Fabrication of a novel thin-film nanocomposite (TFN) membrane containing MCM-41 silica nanoparticles (NPs) for water purification

A thin-film nanocomposite (TFN) membrane containing porous MCM-41 silica nanoparticles (NPs) was prepared by the in situ interfacial polymerization (IP) process. Aqueous m-phenyl diamine (MPD) and organic trimesoyl chloride (TMC)-NPs mixture solutions were used in the IP process. Porous MCM-41 (∼100...

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Published in	Journal of membrane science Vol. 423-424; pp. 238 - 246
Main Authors	Yin, Jun, Kim, Eun-Sik, Yang, John, Deng, Baolin
Format	Journal Article
Language	English
Published	Elsevier B.V 15.12.2012
Subjects	artificial membranes atomic force microscopy Desalination Fourier transform infrared spectroscopy hydrophilicity Interfacial polymerization MCM-41 nanoparticles nanocomposites nanoparticles permeability Polyamide polyamides polymerization roughness scanning electron microscopy silica sodium chloride sodium sulfate Thin-film nanocomposite transmission electron microscopy water purification zeta potential Polyamide Interfacial polymerization Thin-film nanocomposite MCM-41 nanoparticles Desalination
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Abstract	A thin-film nanocomposite (TFN) membrane containing porous MCM-41 silica nanoparticles (NPs) was prepared by the in situ interfacial polymerization (IP) process. Aqueous m-phenyl diamine (MPD) and organic trimesoyl chloride (TMC)-NPs mixture solutions were used in the IP process. Porous MCM-41 (∼100nm) and non-porous spherical silica NPs (∼100nm) were synthesized and used as the fillers to fabricate the TFN membrane at concentrations ranging from 0 to 0.1wt%. The membranes were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), atomic force microscopy (AFM) and attenuated total reflection Fourier transform infrared (ATR FT-IR) spectroscopy, and their performances were evaluated based on the water permeability and salt rejection. Results indicated that the MCM-41 NPs dispersed well in polyamide (PA) thin-film layer and improved membrane performances under optimal concentrations. By increasing concentration of MCM-41 NPs, hydrophilicity, roughness and zeta potential of TFN membranes all increased. Notably, the permeate water flux increased from 28.5±1.0 to 46.6±1.1L/m2h with the incorporation of MCM-41 NPs, while maintaining high rejections of NaCl and Na2SO4 (97.9±0.3% and 98.5±0.2%, respectively). A comparison between the membranes with non-porous silica NPs (S-TFN) and with the porous MCM-41 NPs (M-TFN) suggested that the internal pores of MCM-41 NPs contributed significantly to the increase of water permeability. ► Synthesis of nanoscale ordered mesoporous silica (MCM-41). ► Fabrication of thin-film nano composite (TFN) membrane by MCM-41 NPs. ► Effect of concentration of nano-fillers and TFN surface characteristics. ► Comparison between the TFN membranes with non-porous NPs and with porous NPs. ► The role of internal pores of fillers was explored.
