Synthesis of porous nanododecahedron Co3O4/C and its application for nonenzymatic electrochemical detection of nitrite
Graphical synthesis of Co3O4/C nanocomposite and its application as a nonenzymatic electrocatalyst for nitrite. [Display omitted] •ZIF-67 acts as an ideal sacrificial template and converted to Co3O4/C with regular shape.•Co3O4/C composite exhibits highly porous, fluffy and highly surface area.•Co3O4...
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| Published in | Advanced Powder Technology Vol. 30; no. 10; pp. 2083 - 2093 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English Japanese |
| Published |
Elsevier B.V
01.10.2019
Elsevier BV |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0921-8831 1568-5527 |
| DOI | 10.1016/j.apt.2019.06.022 |
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| Abstract | Graphical synthesis of Co3O4/C nanocomposite and its application as a nonenzymatic electrocatalyst for nitrite.
[Display omitted]
•ZIF-67 acts as an ideal sacrificial template and converted to Co3O4/C with regular shape.•Co3O4/C composite exhibits highly porous, fluffy and highly surface area.•Co3O4/C composite shows high electrocatalytic activity toward NO2−.•An ultralow detection limit of 1.21 nM of the fabricated sensor for NO2− was achieved.
Porous nanododecahedron of Co3O4/C has been synthesized by calcination of the ZIF-67 in air at 400 °C and then be used as electrode material for fabricating a highly sensitive and low overpotential sensor of nitrite ion (NO2−). The structure and morphology characterization show that ZIF-67 behaves as an ideal sacrificial template for preparing Co3O4/C with regular shape. The two components of Co3O4 and carbon are uniformly distributed in the composite. Electrochemical analysis shows that the excellent electrocatalysis performance toward the oxidation of NO2− is based on the synergy of Co3O4 and carbon in the nanocomposite. At NO2− concentration from 2 nM to 8 mM, a fast response time within 3 s is revealed and 1.21 nM of detection limit is achieved. The sensor is also reliable to analysis of NO2− existed in the real samples of soil leaching liquid and macrophage supernate. |
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| AbstractList | Graphical synthesis of Co3O4/C nanocomposite and its application as a nonenzymatic electrocatalyst for nitrite.
[Display omitted]
•ZIF-67 acts as an ideal sacrificial template and converted to Co3O4/C with regular shape.•Co3O4/C composite exhibits highly porous, fluffy and highly surface area.•Co3O4/C composite shows high electrocatalytic activity toward NO2−.•An ultralow detection limit of 1.21 nM of the fabricated sensor for NO2− was achieved.
Porous nanododecahedron of Co3O4/C has been synthesized by calcination of the ZIF-67 in air at 400 °C and then be used as electrode material for fabricating a highly sensitive and low overpotential sensor of nitrite ion (NO2−). The structure and morphology characterization show that ZIF-67 behaves as an ideal sacrificial template for preparing Co3O4/C with regular shape. The two components of Co3O4 and carbon are uniformly distributed in the composite. Electrochemical analysis shows that the excellent electrocatalysis performance toward the oxidation of NO2− is based on the synergy of Co3O4 and carbon in the nanocomposite. At NO2− concentration from 2 nM to 8 mM, a fast response time within 3 s is revealed and 1.21 nM of detection limit is achieved. The sensor is also reliable to analysis of NO2− existed in the real samples of soil leaching liquid and macrophage supernate. |
| Author | Huang, Mingqiang Gao, Feng Wang, Qingxiang Qiu, Weiwei Tanaka, Hidekazu |
| Author_xml | – sequence: 1 givenname: Weiwei surname: Qiu fullname: Qiu, Weiwei email: Qiuweiwei@mnnu.edu.cn organization: College of Chemistry and Environment, Fujian Province Key Laboratory of Morden Analytical Science and Separation Technology, Minnan Normal University, Zhangzhou 363000, PR China – sequence: 2 givenname: Hidekazu surname: Tanaka fullname: Tanaka, Hidekazu email: hidekazu@riko.shimane-u.ac.jp organization: Department of Chemistry, Graduate School of Science and Engineering, Shimane University, 1060 Nishikawatsu, Matsue, Shimane 690-8504, Japan – sequence: 3 givenname: Feng surname: Gao fullname: Gao, Feng organization: College of Chemistry and Environment, Fujian Province Key Laboratory of Morden Analytical Science and Separation Technology, Minnan Normal University, Zhangzhou 363000, PR China – sequence: 4 givenname: Qingxiang surname: Wang fullname: Wang, Qingxiang organization: College of Chemistry and Environment, Fujian Province Key Laboratory of Morden Analytical Science and Separation Technology, Minnan Normal University, Zhangzhou 363000, PR China – sequence: 5 givenname: Mingqiang surname: Huang fullname: Huang, Mingqiang organization: College of Chemistry and Environment, Fujian Province Key Laboratory of Morden Analytical Science and Separation Technology, Minnan Normal University, Zhangzhou 363000, PR China |
| BackLink | https://cir.nii.ac.jp/crid/1873398392726568448$$DView record in CiNii |
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| Title | Synthesis of porous nanododecahedron Co3O4/C and its application for nonenzymatic electrochemical detection of nitrite |
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