Removal of anionic dye eosin Y from aqueous solution using ethylenediamine modified chitosan
In this study, chitosan was cross-linked with ethylenediamine (EDA) to prepare an outstanding sorbent for the removal of anionic dye eosin Y from aqueous solution. FTIR, DTG, XPS and zeta potential analysis were used to characterize the sorbent. The effect of particle size, solution pH, agitation ra...
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| Published in | Carbohydrate polymers Vol. 84; no. 4; pp. 1350 - 1356 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Kidlington
Elsevier Ltd
02.04.2011
Elsevier |
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| Online Access | Get full text |
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| Abstract | In this study, chitosan was cross-linked with ethylenediamine (EDA) to prepare an outstanding sorbent for the removal of anionic dye eosin Y from aqueous solution. FTIR, DTG, XPS and zeta potential analysis were used to characterize the sorbent. The effect of particle size, solution pH, agitation rate, temperature, adsorbent dosage (50–500mg/L), contact time (10min–24h) and initial concentration of dye (50–300mg/L) on the adsorption process was investigated. Langmuir and Freundlich adsorption models were applied to describe the isotherms and isotherm constants, and the data fitted well with Langmuir model with a maximum adsorption capacity of 294.12mg/g at 25°C. Kinetic studies followed the pseudo second-order rate model, which indicated that the chemisorption is the rate-limiting step. Thermodynamic parameters such as enthalpy change (ΔH°=−5.004kJ/mol), free energy change (ΔG°<0) and entropy change (ΔS°=−11.656J/(molK)) indicate the exothermic and spontaneous nature of adsorption. |
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| AbstractList | In this study, chitosan was cross-linked with ethylenediamine (EDA) to prepare an outstanding sorbent for the removal of anionic dye eosin Y from aqueous solution. FTIR, DTG, XPS and zeta potential analysis were used to characterize the sorbent. The effect of particle size, solution pH, agitation rate, temperature, adsorbent dosage (50–500mg/L), contact time (10min–24h) and initial concentration of dye (50–300mg/L) on the adsorption process was investigated. Langmuir and Freundlich adsorption models were applied to describe the isotherms and isotherm constants, and the data fitted well with Langmuir model with a maximum adsorption capacity of 294.12mg/g at 25°C. Kinetic studies followed the pseudo second-order rate model, which indicated that the chemisorption is the rate-limiting step. Thermodynamic parameters such as enthalpy change (ΔH°=−5.004kJ/mol), free energy change (ΔG°<0) and entropy change (ΔS°=−11.656J/(molK)) indicate the exothermic and spontaneous nature of adsorption. |
| Author | Huang, Xiao-Yi Bin, Jian-Ping Bu, Huai-Tian Zeng, Ming-Hua Jiang, Gang-Biao |
| Author_xml | – sequence: 1 givenname: Xiao-Yi surname: Huang fullname: Huang, Xiao-Yi organization: College of Natural Resources and Environment, South China Agricultural University, Guangzhou 510642, China – sequence: 2 givenname: Jian-Ping surname: Bin fullname: Bin, Jian-Ping organization: Department of Cardiology, Nanfang Hospital, Southern Medical University, Guangzhou 510515, China – sequence: 3 givenname: Huai-Tian surname: Bu fullname: Bu, Huai-Tian organization: SINTEF Materials and Chemistry, P.O. Box 124 Blindern, N-0314 Oslo, Norway – sequence: 4 givenname: Gang-Biao surname: Jiang fullname: Jiang, Gang-Biao email: jgb3h@163.com organization: College of Natural Resources and Environment, South China Agricultural University, Guangzhou 510642, China – sequence: 5 givenname: Ming-Hua surname: Zeng fullname: Zeng, Ming-Hua email: zmh@mailbox.gxnu.edu.cn organization: The Key Laboratory for the Chemistry and Molecular Engineering of Medicinal Resources (Ministry of Education), School of Chemistry and Chemical Engineering of Guangxi Normal University, Guilin 541004, China |
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| Keywords | Effluent treatment Eosin Y Chitosan Adsorption Chitosan derivative Sorbent Epichlorhydrin Adsorption isotherm Temperature effect Eosin Aqueous medium Crosslinked polymer Organic dye Liquid solid adsorption Crosslinking Experimental study Organic adsorbent Diamine Chemical modification Chitosan derivatives Preparation Oside polymer Kinetics Heat of adsorption Successive reaction |
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| Snippet | In this study, chitosan was cross-linked with ethylenediamine (EDA) to prepare an outstanding sorbent for the removal of anionic dye eosin Y from aqueous... |
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| SubjectTerms | Adsorbents Adsorption agitation Applied sciences aqueous solutions Chemistry Chitosan Chitosan derivative crosslinking Effluent treatment energy enthalpy entropy Eosin Y Exact sciences and technology Fourier transform infrared spectroscopy General and physical chemistry heat production Natural polymers particle size Physicochemistry of polymers Sorbent sorption isotherms Starch and polysaccharides Surface physical chemistry temperature X-ray photoelectron spectroscopy zeta potential |
| Title | Removal of anionic dye eosin Y from aqueous solution using ethylenediamine modified chitosan |
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