AbstractList	A thin-film nanocomposite (TFN) membrane containing porous MCM-41 silica nanoparticles (NPs) was prepared by the in situ interfacial polymerization (IP) process. Aqueous m-phenyl diamine (MPD) and organic trimesoyl chloride (TMC)-NPs mixture solutions were used in the IP process. Porous MCM-41 (∼100nm) and non-porous spherical silica NPs (∼100nm) were synthesized and used as the fillers to fabricate the TFN membrane at concentrations ranging from 0 to 0.1wt%. The membranes were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), atomic force microscopy (AFM) and attenuated total reflection Fourier transform infrared (ATR FT-IR) spectroscopy, and their performances were evaluated based on the water permeability and salt rejection. Results indicated that the MCM-41 NPs dispersed well in polyamide (PA) thin-film layer and improved membrane performances under optimal concentrations. By increasing concentration of MCM-41 NPs, hydrophilicity, roughness and zeta potential of TFN membranes all increased. Notably, the permeate water flux increased from 28.5±1.0 to 46.6±1.1L/m2h with the incorporation of MCM-41 NPs, while maintaining high rejections of NaCl and Na2SO4 (97.9±0.3% and 98.5±0.2%, respectively). A comparison between the membranes with non-porous silica NPs (S-TFN) and with the porous MCM-41 NPs (M-TFN) suggested that the internal pores of MCM-41 NPs contributed significantly to the increase of water permeability. ► Synthesis of nanoscale ordered mesoporous silica (MCM-41). ► Fabrication of thin-film nano composite (TFN) membrane by MCM-41 NPs. ► Effect of concentration of nano-fillers and TFN surface characteristics. ► Comparison between the TFN membranes with non-porous NPs and with porous NPs. ► The role of internal pores of fillers was explored. A thin-film nanocomposite (TFN) membrane containing porous MCM-41 silica nanoparticles (NPs) was prepared by the in situ interfacial polymerization (IP) process. Aqueous m-phenyl diamine (MPD) and organic trimesoyl chloride (TMC)-NPs mixture solutions were used in the IP process. Porous MCM-41 (∼100nm) and non-porous spherical silica NPs (∼100nm) were synthesized and used as the fillers to fabricate the TFN membrane at concentrations ranging from 0 to 0.1wt%. The membranes were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), atomic force microscopy (AFM) and attenuated total reflection Fourier transform infrared (ATR FT-IR) spectroscopy, and their performances were evaluated based on the water permeability and salt rejection. Results indicated that the MCM-41 NPs dispersed well in polyamide (PA) thin-film layer and improved membrane performances under optimal concentrations. By increasing concentration of MCM-41 NPs, hydrophilicity, roughness and zeta potential of TFN membranes all increased. Notably, the permeate water flux increased from 28.5±1.0 to 46.6±1.1L/m²h with the incorporation of MCM-41 NPs, while maintaining high rejections of NaCl and Na₂SO₄ (97.9±0.3% and 98.5±0.2%, respectively). A comparison between the membranes with non-porous silica NPs (S-TFN) and with the porous MCM-41 NPs (M-TFN) suggested that the internal pores of MCM-41 NPs contributed significantly to the increase of water permeability.
Author	Deng, Baolin Yang, John Kim, Eun-Sik Yin, Jun
Author_xml	– sequence: 1 givenname: Jun surname: Yin fullname: Yin, Jun organization: Department of Civil & Environmental Engineering, University of Missouri, Columbia, MO 65211, USA – sequence: 2 givenname: Eun-Sik surname: Kim fullname: Kim, Eun-Sik organization: Department of Civil & Environmental Engineering, University of Missouri, Columbia, MO 65211, USA – sequence: 3 givenname: John surname: Yang fullname: Yang, John organization: Department of Agriculture and Environmental Sciences, Lincoln University, Jefferson city, MO 65101, USA – sequence: 4 givenname: Baolin surname: Deng fullname: Deng, Baolin email: dengb@missouri.edu organization: Department of Civil & Environmental Engineering, University of Missouri, Columbia, MO 65211, USA
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Snippet	A thin-film nanocomposite (TFN) membrane containing porous MCM-41 silica nanoparticles (NPs) was prepared by the in situ interfacial polymerization (IP)...
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SubjectTerms	artificial membranes atomic force microscopy Desalination Fourier transform infrared spectroscopy hydrophilicity Interfacial polymerization MCM-41 nanoparticles nanocomposites nanoparticles permeability Polyamide polyamides polymerization roughness scanning electron microscopy silica sodium chloride sodium sulfate Thin-film nanocomposite transmission electron microscopy water purification zeta potential
Title	Fabrication of a novel thin-film nanocomposite (TFN) membrane containing MCM-41 silica nanoparticles (NPs) for water purification
URI	https://dx.doi.org/10.1016/j.memsci.2012.08.020 https://www.proquest.com/docview/1803102939
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