as a remote‐controllable molecular knob for the optically tunable thin film. First of all, phase evolutions and ordered structures of AZ 4 ICD are systematically investigated by a combination of thermal, microscopic, scattering, and simulation techniques. Wide‐angle X‐ray diffractions of oriented AZ 4 ICD samples indicate that the AZ 4 ICD molecule itself basically forms layer structures: one is a low‐ordered chiral smectic A LC phase (SmA) with 5.61 nm layer periodicity at high temperatures, and two highly ordered smectic crystal (SmCr 1 and SmCr 2 ) phases are subsequently formed at lower temperatures with the anticlinically tilted molecular packing structures. The helical superstructures of chiral nematic LC phase (N) can be spontaneously constructed by doping AZ 4 ICD chiral agents into the achiral nematic molecules. Due to the bent conformational geometry of AZ 4 ICD, the thermal window of blue LC phase (BP) is expanded by stabilizing the double twisted cylindrical building blocks. Remote‐controllable phase transformations in the mesomorphic helical superstructures are demonstrated by tuning the wavelength of light. A programed light-responsive chiral liquid crystal (LC) containing four photochromic azobenzene moieties covalently connected to a central bicyclic chiral core (abbreviated as AZ sub(4)ICD) is newly designed, precisely synthesized, and efficiently applied as a remote-controllable molecular knob for the optically tunable thin film. First of all, phase evolutions and ordered structures of AZ sub(4)ICD are systematically investigated by a combination of thermal, microscopic, scattering, and simulation techniques. Wide-angle X-ray diffractions of oriented AZ sub(4)ICD samples indicate that the AZ sub(4)ICD molecule itself basically forms layer structures: one is a low-ordered chiral smectic A LC phase (SmA) with 5.61 nm layer periodicity at high temperatures, and two highly ordered smectic crystal (SmCr sub(1) and SmCr sub(2)) phases are subsequently formed at lower temperatures with the anticlinically tilted molecular packing structures. The helical superstructures of chiral nematic LC phase (N) can be spontaneously constructed by doping AZ sub(4)ICD chiral agents into the achiral nematic molecules. Due to the bent conformational geometry of AZ sub(4)ICD, the thermal window of blue LC phase (BP) is expanded by stabilizing the double twisted cylindrical building blocks. Remote-controllable phase transformations in the mesomorphic helical superstructures are demonstrated by tuning the wavelength of light. By taking intramolecular conformations and intermolecular interactions into account, a photochromic chiral liquid crystal is synthesized that functions as a remote-controllable molecular knob for tuning the mesomorphic helical superstructures.
Author	Choi, Yu-Jin Kim, Jin Soo Yu, Yeon-Tae Kim, Dae-Yoon Lee, Sang-A Jeong, Kwang-Un Park, Minwook Yoon, Won-Jin
Author_xml	– sequence: 1 givenname: Dae-Yoon surname: Kim fullname: Kim, Dae-Yoon organization: Polymer Materials Fusion Research Center & Department of Polymer-Nano Science and Technology, Chonbuk National University, Jeonbuk, 561-756, Jeonju, Korea – sequence: 2 givenname: Sang-A surname: Lee fullname: Lee, Sang-A organization: Polymer Materials Fusion Research Center & Department of Polymer-Nano Science and Technology, Chonbuk National University, Jeonbuk, 561-756, Jeonju, Korea – sequence: 3 givenname: Minwook surname: Park fullname: Park, Minwook organization: Polymer Materials Fusion Research Center & Department of Polymer-Nano Science and Technology, Chonbuk National University, Jeonbuk, 561-756, Jeonju, Korea – sequence: 4 givenname: Yu-Jin surname: Choi fullname: Choi, Yu-Jin organization: Polymer Materials Fusion Research Center & Department of Polymer-Nano Science and Technology, Chonbuk National University, Jeonbuk, 561-756, Jeonju, Korea – sequence: 5 givenname: Won-Jin surname: Yoon fullname: Yoon, Won-Jin organization: Polymer Materials Fusion Research Center & Department of Polymer-Nano Science and Technology, Chonbuk National University, Jeonbuk, 561-756, Jeonju, Korea – sequence: 6 givenname: Jin Soo surname: Kim fullname: Kim, Jin Soo organization: Division of Advanced Materials Engineering, Chonbuk National University, Jeonbuk, 561-756, Jeonju, Korea – sequence: 7 givenname: Yeon-Tae surname: Yu fullname: Yu, Yeon-Tae organization: Division of Advanced Materials Engineering, Chonbuk National University, Jeonbuk, 561-756, Jeonju, Korea – sequence: 8 givenname: Kwang-Un surname: Jeong fullname: Jeong, Kwang-Un email: kujeong@jbnu.ac.kr organization: Polymer Materials Fusion Research Center & Department of Polymer-Nano Science and Technology, Chonbuk National University, Jeonbuk, 561-756, Jeonju, Korea
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Snippet	A programed light‐responsive chiral liquid crystal (LC) containing four photochromic azobenzene moieties covalently connected to a central bicyclic chiral core... A programed light-responsive chiral liquid crystal (LC) containing four photochromic azobenzene moieties covalently connected to a central bicyclic chiral core...
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SubjectTerms	Doping Helical helical superstructure Knobs layer structure light-responsive liquid crystal Liquid crystals Molecular structure Nematic self-assembly Superstructures Tuning
Title	Remote-Controllable Molecular Knob in the Mesomorphic Helical Superstructures
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