In-Depth Characterization of Two Bioactive Coatings Obtained Using MAPLE on TiTaZrAg

TiZrTaAg alloy is a remarkable material with exceptional properties, making it a unique choice among various industrial applications. In the present study, two types of bioactive coatings using MAPLE were obtained on a TiZrTaAg substrate. The base coating consisted in a mixture of chitosan and biogl...

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Published inMaterials Vol. 17; no. 12; p. 2989
Main Authors Prodana, Mariana, Stoian, Andrei Bogdan, Ionita, Daniela, Brajnicov, Simona, Boerasu, Iulian, Enachescu, Marius, Burnei, Cristian
Format Journal Article
LanguageEnglish
Published Switzerland MDPI AG 18.06.2024
MDPI
Subjects
Alloys
Analysis
Atomic force microscopy
bioactive
Biocompatibility
Bioglass
Biological activity
Bones
Chitosan
Coatings
Corrosion and anti-corrosives
Corrosion rate
Corrosion resistance
Diamond pyramid hardness tests
Electrochemical impedance spectroscopy
Ellipsometry
Fourier transforms
Graphene
Industrial applications
Infrared analysis
Infrared spectroscopy
Lasers
MAPLE
Mechanical properties
Microscopy
Nanoparticles
Penetration depth
R&D
Research & development
Spectrum analysis
Substrates
Thin films
Tissue engineering
titanium alloy
Titanium alloys
Zinc oxide
Zinc oxides
Romania
United Kingdom > UK
France
United States > US
chitosan
titanium alloy
bioglass
MAPLE
bioactive
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Abstract TiZrTaAg alloy is a remarkable material with exceptional properties, making it a unique choice among various industrial applications. In the present study, two types of bioactive coatings using MAPLE were obtained on a TiZrTaAg substrate. The base coating consisted in a mixture of chitosan and bioglass in which zinc oxide and graphene oxide were added. The samples were characterized in-depth through a varied choice of methods to provide a more complete picture of the two types of bioactive coating. The analysis included Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), ellipsometry, and micro-Raman. The Vickers hardness test was used to determine the hardness of the films and the penetration depth. Film adhesion forces were determined using atomic force microscopy (AFM). The corrosion rate was highlighted by polarization curves and by using electrochemical impedance spectroscopy (EIS). The performed tests revealed that the composite coatings improve the properties of the TiZrTaAg alloy, making them feasible for future use as scaffold materials or in implantology.
AbstractList TiZrTaAg alloy is a remarkable material with exceptional properties, making it a unique choice among various industrial applications. In the present study, two types of bioactive coatings using MAPLE were obtained on a TiZrTaAg substrate. The base coating consisted in a mixture of chitosan and bioglass in which zinc oxide and graphene oxide were added. The samples were characterized in-depth through a varied choice of methods to provide a more complete picture of the two types of bioactive coating. The analysis included Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), ellipsometry, and micro-Raman. The Vickers hardness test was used to determine the hardness of the films and the penetration depth. Film adhesion forces were determined using atomic force microscopy (AFM). The corrosion rate was highlighted by polarization curves and by using electrochemical impedance spectroscopy (EIS). The performed tests revealed that the composite coatings improve the properties of the TiZrTaAg alloy, making them feasible for future use as scaffold materials or in implantology.
TiZrTaAg alloy is a remarkable material with exceptional properties, making it a unique choice among various industrial applications. In the present study, two types of bioactive coatings using MAPLE were obtained on a TiZrTaAg substrate. The base coating consisted in a mixture of chitosan and bioglass in which zinc oxide and graphene oxide were added. The samples were characterized in-depth through a varied choice of methods to provide a more complete picture of the two types of bioactive coating. The analysis included Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), ellipsometry, and micro-Raman. The Vickers hardness test was used to determine the hardness of the films and the penetration depth. Film adhesion forces were determined using atomic force microscopy (AFM). The corrosion rate was highlighted by polarization curves and by using electrochemical impedance spectroscopy (EIS). The performed tests revealed that the composite coatings improve the properties of the TiZrTaAg alloy, making them feasible for future use as scaffold materials or in implantology.TiZrTaAg alloy is a remarkable material with exceptional properties, making it a unique choice among various industrial applications. In the present study, two types of bioactive coatings using MAPLE were obtained on a TiZrTaAg substrate. The base coating consisted in a mixture of chitosan and bioglass in which zinc oxide and graphene oxide were added. The samples were characterized in-depth through a varied choice of methods to provide a more complete picture of the two types of bioactive coating. The analysis included Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), ellipsometry, and micro-Raman. The Vickers hardness test was used to determine the hardness of the films and the penetration depth. Film adhesion forces were determined using atomic force microscopy (AFM). The corrosion rate was highlighted by polarization curves and by using electrochemical impedance spectroscopy (EIS). The performed tests revealed that the composite coatings improve the properties of the TiZrTaAg alloy, making them feasible for future use as scaffold materials or in implantology.
Audience Academic
Author Ionita, Daniela
Stoian, Andrei Bogdan
Burnei, Cristian
Boerasu, Iulian
Prodana, Mariana
Brajnicov, Simona
Enachescu, Marius
AuthorAffiliation 4 Clinical Department of Orthopedics and Traumatology II, Clinical Emergency Hospital, Calea Floreasca 8, 014461 Bucharest, Romania; cristian.burnei@umfcd.ro
2 Lasers Department, National Institute for Lasers, Plasma and Radiation Physics, 409 Atomistilor Street, 077125 Magurele, Romania; brajnicov.simona@inflpr.ro
3 Center for Surface Science and Nanotechnology, National University of Science and Technology Politehnica Bucharest, 313 Splaiul Independentei, 060042 Bucharest, Romania; iulian.boerasu@cssnt-upb.ro (I.B.); marius.enachescu@cssnt-upb.ro (M.E.)
1 Department of General Chemistry, Faculty of Chemical Engineering and Biotechnologies, National University of Science and Technology Politehnica Bucharest, 313 Splaiul Independentei, 060042 Bucharest, Romania; mariana.prodana@upb.ro (M.P.); andreibstoian@yahoo.com (A.B.S.)
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Keywords chitosan
titanium alloy
bioglass
MAPLE
bioactive
Language English
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Snippet TiZrTaAg alloy is a remarkable material with exceptional properties, making it a unique choice among various industrial applications. In the present study, two...
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StartPage 2989
SubjectTerms Alloys
Analysis
Atomic force microscopy
bioactive
Biocompatibility
Bioglass
Biological activity
Bones
Chitosan
Coatings
Corrosion and anti-corrosives
Corrosion rate
Corrosion resistance
Diamond pyramid hardness tests
Electrochemical impedance spectroscopy
Ellipsometry
Fourier transforms
Graphene
Industrial applications
Infrared analysis
Infrared spectroscopy
Lasers
MAPLE
Mechanical properties
Microscopy
Nanoparticles
Penetration depth
R&D
Research & development
Spectrum analysis
Substrates
Thin films
Tissue engineering
titanium alloy
Titanium alloys
Zinc oxide
Zinc oxides
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Title In-Depth Characterization of Two Bioactive Coatings Obtained Using MAPLE on TiTaZrAg
URI https://www.ncbi.nlm.nih.gov/pubmed/38930358
https://www.proquest.com/docview/3072568148
https://www.proquest.com/docview/3072808026
https://pubmed.ncbi.nlm.nih.gov/PMC11205300
https://doaj.org/article/09c92e61278d4290b6a53d2a3c983b95
Volume 17
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